全文获取类型
收费全文 | 3304篇 |
免费 | 41篇 |
国内免费 | 31篇 |
专业分类
化学 | 1784篇 |
晶体学 | 2篇 |
力学 | 71篇 |
综合类 | 35篇 |
数学 | 647篇 |
物理学 | 837篇 |
出版年
2024年 | 1篇 |
2023年 | 55篇 |
2022年 | 245篇 |
2021年 | 216篇 |
2020年 | 283篇 |
2019年 | 218篇 |
2018年 | 200篇 |
2017年 | 192篇 |
2016年 | 248篇 |
2015年 | 179篇 |
2014年 | 173篇 |
2013年 | 173篇 |
2012年 | 125篇 |
2011年 | 138篇 |
2010年 | 98篇 |
2009年 | 84篇 |
2008年 | 75篇 |
2007年 | 109篇 |
2006年 | 80篇 |
2005年 | 86篇 |
2004年 | 82篇 |
2003年 | 56篇 |
2002年 | 69篇 |
2001年 | 45篇 |
2000年 | 24篇 |
1999年 | 19篇 |
1998年 | 16篇 |
1997年 | 12篇 |
1996年 | 9篇 |
1995年 | 5篇 |
1994年 | 6篇 |
1993年 | 1篇 |
1991年 | 1篇 |
1989年 | 1篇 |
1988年 | 1篇 |
1986年 | 33篇 |
1985年 | 2篇 |
1981年 | 1篇 |
1979年 | 14篇 |
1977年 | 1篇 |
排序方式: 共有3376条查询结果,搜索用时 46 毫秒
51.
52.
用在线萃取-流动注射分光光度法(FISP)测定了作为杂质与2,5-二羟基苯磺酸钙共存的对苯二酚。专门设计并制作了与流动注射分光光度测定单元组合在一起的在线萃取流路,对苯二酚用乙醚萃取进入有机相并在此相中于其吸收峰297.5 nm波长处测定其吸光度,通过萃取基体成分,即2,5-二羟基苯磺酸钙的干扰,由于其在乙醚中不溶解而得以消除。对苯二酚的吸光度与其相应浓度在3.5×10-6~5.0×10-4mol.L-1之间呈线性关系,相关系数达0.999 4。该方法的检出限为2.53×10-6mol.L-1。应用此方法分析了来自不同批次的3个试样,所得结果的RSD在0.69%~1.65%之间,且其值与药典法所测得结果相符。 相似文献
53.
L.A. Rodríguez-Guadarrama 《European Polymer Journal》2007,43(3):928-937
Online Fourier-transform near infrared (FT-NIR) spectroscopy in combination with a fiber optic probe was utilized to study the kinetics of the anionic polymerization of butadiene. The conversion of the butadiene to methylene protons in the polymer was monitored in solution polymerization conditions by monitoring the absorbance at 1632 nm. The off-line gel permeation chromatography, GPC, technique was used to validate the online FT-NIR spectroscopy method. Butadiene polymerization kinetics in cyclohexane initiated with n-butyllithium at different initiator concentrations and temperatures was studied. A phenomenological kinetic expression for the anionic polymerization of butadiene in cyclohexane initiated with n-butyllithium was determined. The predictions of the kinetic expression were in agreement with kinetic data reported in the literature. 相似文献
54.
以常见的阴、阳离子的检验为例,研究了如何实施基于标准的教学。校本教材的开发为标准、教材、教学、评价的一致性提供保障;以学生应知的和能做的驱动课堂活动;根据达成标准应有怎样的质量表现,试卷编制先于教学设计。课堂上,“教”“学”双方都明确学习目标,教师提供多种策略来满足学生多样的学习需要,如提供工具,搭建脚手架,并以“微”研究性学习的方式展开教学,给学生提供了充分的进步空间。 相似文献
55.
《Operations Research Letters》2022,50(4):399-406
We consider the problem faced by an online service platform that matches suppliers with consumers. Unlike traditional matching models, which treat them as passive participants, we allow both sides of the market to exercise their choices. To model this setting, we introduce a two-sided assortment optimization model wherein each participant's choice is modeled using a multinomial logit choice function, and the platform's objective is to maximize its expected revenue. We first show that the problem is NP-hard even when the number of suppliers is limited to two and provide a mixed-integer linear programming formulation. Next, we discuss two simple greedy heuristics and argue that these can lead to arbitrarily bad solutions. We then develop relaxations that provide upper and lower bounds and investigate the tightness of these relaxations by obtaining parametric approximation guarantees. Finally, we present numerical results on synthetic data demonstrating the practical utility of these relaxations. 相似文献
56.
化学教学内容情感性艺术处理的策略 总被引:1,自引:0,他引:1
化学教学内容是教学系统的基本要素之一。对教学内容作情感性艺术处理,显示了教师高超的化学教学艺术。其艺术策略分为:一是巧妙组织教学内容来调节学生的学习心向,包括心理匹配策略、超出预期策略;二是有效地利用教学内容中的情感资源来陶冶学生的情操,包括展示情感策略、发掘情感策略、诱发情感策略、赋予情感策略。 相似文献
57.
A review is given on the history of the development of analytical chemistry in Romania, its present role in University teaching, and on measures that are planned in order to improve teaching and education.Received January 12, 2003; accepted March 7, 2003
Published online July 16, 2003 相似文献
58.
High-quality online course materials were reconstructed through feedback from undergraduate students and online data analysis regarding constructed learning materials on the Chao Xing Learning Platform. They were used for studying organic chemistry courses online and offline in university for nationalities. This model, based on student-centered teaching, can effectively transform students from passively accepting knowledge to actively learning and internalizing knowledge. This strategy can also enhance the students' learning initiative and the effects of learning, and hopefully be helpful to the universities in multi-ethnic areas in developing fundamental disciplined construction of organic chemistry and other courses. 相似文献
59.
为了应对新冠病毒肺炎(COVID-19)蔓延和响应教育部"停课不停教,停课不停学"的号召,作者从"两问题三误区"入手分析了现有在线教学存在的问题,并对比了不同直播平台的优缺点,提出了在线教学的具体教学建议。以基于"超星直播+学习通"的在线教学为例进行了教学示范指导。 相似文献
60.
Based on the analysis of the courses and the investigation of students' online learning needs, an online teaching mode of "Tencent Classroom" and "Rain Classroom" with "split screen" is designed. This mode is used for the online teaching of "Foundation of Innovation and Entrepreneurship" and "Chemical Instrumentation and Automation". After two months of teaching practice, the teaching and learning were reflected and summarized, aiming to improve the performance of online teaching. 相似文献