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121.
Summary Furocoumarins from extracts ofHeracleum genus fruits were separated using normal and reversed phase TLC and HPLC and isolated in the milligram scale using overloaded
systems of column chromatography. Binary or ternary solvents containing a polar modifier (methanol, diisopropyl ether or acetonitrile)
were used as the mobile phases.
Preliminary report on this work was presented at the 47th International Congress of Pharmaceutical Sciences of F.I.P. in Amsterdam.
The Netherlands, 30 August–5 September 1987. 相似文献
122.
Wen-Rong Dai 《Journal of Differential Equations》2007,235(1):127-165
In this paper, we study the global existence and the asymptotic behavior of classical solution of the Cauchy problem for quasilinear hyperbolic system with constant multiple and linearly degenerate characteristic fields. We prove that the global C1 solution exists uniquely if the BV norm of the initial data is sufficiently small. Based on the existence result on the global classical solution, we show that, when the time t tends to the infinity, the solution approaches a combination of C1 traveling wave solutions. Finally, we give an application to the equation for time-like extremal surfaces in the Minkowski space-time R1+n. 相似文献
123.
124.
We give general conditions on a generator of a C0-semigroup (resp. of a C0-resolvent) on Lp(E,μ), p ≥ 1, where E is an arbitrary (Lusin) topological space and μ a σ-finite measure on its Borel σ-algebra, so that it generates a sufficiently
regular Markov process on E. We present a general method how these conditions can be checked in many situations. Applications to solve stochastic differential
equations on Hilbert space in the sense of a martingale problem are given.
Dedicated to Giuseppe Da Prato on the occasion of his 70th birthday 相似文献
125.
Piotr Niemiec 《Topology and its Applications》2006,153(18):3373-3382
Equicontinuous semigroups of transformations of a compact Hausdorff space and their sets of all invariant (Borel, regular and probabilistic) measures are studied. Conditions equivalent to the existence of at least one invariant measure are given. The (algebraic and topological) structure of the set of invariant measures is researched. 相似文献
126.
The problem of analytic representation of integrable CR functions on hypersurfaces with singularities is treated. The nature of singularities does not matter while the set of singularities
has surface measure zero. For simple singularities like cuspidal points, edges, corners, etc., also the behaviour of representing
analytic functions near singular points is studied.
Received: 8 December 2000; in final form: 24 June 2001/Published online: 1 February 2002 相似文献
127.
Two methods for sampling and concentration of volatile organic compounds are reported. In the first method, traps coated with a very thick film (ca. 100 μm) of cross-linked silicone stationary phase are employed. Such thick films can be prepared with a modified dynamic coating procedure, which is briefly described. The low phase ratio traps can be utilized for enrichment of volatiles from gaseous as well as aqueous matrices. The second technique is based on chromatographic evaporation of a solvent in a capillary tube, where the process is sustained by a repeated sample injection and a cyclic flow reversal. In this way, large solvent volumes can be handled by a small volume system. Under optimal conditions, when using a solvent barrier, quantitative recovery is possible even for compounds of comparatively high volatility. Another important application of the technique is extraction of trace components from gases such as headspace samples, polluted air, etc. 相似文献
128.
Global Existence and Exponential Stability of Smooth Solutions to a Full Hydrodynamic Model to Semiconductors 总被引:1,自引:0,他引:1
We study a full hydrodynamic semiconductor model in multi-space dimension. The global existence of smooth solutions is established
and the exponential stability of the solutions as is investigated.
Received November 14, 2000; in revised form March 25, 2002 Published online August 5, 2002 相似文献
129.
Technical cellulose-2.5-acetates (CA 2.5) were characterized regarding their carbohydrate composition in comparison to the raw material. The association of the CA 2.5 samples in acetone was studied by size exclusion chromatography (SEC) using various acetone grades and styrene divinylbenzene copolymer columns. In HPLC grade acetone with and without addition of 1% water up to three different pre-humps eluted in front of the main fraction of the polymer. The evaluation of the main peak by light scattering measurements resulted in high molar masses indicating that for these technical CA 2.5 samples even the main fraction is not dissolved without association. No pre-humps or association phenomena were observed after addition of 1 ppm LiBr to HPLC grade acetone or with p.a. grade acetone. In addition pre-hump enriched and pre-hump free fractions were isolated by fractionated precipitation. The carbohydrate composition of these fractions was determined and correlated with their association pattern in SEC investigations. 相似文献
130.
Cyrille Ospel 《Journal of Pure and Applied Algebra》2002,173(3):315-337
For a commutative algebra the shuffle product is a morphism of complexes. We generalize this result to the quantum shuffle product, associated to a class of non-commutative algebras (for example all the Hopf algebras). As a first application we show that the Hochschild-Serre identity is the dual statement of our result. In particular, we extend this identity to Hopf algebras. Secondly, we clarify the construction of a class of quasi-Hopf algebras. 相似文献