HPLC法测定阿奇霉素葡萄糖注射液中阿奇霉素的含量

利用高效液相色谱法，以VP-ODS型色谱柱，乙腈-异丙醇-水-氨水（60：25：15：0.1)为流动相，于210nm波长处测定了阿奇霉素葡萄糖注射液中阿奇霉素葡萄糖注射液中阿奇霉素的含量。阿奇霉素的浓度在0.75-1.75mg/mL线性关系良好，线性方程的A=881910.4c-16208.2，相关系数r=0.9999。阿奇霉素的平均回收率为99.59%，测定结果的相对标准偏差为1.31%。     

Measurement of small-signal and large-signal responses of packaged laser modules at high temperature

In this paper, the pulsed injection method is extended to measure the chip temperature of various packaged laser modules, such as the DFB laser modules, the FP laser modules, and the EML laser modules. An optimal injection condition is obtained by investigating the dependence of the lasing wavelength on the width and period of the injection pulse in a relatively wide temperature range. The small-signal frequency responses and large-signal performances of packaged laser modules at different chip temperature are measured. The adiabatic small-signal modulation characteristics of packaged LD are first extracted. In the large-signal measurement, the effects of chip temperature, bias current and driving signal on the performances of the laser modules are discussed. It has been found that the large-signal performances of the EML modules depend on the different red-shift speeds of the DFB and EAM sections as chip temperature varying, and the optimal characteristics may be achieved at higher temperature.     

ECR-SFC轴向注入系统聚束器效率的研究

为了减少目前SFC轴向注入系统中聚束器杂散电场对束流轴向注入效率的影响, 提高新系统中SFC的束流俘获效率, 参考原始设计, 对目前聚束器的电极结构进行了设计改进. 两种情况下的聚束器杂散场对注入效率影响的计算表明, 改进后0B02的聚束效率较目前有较大提高. 同时计算了束流空间电荷效应对聚束效率的影响, 据此对新SFC轴向注入系统中聚束器的位置进行了重新调整.     

Fast Fourier Continuous Cyclic Voltammetry at Gold Ultramicroelectrode in Flowing Solution for Determination of Ultra Trace Amounts of Penicillin G

In this work, for the first time a fast continuous cyclic voltammetry was used as a highly sensitive detection method for Penicillin G in a flow‐injection system. A special computer‐based numerical calculation method (using Fast Fourier Transformation) is introduced here for enhancing the analyte signal and noise reduction. During the measurements, the potential waveform (consists of potential steps for cleaning, stripping and potential ramp) was continuously applied on an Au disk microelectrode (with a radius 12.5 μm in radius). The stripping time was less than 200 ms. Effects of rest potential, sweep rate, and delay time on the sensitivity of the method were investigated. The limit of detection of the method was 1.0 × 10^?11 M. The detection limit of the method is 660 times lower than the most sensitive reported method. The relative standard deviation of the method at 1.0×10^?7 M of Penicillin G was 2.7% for 10 runs.     

Theoretical and computational studies of vectorial processes in biomolecular systems

Efficient vectorial processes such as the transduction of bioenergy and signals are characteristics that strikingly distinguish living systems from inanimate materials. Recent developments in biophysical and biochemical techniques have provided new information about the structure, dynamics and interaction of biomolecules involved in vectorial life processes at multiple length and temporal scales. This wealth of data makes it possible to carry out theoretical and computational studied of key mechanistic questions associated with complex life processes at an unprecedented level. Using two “vectorial biomolecular machines”, myosin and cytochrome c oxidase, as examples, we discuss the identification of interesting and biologically relevant questions that require thorough theoretical analysis. Technical challenges and recent progress related to these theoretical investigations are briefly summarized     

Pulsed pump: Thermal effects in solid state lasers under super-Gaussian pulses

Solid state laser (SSL) powers can be realistically scaled when pumped by a real, efficient and multimode pulse. In this work, a fourth-order super-Gaussian pulse was assumed as a pump for SSL’s and a complete analytical expression for the thermal phase shift is given. Moreover, the focal length of thermal lens in paraxial ray approximation regime was studied. The results when applied to a Ti: sapphire crystal show an appreciable correction for abberation compared to a top-hat pulse.     

激光二极管泵浦的高重复频率Nd：YAG激光器

报道两个１．５Ｗ连续激光二极管端面泵浦的声光调ＱＮｄ：ＹＡＧ激光器，输出激光脉冲的最高重复频率为３０ｋＨｚ重复频率１ｋＨｚ时，最窄脉宽为１２ｎｓ，最高峰值功率为１２．１ｋＷ。     

半导体激光泵浦预激光锁模调Q固体激光器研究

报道半导体激光侧面泵浦预激光锁模调Ｑ的Ｎｄ：ＹＡＧ固体板条激光器，预激光锁模调Ｑ的激光脉冲宽度为３６ｐｓ，调Ｑ包纤各心的锁模单脉冲能量超过７μＪ，相应的峰值功率达２００ｋＷ。     

断续喷洒去溶电热雾化法在电感耦合等离子体原子发射光谱方法中的应用研究

本文所讨论的电热雾化法是采用继续喷洒去溶技术,使试样在石墨炉表面逐步积累的进样方法。文章简要介绍了实验条件的选择和控制以及石墨炉装置的结构,探讨了提高电热雾化法相对检测能力的途径。实验结果表明:谱线黑度值与试样积累时间的对数值之间具有较好的线性关系。