基于单片机控制的实验线路故障诊断系统

介绍了基于单片机控制技术的强电实验线路故障自动诊断系统的结构及功能,阐述了系统硬件设计、软件设计的基本原理．     

Numerical simulation and experimental validation of heat transfer within rotating flows for three‐dimensional non‐axisymmetric,turbulent conditions

A control volume type numerical methodology for the analysis of steady three‐dimensional rotating flows with heat transfer, in both laminar and turbulent conditions, is implemented and experimentally tested. Non‐axisymmetric momentum and heat transfer phenomena are allowed for. Turbulent transport is alternatively represented through three existing versions of the k–ε model that were adjusted to take into account the turbulence anisotropy promoted by rotation, streamline curvature and thermal buoyancy. Their relative performance is evaluated by comparison of calculated local and global heat balances with those obtained through measurements in a laboratory device. A modified version of the Lam and Bremhorst, low Reynolds number model is seen to give the best results. A preliminary analysis focused on the flow structure and the transfer of heat is reported. Copyright © 2002 John Wiley & Sons, Ltd.     

对2005年高考试题中关于螺旋测微计实验试题的解析与拓展

解析了2005年普通高等学校全国联考(理综卷)中考察螺旋测微计原理的实验填空题,并给出了3方面的拓展:不常见的游标卡尺、圆弧游标、具有游标的螺旋测微计.     

浅析用图像法处理实验数据

指出了图像法在解决物理问题中的优势及应注意的问题,并对用图像法处理实验数据的考题进行了归类．     

Qualitative Theory and Identification of Dynamic System with One Degree of Freedom

Dynamic systems described by nonlinear differential equations of the second order are studied. It is assumed that certain preliminary information on the dissipative or elastic characteristics of systems is known. A new approach is demonstrated to obtaining full information on unknown or partially known characteristics of a system from measurements of not only displacements but also velocities and accelerations __________ Published in Prikladnaya Mekhanika, Vol. 41, No. 6, pp. 139–143, June 2005.     

垂直上升管内液体横掠流动传热特性研究

本文对单相水和单相油横掠流动时的平均换热特性进行了实验研究,对试验的结果进行了分析和讨论,并对实验数据进行关联,得到了垂直上升管内单相水和单相油横掠流动时的换热准则关系式。结果表明,狭窄空间条件下的液体横掠柱体时的流动换热对液相Re数的依赖,较大空间条件下的流动换热相比明显减小,并对单相水和单相油横掠流动时的换热性能进行了比较。     

微型硅谐振式力传感器的振动分析

介绍了谐振式力传感器的工作原理，并从理论上和实验上对中科院合肥智能所研制的第一代微型硅谐振梁（３×０．４×０．０４５ｍｍ＾３）式测力传感器进行了全面的振动分析，所得结构为其进一步优化设计提供了科学根据，文中使用的实验分析方法，为其它微小物体的动态和识别提供了一条有效途径。     

正交试验法优化CS汽化吸附条件

通过正交试验设计,优化了影响西埃斯(CS)标准样品管制备的参数:汽化温度、采样流速、采样时间。结果表明,CS标准样品管的最佳吸附条件为汽化吸附温度:260℃,采样N2流速:330mL/min,采样时间:15min。在15~1500ng范围内,色谱峰面积与进样量有良好的线性关系,线性相关系数为0.9995,检出限为6.0ng。     

Compatibility Studies of Multicomponent Tablet Formulations. DSC and experimental mixture design

An experimental mixture design was applied to a differential scanning calorimetry (DSC) study performed to evaluate naproxen compatibility in tablet formulations consisting of four classic excipients (sorbitol, sodium carboxymethylcellulose, poly(ethylene glycol) 20000 and Veegum) each in adequate concentration ranges accounting for the relevant values actually used in pharmaceutical formulations. Twenty-seven different tablets were obtained from as many mixtures prepared according to the experimental design plan and analyzed in a random order by DSC. Statistical evaluation of experimental data enabled correlation of both enthalpy and onset temperature variations of drug melting endotherm (selected as responses indicative of the presence of drug-excipient interactions) with the mixture composition. Variance analysis (Anova) confirmed the reliability of the postulated polynomial model in providing adequate prediction of true system behaviour. This revised version was published online in August 2006 with corrections to the Cover Date.     

Validation of an analytical method to determine trace metal impurities in fluoride compounds by flame atomic absorption spectroscopy

 The development of an analytical method for the determination of some heavy metals (Fe, Cu, Co, Zn and Ni) in fluoride compounds [Cu(BF₄)₂, Sn(BF₄)₂, Pb(BF₄)₂ and HBF₄] by flame atomic absorption spectroscopy is described. This method is to be used as a routine analytical method in an industrial quality control laboratory. To this end the "performance characteristics" of an instrumental analytical method such as matrix effects, sensitivity, linearity, detection and quantitation limits, precision and accuracy were evaluated for every system under study. The results of these investigations showed that non-spectral interferences (due to the presence of large concentrations of major metals such as Cu, Sn and Pb) were observed. Nevertheless it was possible to define a matrix concentration interval where matrix effects were not statistically significant, and therefore a direct calibration approach could be used as the calibration tool whenever the major metal concentration was not higher than 40×10^–3 kg l^–1. A guide to the developement of an analytical method for trace metal determination is provided. General tools for quality control have been used in order to show how an analytical method can be tested daily and evaluated in a convenient manner. Received: 29 January 1997 Accepted: 11 March 1997