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911.
采用气相色谱-质谱(GC-MS)选择离子监测法(SIM),建立了准确可靠、灵敏度高、快速简便的测定维生素C泡腾片中甜蜜素含量的新方法.样品中的甜蜜素衍生后用有机试剂提取,在选择离子模式下进行测定,以保留时间和特征离子比例进行定性,单离子定量.甜蜜素的线性范围为0.05-10mg/L,检出限为0.6mg/kg,回收率为90.5%-96.9%,相对标准偏差小于4.4%.方法分析所用时间短,结果准确可靠,选择性好,适用于维生素C泡腾片中甜蜜素含量的检验. 相似文献
912.
S. Fumeron P. Ben-Abdallah 《Journal of Quantitative Spectroscopy & Radiative Transfer》2006,97(2):195-208
The aim of this paper is to present several features of the couplings occurring between radiative transfer and the kinetics of a moving dielectric. After determining how the velocity field affects the apparent thermo-optical properties of matter, the energy transport problem is investigated in instationary regime and the general form of transient radiative transfer equation inside a moving medium is built. Then, the model is applied to the particular case of turbulent flows: a system of two equations for mean and fluctuating radiative energies is presented, and the resolution of this system is finally carried out. 相似文献
913.
914.
In this paper we report some of the important results of experimental investigations of the flicker noise near the metal-insulator
(MI) transition in doped silicon single crystals. This is the first comprehensive work to study low-frequency noise in heavily
doped Si over an extensive temperature range (2 K<T<500 K). The measurements of conductance fluctuations (flicker noise) were carried out in the frequency range 10−2<f<4 × 101 Hz in single crystalline Si across the MI transition by doping with phosphorous and boron. The magnitude of noise in heavily
doped Si is much larger than that seen in lightly doped Si over the whole temperature range. The extensive temperature range
covered allowed us to detect two distinct noise mechanisms. At low temperatures (T<100 K) universal conductance fluctuations (UCF) dominate and the spectral dependence of the noise is determined by dephasing
the electron from defects with two-levels (TLS). At higher temperatures (T>200 K) the noise arises from activated defect dynamics. As the MI transition is approached, the 1/f spectral power, typical of the metallic regime, gets modified by the presence of discrete Lorentzians which arise from generation-recombination
process which is the characteristic of a semiconductor. 相似文献
915.
采用MOCVD技术在Al2O3(0001)衬底上生长了GaN薄膜,使用透射光谱、光致发光光谱和X射线双晶衍射三种技术测试了五类GaN薄膜样品,实验结果表明:GaN薄膜透射谱反映出的GaN质量与X射线双晶衍射测量的结果一致,即透射率越大,半高宽越小,结晶质量越好;而X射线双晶衍射峰半高宽最小的样品,其PL谱的带边峰却很弱,这说明PL谱反映样品的光学性能与X射线双晶衍射获得的结晶质量不存在简单的对应关系,同时还报导了一种特殊工艺生长的高阻GaN样品的RBS/沟道结果。 相似文献
916.
IntroductionThemethoxyradical (CH3O)isanimportantinter mediateinthephotochemicaloxidationofhydrocarbonsintheatmosphere ,1 3andplaysasignificantroleintrans formingnitricoxidetonitrogendioxide .4 Similarly ,thereactionmechanismsofhydroxylandcarbonmonoxide5,6ando… 相似文献
917.
L. Stoyanov 《Mathematische Annalen》2002,324(4):743-771
In this paper we consider properties of obstacles satisfying some non-degeneracy conditions that can be recovered from the
scattering length spectrum (SLS). Clearly the latter tells us whether the obstacle K is trapping or non-trapping. If the set of trapped points is relatively small, then the SLS also determines the volume of
the obstacle, the number of its connected components, and whether its boundary is convex everywhere or it has non-trivial
concavities. Under the additional assumption that the curvature of the obstacle does not vanish of infinite order, it is proved
that from the SLS one can recover certain information about the number of reflection points of any simply reflecting ray in
the exterior of the obstacle. Finally, for some special classes of obstacles (e.g. star-shaped ones), it is shown that the
SLS completely determines the obstacle.
Received: 2 March 1999 / Revised version: 16 January 2001 / Published online: 5 September 2002 相似文献
918.
Let (X,0) be the germ of a normal space of dimension n+1 and let f be the germ at 0 of a holomorphic function on X. Assume both X and f have an isolated singularity at 0. Denote by J the image of the restriction map , where F is the Milnor fibre of f at 0. We prove that the canonical Hermitian form on , given by poles of order at in the meromorphic extension of , passes to the quotient by J and is non-degenerate on . We show that any non-zero element in J produces a “mass concentration” at the singularity which is related to a simple pole concentrated at for (in a non-na?ve sense). We conclude with an application to the asymptotic expansion of oscillatory integrals , for , when .
Received: 28 May 2001 / Published online: 26 April 2002 相似文献
919.
In this paper we face the problem of stowing a containership, referred to as the Master Bay Plan Problem (MBPP); this problem
is difficult to solve due to its combinatorial nature and the constraints related to both the ship and the containers. We
present a decomposition approach that allows us to assign a priori the bays of a containership to the set of containers to
be loaded according to their final destination, such that different portions of the ship are independently considered for
the stowage. Then, we find the optimal solution of each subset of bays by using a 0/1 Linear Programming model. Finally, we
check the global ship stability of the overall stowage plan and look for its feasibility by using an exchange algorithm which
is based on local search techniques. The validation of the proposed approach is performed with some real life test cases.
This work has been developed within the research area: “The harbour as a logistic node” of the Italian Centre of Excellence
on Integrated Logistics (CIELI) of the University of Genoa, Italy 相似文献
920.
Fumiyasu Komaki 《Journal of multivariate analysis》2006,97(8):1815-1828
Simultaneous prediction and parameter inference for the independent Poisson observables model are considered. A class of proper prior distributions for Poisson means is introduced. Bayesian predictive densities and estimators based on priors in the introduced class dominate the Bayesian predictive density and estimator based on the Jeffreys prior under Kullback-Leibler loss. 相似文献