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181.
Multiphase flow metering with operationally robust, low-cost real-time systems that provide accuracy across a broad range of produced volumes and fluid properties, is a requirement across a range of process industries, particularly those concerning petroleum. Especially the wide variety of multiphase flow profiles that can be encountered in the field provides challenges in terms of metering accuracy. Recently, low-field magnetic resonance (MR) measurement technology has been introduced as a feasible solution for the petroleum industry. In this work, we study two phase air-water horizontal flows using MR technology. We show that low-field MR technology applied to multiphase flow has the capability to measure the instantaneous liquid holdup and liquid flow velocity using a constant gradient low flip angle CPMG (LFA-CPMG) pulse sequence. LFA-CPMG allows representative sampling of the correlations between liquid holdup and liquid flow velocity, which allows multiphase flow profiles to be characterized. Flow measurements based on this method allow liquid flow rate determination with an accuracy that is independent of the multiphase flow profile observed in horizontal pipe flow for a wide dynamic range in terms of the average gas and liquid flow rates. 相似文献
182.
Rate constant measurements for initial addition reactions of radicals at the propagation step of photo‐polymerization as studied by pulsed EPR spectroscopy 下载免费PDF全文
Yusuke Miyake Yutaka Marushima Hirona Takahashi Nobuyuki Akai Kazuhiko Shibuya Akio Kawai 《Journal of Physical Organic Chemistry》2016,29(9):468-475
Pulsed EPR spectroscopy was employed to determine reaction rate constants at an early stage of addition reactions in radical polymerizations triggered by four initiator radicals, which were generated by photodissociation of four parent molecules. Two monomers (tert‐butylacrylate and tert‐butylmethacrylate) were examined as reactant. Stern–Volmer analysis on the measured decay time of electron spin echo intensity of reacting radicals provides rate constants for addition reactions. We focused on rate constants for the second step reaction between monomer and adduct radical that is produced by the first step addition reaction between initiator radical and monomer. The rate constant measured by pulsed EPR was evaluated by theoretical calculations in the light of (1) enthalpy difference between product radical and reactants and (2) charge transfer interaction between reacting radical and monomer. Copyright © 2016 John Wiley & Sons, Ltd. 相似文献
183.
本文基于飞秒激光模间拍频法实现多波长相位式绝对距离测量, 通过改变光频梳重复频率合成波长扩大测距量程, 并采用监测臂和双快门切换系统补偿和消除由电路产生的相位差单向漂移和大幅抖动. 实验中以20倍重复频率的拍频进行测量, 在30 min内相位测量的标准偏差为0.022°; 与双频激光干涉仪比对1125 mm行程内位移测量结果, 测距精度优于50 μm; 实验验证了合成波长方法扩大量程方案的可行性, 获得的测距重复性优于3 μm, 该系统理论上可扩展量程至7.5 km. 相似文献
184.
如何实现高精度的测量是现代制造业及微电子技术领域的热点问题之一. 基于微纳米测头的三坐标测量机是当前实现高精度测量的重要手段. 随着测量尺寸的减小, 常用的纳米/微纳尺度的测头与待测表面之间形成静态接触, 其表面相互作用成为了影响其测量精度和可靠性的关键因素之一. 本文基于一种触发式振动测头, 研究了其动力学模型, 并通过对测头纳米尺度表面相互作用的理论分析及数值模拟, 确立了测头振动参数与表面相互作用之间的关联. 实验研究表明, 参数优化后的谐振微纳测头能有效抑制表面作用带来的干扰, 提高测量精度. 相似文献
185.
Accurate measurement of gas turbine blades’ temperature is one of the greatest challenges encountered in gas turbine temperature measurements. Within an enclosed gas turbine environment with surfaces of varying temperature and low emissivities, a new challenge is introduced into the use of radiation thermometers due to the problem of reflection error. A method for correcting this error has been proposed and demonstrated in this work through computer simulation and experiment. The method assumed that emissivities of all surfaces exchanging thermal radiation are known. Simulations were carried out considering targets with low and high emissivities of 0.3 and 0.8 respectively while experimental measurements were carried out on blades with emissivity of 0.76. Simulated results showed possibility of achieving error less than 1% while experimental result corrected the error to 1.1%. It was thus concluded that the method is appropriate for correcting reflection error commonly encountered in temperature measurement of gas turbine blades. 相似文献
186.
Polystyrene latex (PSL) nanoparticle (NP) sample is one of the most widely used standard materials. It is used for calibration of particle counters and particle size measurement tools. It has been reported that the measured NP sizes by various methods, such as Differential Mobility Analysis, dynamic light scattering (DLS), optical microscopy (OM), scanning electron microscopy (SEM) and atomic force microscopy (AFM), differ from each other. Deformation of PSL NPs on mica substrate has been reported in AFM measurements: the lateral width of PSL NPs is smaller than their vertical height. To provide a reliable calibration standard, the deformation must be measured by a method that can reliably visualize the entire three dimensional (3D) shape of the PSL NPs. Here we present a method for detailed measurement of PSL NP 3D shape by means of electron tomography in a transmission electron microscope. The observed shape of the PSL NPs with 100 nm and 50 nm diameter were not spherical, but squished in direction perpendicular to the support substrate by about 7.4% and 12.1%, respectively. The high difference in surface energy of the PSL NPs and that of substrate together with their low Young modulus appear to explain the squishing of the NPs without presence of water film. 相似文献
187.
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189.
《Current Applied Physics》2015,15(3):302-306
We propose a method for simultaneously measuring the front and back surface profiles of transparent optical components. The proposed method combines dual wavelength transmission deflectometry with liquids to record distorted phases at different wavelengths, and then numerically reconstructs the three-dimensional phase information to image the front and back surfaces of the lens. We propose a theoretical model to determine the surface information, and the imaging of achromatic lenses is experimentally demonstrated. Unlike conventional transmission deflectometry, our proposed method supports direct observation of the front and back surface profiles of the optical elements. Compared with other techniques such as interferometry, the proposed setup is simpler to align, has lower cost, and does not require coherent illumination. The proposed method can be applied to normal transmission deflectometry for determining the three-dimensional surface profiles of optical components. 相似文献
190.