基于空穴注入层摩擦定向的偏振蓝光聚合物电致发光器件

研究了利用摩擦空穴注入层3,4-乙撑二氧噻吩:聚苯乙烯磺酸(PEDOT:PSS)作为定向层实现聚芴(PFO)薄膜的偏振电致发光,蓝光的色坐标为(0.20,0.21).从聚合物薄膜的紫外可见吸收和光致发光偏振特性,研究了不同定向层摩擦强度、退火温度以及退火时间下PFO薄膜的二向色性,并证明退火温度是决定器件偏振性能的关键因素.当摩擦强度为25 mm退火温度和时间分别为200℃和30 min时,得到较好的偏振性能,器件的电致发光偏振率约为3. 关键词： 偏振发光 摩擦定向 聚合物电致发光 空穴注入层     

EAST装置内置低温冷凝泵低温分配阀箱的研制

在全超导磁约束核聚变试验装置EAST中,为了防止杂质从偏虑器靶板附近进入等离子体核心,为EAST长脉冲放电试验提供持续的排灰能力以及装置长冲放电等,低温冷凝泵是必不可少的部件之一,在装置真空室上下安装了内置低温凝泵以提高装置运行参数,为满足低温泵的低温条件,增加一低温分配阀箱给内置低温冷凝泵提供低温条件。文中介绍应用于EAST装置系统中的内置低温冷凝泵分配阀箱研制的技术要求、冷却流程、结构特征。     

Magnetic alignment in nominally non-magnetic hexagonal metal hydrides: NMR

Powders of three hexagonal metal-hydrides or -deuterides are found to align in 4.4–8.3 T magnetic fields used for NMR. The field-alignment is unexpected, since all three systems have very small susceptibilities, as demonstrated by sharp NMR lines. The extent of alignment runs from nearly complete to barely detectable in ZrBe₂(H,D)_x, LuD₃, and YD₃, respectively. The preferred alignment direction in ZrBe₂(H,D)_x is with the crystallites’ c-axis perpendicular to B, while the c-axis and B tend to be parallel in LuD₃ and YD₃. The susceptibilities χ_|| and χ are determined from bulk magnetization measurements in aligned ZrBe₂H_1.4 powder. The alignment must be considered for proper analysis of NMR spectra in these and related materials.     

光学工程分析中的镜面面形处理新方法

光学系统在载荷的作用下会发生变形。基于干涉检验理论,提出了一种先调整后再拟合的处理方法。首先利用下山法计算光学镜面在法线方向的变形;然后利用Zernike多项式拟合变形曲面得到Zernike系数;最后去除刚体位移,作等高线图。新的数据处理方法可以更好的与干涉检验保持一致。对某相机的主镜进行仿真试验,结果表明,下山法计算效率较高,先调整后再拟合的处理结果与干涉检验结果的一致性较好。     

Effects of thermal annealing on structural and magnetic properties of thin Pt/Cr/Co multilayers

Thermal stability of thin Pt/Cr/Co multilayers and the subsequent changes in their structural, magnetic, and magneto-optical properties are reported. We observe CoCrPt ternary alloy phase formation due to annealing at temperatures about 773 K, which is accompanied by enhancement in the coercivity value. In addition, 360° domain wall superimposed on a monodomain like background has been observed in the pristine multilayer, which changes into a multidomain upon annealing at 873 K.     

The structural instabilities in ferronematic based on liquid crystal with negative diamagnetic susceptibility anisotropy

The studied ferronematic is a nematic liquid crystal (ZLI1695) of low negative anisotropy of the diamagnetic susceptibility (χ_a<0) doped with the magnetic particles Fe₃O₄. Structural instabilities are interpreted within Burylov and Raikher's theory. The high magnetic fields were oriented perpendicular (Freedericksz transition) or parallel to the initial director. Using capacitance measurements the Freedericksz threshold magnetic field of the ferronematic B_FN, and the critical magnetic field B_max, at which the initial parallel orientation between the director and the magnetic moment of magnetic particles breaks down, have been determined. The values of these quantities have been used to estimate the surface density of the anchoring energy W of liquid crystal molecules on the surface of the magnetic particles. The obtained values indicate a soft anchoring of the liquid crystal on the magnetic particles with a preferred parallel orientation of the magnetic moment of magnetic particles and the director.     

非稳腔中调腔孔对光束质量的影响

在中、远红外波段的激光器中，组成谐振腔的反射镜基底材料多数是对可见光不透明的，采用在腔镜上开一小孔输入调腔光方法是最简便的。本文用Ｆｏｘ－Ｌｉ迭代法计算了无开孔及有开孔时正支非稳共焦腔空腔的模式，结果表明当调腔光开孔直径小于３ｍｍ时，对光束质量基本没有影响。     

激光能量叠加过程中对准精度对焦斑的影响

利用多光束激光输出耦合叠加是一种提高激光器输出功率的有效方法。采用两束矩形激光对准系统,分析两光束不同对准情况下的焦斑特性。完全对准的情况下,两束光的远场焦斑重合在一起,焦斑能量是两光束能量之和。在实际光束对准系统中,讨论了三种常见的对准误差,并比较了这些误差对焦斑特性的影响。利用ZEMAX软件对设计系统进行了模拟分析,并进行了实验验证。结果表明,元件的位置误差会使远场焦斑能量集中度降低,焦斑半径增大。     

机械阻抗测量的一种新方法

本文介绍了一种新的机械阻抗测量方法－声强法，由定义出发将机械阻抗表为功率流和加速度响应谱的函数，应用结构声强技术测量功率流，声强法不需要测量作用力信号，可以用于测量任意结构中的各类机械阻抗，实验结果表明，声强获得的测量值与直接获得的测量值相近，声强法能较准确地测量一维和二维匀质结构中机械阻抗。     

Effect of ultrasound on the properties of rice bran protein and its chlorogenic acid complex

Ultrasound technology was used to treat rice bran protein (RBP), and the structural and functional properties of ultrasonically treated RBP (URBP) and its chlorogenic acid (CA) complex were studied. When ultrasonic power of 200 W was applied for 10 min, the maximum emission peak λ_max of the URBP-CA complex in the fluorescence spectrum was red-shifted by 3.6 nm compared to that of the untreated complex. The atomic force microscope (AFM) analysis indicated that the surface roughness of the complex was minimized (3.89 nm) at the ultrasonic power of 200 W and treatment time of 10 min. Under these conditions, the surface hydrophobicity (H₀) was 1730, the contents of the α-helix and β-sheet in the complex were 2.97% and 6.17% lower than those in the untreated sample, respectively, the particle size decreased from 106 nm to 18.2 nm, and the absolute value of the zeta-potential increased by 11.0 mV. Therefore, ultrasonic treatment and the addition of CA changed the structural and functional properties of RBP. Moreover, when ultrasonic power of 200 W was applied for 10 min, the solubility, emulsifying activity index (EAI), and emulsion stability index (ESI) were 68%, 126 m²/g, and 37 min, respectively.