Fiber-Optic pH Sensor

The new enhancement in the determination of pH using optical fiber system is described here. This work uses the membrane made of cellulose acetate membrane for reagent immobilization and congo red (pK_a 3.7) and neutral red (pK_a 7.2) as pH indicators. An effective covalent chemical binding procedure is used to immobilize the indicators. The response time, reversibility, linear range, reproducibility, and long-term stability of fiber optic sensor with congo red as well as neutral red have been determined. The linear range measured for the sensor based on the congo red and neutral red is 4.2-6.3 and 4.1-9.0, respectively. The response time of sensor membrane is measured by varying the substance pH values between 11.0 and 2.0.     

一种新颖的涂层光纤传感器

作者提出一种新型的涂层光纤传感器,传感头是在裸光纤外周涂以SnO₂薄层。理论推知,它对还原性液体敏感。对甲醇溶液浓度进行测量的结果与理论预期相符。测量范围为0～90%体积浓度。分辨率为1.3%体积浓度。     

Data handling in HPLC-diode array UV-spectrometry

Summary The mathematical resolution of overlapped chromatographic peaks obtained in HPLC with a diode array UV detector has received considerable attention recently. The purpose of the proposed methods is the quantitation and identification of unknown solutes in complex mixtures by an efficient use of all available data. Basically two approaches have been proposed: the first one resolves the concentration profiles and calculates the pure spectra by applying a minimal number of assumptions, which is denoted self-modeling-curve resolution. The second one is based on a match of pure spectra available in a spectral library with the measured mixture spectra. In this paper both approaches are evaluated with respect to their performance to provide the pure spectra and an accurate quantitation of the concentrations.     

Enzymatic Determination of Glucose by Optical-Fiber Sensor Sequential Injection Renewable Surface Spectrophotometry

Introduction Determinationofglucoseisrequiredinmedicine industry,foodindustry,clinicaldiagnosisaswellas variousresearchfields.Therefore,intensiveefforts havebeendirectedtothedevelopmentofanalytical methodsfordeterminationofglucose,suchasthose basedonbiose…     

模糊传感器训练算法

本文提出了模糊传感器的一种分段式训练调参方法。对温度模糊传感器的仿真结果表明，该方法能在不同的测量结构下，较好地解决人类感知温度的模糊语言描述问题。     

新型自扫描激光干涉系统

本文介绍了一种新型自扫描激光干涉系统的原理和结构。该系统采用自扫描光电二极管列阵（以下简称ＳＳＰＤＡ）接收器件，实现对干涉仪信号的调制，使测量信号转换成交流信号，避免了直流放大器零点漂移，消除了低频干扰。实验证明，该系统在采用普通器件的情况下，其分辨率优于０．０２μｍ。     

A computer controlled continuous dilution dilatometer for the determination of solute molar volumes and direct measurement of reaction volumes in solution

The design and operation of a computer controlled continuous dilution dilatometer utilizing a diode array detection system is presented. To test the accuracy and reproducibility of the technique, apparent molar volumes of dilute aqueous solutions of potassium ferricyanide and potassium ferrocyanide have been measured. To provide supporting data for high pressure studies of reaction volumes and molar volume change in solutions of high ionic strength, study of these electrolytes was extended by dilution into 0.1M and 1.0M potassium nitrate solutions rather than extrapolation to zero ionic strength as is normal. In addition, the system has been used to determine reaction volumes of some acid-base reactions by direct measurement, using the equipment as an automatic titration dilatometer.     

利用4400系统构造具有光学多道分析功能的信号处理系统

基于4400系统,通过引入光电二极管列阵作为传感器,构造了具有光学多道分析功能的信号处理系统。利用该系统对实际的激光空间分布进行了描绘,给出了高斯场分布的相应参数。通过进一步观测p偏振光在K9玻璃上下表面反射光强比(γ)的角度调制曲线,获得了玻璃表面层的光学参数。实验结果表明,该系统测量精度高,可应用在激光时间信号及空间场分布的表征与测量领域。     

La détection infrarouge avec les plans focaux non refroidis : état de l'artUncooled focal plane infrared detectors: the state of the art

The emergence of uncooled detectors has opened new opportunities for IR detection for both military and commercial applications. Development of such devices involves a lot of trade-offs between the different parameters that define the technological stack. These trade-offs explain the number of different architectures that are under worldwide development. The key factor is to find a high sensitivity and low noise thermometer material compatible with silicon technology in order to achieve high thermal isolation in the smallest area as possible. Ferroelectric thermometer based hybrid technology and electrical resistive thermometer based (microbolometer) technology are under development. LETI and ULIS have chosen from the very beginning to develop first a monolithic microbolometer technology fully compatible with commercially available CMOS technology and secondly amorphous silicon based thermometer. This silicon approach has the greatest potential for reducing infrared detector manufacturing cost. After the development of the technology, the transfer to industrial facilities has been performed in a short period of time and the production is now ramping up with ULIS team in new facilities. LETI and ULIS are now working to facilitate the IRFPA integration into equipment in order to address a very large market. Achievement of this goal needs the development of smart sensors with on-chip advanced functions and the decrease of manufacturing cost of IRFPA by decreasing the pixel pitch and simplifying the vacuum package. We present in this paper the technology developed by CEA/LETI and its improvement for being able to designs 384×288 and 160×120 arrays with a pitch of 35 μm. Thermographic application needs high stability infrared detector with a precise determination of the amount of absorbed infrared flux. Hence, infrared detector with internal temperature stabilized shield has been developed and characterized. These results will be presented. To cite this article: J.-L. Tissot, C. R. Physique 4 (2003).     

连续表面微透镜列阵元件检测

系统分析了连续表面微透镜列阵的几何参量和光学性能的检测方法和评价标准,针对典型的折射型聚焦列阵元件,给出其结构尺寸及光学性能的测试结果,两者结果一致.从而建立了一套通过测试元件的几何参量、加工误差及光学性能指标来综合评估微光学元件性能的方法.