On the monotonicity of the power functions of tests based on traces of multivariate beta matrices

It is shown that for the MANOVA problem the power function of the test based on the trace of a multivariate beta matrix is monotonically increasing in each noncentrality parameter provided that the cutoff point is not too large. This result is also true for the problem of testing independence of two sets of variates.     

Viscoelastic characterization of compacted pharmaceutical excipient materials by analysis of frequency-dependent mechanical relaxation processes

A newly developed method for determining the frequency-dependent complex Young's modulus was employed to analyze the mechanical response of compacted microcrystalline cellulose, sorbitol, ethyl cellulose and starch for frequencies up to 20 kHz. A Debye-like relaxation was observed in all the studied pharmaceutical excipient materials and a comparison with corresponding dielectric spectroscopy data was made. The location in frequency of the relaxation peak was shown to correlate to the measured tensile strength of the tablets, and the relaxation was interpreted as the vibrational response of the interparticle hydrogen and van der Waals bindings in the tablets. Further, the measured relaxation strength, holding information about the energy loss involved in the relaxation processes, showed that the weakest material in terms of tensile strength, starch, is the material among the four tested ones that is able to absorb the most energy within its structure when exposed to external perturbations inducing vibrations in the studied frequency range. The results indicate that mechanical relaxation analysis performed over relatively broad frequency ranges should be useful for predicting material properties of importance for the functionality of a material in applications such as, e.g., drug delivery, drug storage and handling, and also for clarifying the origin of hitherto unexplained molecular processes.     

A new technique for the identification of ultrasonic flaw signals using deconvolution

The identification of ultrasonic flaw signals is a difficult task in the angle beam ultrasonic testing of welded joints due to the presence of non-relevant signals from the geometric reflectors such as weld-roots and counter-bores. This paper describes a new approach to identify ultrasonic flaw signals in such a problematic situation. A similarity function is defined as the deconvolution of a target signal by a reference signal. The similarity functions for the same type of flaws/references are symmetric bandlimited impulse-like patterns with larger amplitudes while those for different types of flaws/references are asymmetrical broad patterns with relatively smaller amplitudes. Therefore, ultrasonic signals could be identified by the pattern of the similarity function. In the initial experiments, the proposed technique showed great potential for identifying ultrasonic flaw signals in the inspection of weld joints.     

CT重构中射线硬化的校正研究

在工业CT(ComputedTomography)重构中,由于射束硬化使得重建图像中出现"杯状"伪影。为了消除这种影响,提出了一种校正方法。该方法基于Beer理论,根据多色射束和数据,首先拟合出等效单色射束和数据,然后进行卷积反投影重构。这种方法不仅较好地消除了射线硬化的影响,同时也使重构图像的信息损失不大。     

Cholinesterase sensors based on screen-printed electrodes for detection of organophosphorus and carbamic pesticides

Cholinesterase sensors based on screen-printed electrodes modified with polyaniline, 7,7,8,8-tetracyanoquinodimethane (TCNQ), and Prussian blue have been developed and tested for detection of anticholinesterase pesticides in aqueous solution and in spiked grape juice. The influence of enzyme source and detection mode on biosensor performance was explored. It was shown that modification of the electrodes results in significant improvement of their analytical characteristics for pesticide determination. Thus, the slopes of the calibration curves obtained with modified electrodes were increased twofold and the detection limits of the pesticides were reduced by factors of 1.6 to 1.8 in comparison with the use of unmodified transducers. The biosensors developed make it possible to detect down to 2×10^–8 mol L^–1 chloropyrifos-methyl, 5×10^–8 mol L^–1 coumaphos, and 8×10^–9 mol L^–1 carbofuran in aqueous solution and grape juice. The optimal conditions for grape juice pretreatment were determined to diminish interference from the sample matrix.Abbreviations ChE Cholinesterase - TCNQ 7,7,8,8-Tetracyanoquinodimethane - ChO Choline oxidase - AChE Acetylcholinesterase - BChE Butyrylcholinesterase - BSA Bovine serum albumin - 2-PAM 2-Pyridine aldoxime methiodide     

Testing multivariate uniformity and its applications

Some new statistics are proposed to test the uniformity of random samples in the multidimensional unit cube These statistics are derived from number-theoretic or quasi-Monte Carlo methods for measuring the discrepancy of points in . Under the null hypothesis that the samples are independent and identically distributed with a uniform distribution in , we obtain some asymptotic properties of the new statistics. By Monte Carlo simulation, it is found that the finite-sample distributions of the new statistics are well approximated by the standard normal distribution, , or the chi-squared distribution, . A power study is performed, and possible applications of the new statistics to testing general multivariate goodness-of-fit problems are discussed.

     

Irreducibility testing over local fields

The purpose of this paper is to describe a method to determine whether a bivariate polynomial with rational coefficients is irreducible when regarded as an element in , the ring of polynomials with coefficients from the field of Laurent series in with rational coefficients. This is achieved by computing certain associated Puiseux expansions, and as a result, a polynomial-time complexity bound for the number of bit operations required to perform this irreducibility test is computed.

     

工业X射线机的射束均匀性检验

在与法国某公司的合作项目中,对射线机的性能做了充分的评估,针对工业X射线机射束均匀性的检验给出了实验内容、过程和结果分析。实验所用射线机分别为ISOVOLT320/13与XYD-225/10,两台设备的实验结果均符合该公司质控文件规定,满足黑度差不超过0.3的要求。定期对射线机进行射束均匀性检验,将有利于监测射线机的工作状态,以保证检测工作的准确性和一致性。     

Collimation testing using a circular Dammann grating

A novel technique for collimation testing with a circular Dammann grating is proposed. When the beam under test is incident on a one-order circular Dammann grating with limited aperture, double-humped radial rings will be generated at the back focal plane of a focusing lens. If the beam is collimated, the separation between the two rings will reach its minimal, otherwise the two rings will be apart from each other. Therefore, the degree of collimation of the tested beam can be estimated from the separation. The principle and experimental results of the method are presented. Owing to the simplicity and low cost of the method, it is a promising method for quickly checking the collimation of a laser beam.     

WDP-500C型平面光栅单色仪应用于实验教学的技术问题

针对WDP-500C型平面光栅单色仪未设有千位数字,致使其报警时不能正确处理的问题,提出了根据滑块的传动距离加长挡光板或将光电报警开关向短波段移动8.0 nm的解决方案,消除了由于单色仪设计问题而产生的故障.