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91.
苏薇薇 《广东微量元素科学》1996,3(10):40-42
用等离子体原子发射光谱法测定了壮腰健肾丸中18种宏量及微量元素的含量,并对微量元素与壮腰健肾丸疗效之间的关系作了探讨。 相似文献
92.
微量元素与妊娠及围产医学的关系 总被引:1,自引:3,他引:1
郭晓莉 《广东微量元素科学》1995,2(11):59-61
为探讨微量元素与妊娠及围产医学的关系,取49例正常孕产妇和51例异常孕产妇的头发进行微量元素检测.结果表明,异常孕产妇中妊娠高血压综合征组发锌均值(104±17.54)×10-6明显低于正常组(168±22.12)×10-6,而发铜均值(13.3±0.78)×10-6明显高于正常组(11.3±0.94)×10-6,不明原因流产组发锌(115±10.32)×10-6,发铜(9.03±1.03)×10-6两项均值明显低于正常组,羊膜早破组仅发铜均值(7.59±1.97)×10-6低于正常组;畸胎组则锌、铜、铁、钙均值都低于正常组.经统计学处理均有显著性差异(P<0.05或产<0.01) 相似文献
93.
94.
乌江流域沉积岩风化过程中稀土元素的富集与释放 总被引:1,自引:0,他引:1
以乌江流域石灰岩、白云质灰岩、白云岩、硅质岩、页岩和砂岩等沉积岩的13条风化剖面为对象,运用R型分层聚类分析和质量平衡计算方法,研究了这些岩石风化过程中稀土元素(REE)的富集与释放及其对植物生长和河水REE分布的影响,目的是为河水物质来源研究和为农业生产提供依据。结果表明:(1)乌江流域石灰土中REE的富集程度显著高于各自母岩、黄壤、上陆壳(UCC)、中国土壤(CS)和世界土壤(WS);(2)沉积岩风化过程中REE的富集特征和机制可能与母岩中REE分布特征以及风化剖面中有机质、铁(氢)氧化物和粘土矿物的吸附有关;(3)沉积岩风化过程中释放的REE可为植物吸收利用;(4)石灰岩等沉积岩风化过程中REE和F。等元素的释放对河水溶解态REE的分布有重要影响。 相似文献
95.
用计算机多元分析研究冠心病微量元素谱,识别冠心病患者与健康者;非线性映射法判别率男性86.6%,女性96.2%;SIMCA差别法正确回判率男性85.0%,女性88.3%。 相似文献
96.
97.
Lim LW Hirose K Tatsumi S Uzu H Mizukami M Takeuchi T 《Journal of chromatography. A》2004,1033(2):205-212
An on-line sample enrichment system was designed using monolithic precolumns in microcolumn LC. The monolithic ODS capillary columns were prepared via in situ sol-gel processes. The enrichment efficiency of the monolithic columns was tested by using phthalates as the analytes. The relative standard deviations (n = 6) for the retention time, peak area and peak height were between 0.4 and 1.2%, 0.9 and 5.5% and 0.4 and 3.9%, respectively. The system was linear (R2 > 0.99) within the working sample concentration and sample volume ranges. Comparing to 0.2 microl injection with a typical sample injector, the theoretical plate number of a same separation column was increased by 3-6-fold when the precolumn unit was used for sample injection. The recoveries of the analytes were between 88 and 120%, and the sample volume that could be injected into the system was increased up to 5000-fold. The limits of detection were improved by more than 2000-fold and were between 0.21 and 0.87 ng ml(-1) even with a UV absorbance detector. This system was applied to the determination of phthalates contained in laboratory distilled water and tap water samples. 相似文献
99.
Stephen de Mora Jean-Pierre Villeneuve Eric Wyse 《Accreditation and quality assurance》2007,12(11):587-592
Aspects of the International Atomic Energy Agency (IAEA) Analytical Quality Control Services (AQCS) for marine environmental
studies are discussed, focusing on recent laboratory performance studies (LPS) and the production of reference materials for
trace metals and organic compounds in various marine matrices. The IAEA has organized seventeen global interlaboratory studies
for a range of organic contaminants. Of note has been the inclusion of numerous polychlorinated biphenyl congeners (PCBs)
and some sterols of anthropogenic origin. Concurrently, there have been eleven worldwide intercomparison exercises for trace
metals in the marine environment, most of which included methylmercury. Although such interlaboratory studies can help improve
performance in individual laboratories and regional laboratory networks, the results reveal that problems remain in the determination
of some metals and many organic contaminants. 相似文献
100.
A microwave-assisted digestion procedure using HNO3, HF, and H2O2 has been developed for analysis of elements in ambient particulate matter (PM). The samples are collected on cellulose filters and analyzed by inductively coupled plasma mass spectrometry (ICP-MS). The ICP-MS is calibrated with external standards, and recovery of analytes is tested with NIST SRM 1648 Urban Dust. This method has been used to quantify the airborne concentrations of a large number of elements, including Ag, As, Ba, Be, Ca, Cd, Ce, Co, Cr, Cs, Cu, Fe, Ga, K, Li, Mg, Mn, Mo, Ni, Pb, Rb, Se, Sb, Sr, Ti, Tl, V, and Zn. For the majority of these elements, recovery of the NIST SRM is within 15% of the certified values. 相似文献