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51.
Marcos Almeida Bezerra Sérgio Mitihiro do Nascimento Maêda Eliane Padua Oliveira Maria de Fátima Batista de Carvalho Ricardo Erthal Santelli 《Spectrochimica Acta Part B: Atomic Spectroscopy》2007
In the present paper a procedure is proposed for the determination of traces of Cd, Co, Mn and Cr in petroleum industry produced water by inductively coupled plasma optical emission spectrometry. The procedure is based on cloud point extraction of these metals, as their dithizonate complexes, into the surfactant-rich phase of octylphenoxypolyethoxyethanol surfactant (Triton X-114). Extractions were carried out in solutions with salinities between 10‰ and 70‰. Since residual salinity in the surfactant-rich phase caused differences in its transport to the plasma, yttrium was used as an internal standard to correct for this effect. The simultaneous metal extraction procedure was optimized by response surface methodology using a Doehlert design and desirability function. Enhancement factors of 21, 21, 9 and 19, along with limits of quantification of 0.093, 0.20, 0.73 and 1.2 μg L− 1, and precision expressed as relative standard deviation (n = 8, 20.0 μg L− 1) of 5.8, 1.2, 1.7 and 5.7% were obtained for Cd, Co, Mn and Cr, respectively. The accuracy was evaluated by spike recovery tests on the high salinity water samples with salinity of 40 and 63‰. 相似文献
52.
53.
Marie-Laurence Mazure 《Advances in Computational Mathematics》2007,26(1-3):305-322
In order to ensure existence of a de Boor algorithm (hence of a B-spline basis) in a given spline space with (n+1)-dimensional sections, it is important to be able to generate each spline by restriction to the diagonal of a symmetric function of n variables supposed to be pseudoaffine w.r. to each variable. We proved that a way to obtain these three properties (symmetry, n-pseudoaffinity, diagonal property) is to suppose the existence of blossoms on the set of admissible n-tuples, given that blossoms are defined in a geometric way by means of intersections of osculating flats. In the present paper, we examine the converse: do symmetry, n-pseudoaffinity, and diagonal property imply existence of blossoms? 相似文献
54.
J. Teixeira 《Il Nuovo Cimento D》1994,16(9):1433-1437
Summary The dynamics of water molecules occupying very small volumes can be probed by incoherent quasi-elastic neutron scattering.
We summarise some results obtained with wet samples of porous silica and hydrated proteins. The movements of the molecules
in the vicinity of the substrate are extremely reduced as compared to those of bulk water at the same temperature. Almost
only rotational movements subsist and the local diffusion is of the order of that observed in deeply supercooled water.
Paper presented at the I International Conference on Scaling Concepts and Complex Fluids, Copanello, Italy, July 4–8, 1994. 相似文献
55.
Andrea Vietri 《Graphs and Combinatorics》2007,23(1):111-121
We analyse 3-subset difference families of Z2d+1⊕Z2d+1 arising as reductions (mod 2d+1) of particular families of 3-subsets of Z⊕Z. The latter structures, namely perfect d-families, can be viewed as 2-dimensional analogues of difference triangle sets having the least scope. Indeed, every perfect d-family is a set of base blocks which, under the natural action of the translation group Z⊕Z, cover all edges {(x,y),(x′,y′)} such that |x−x′|, |y−y′|≤d. In particular, such a family realises a translation invariant (G,K3)-design, where V(G)=Z⊕Z and the edges satisfy the above constraint. For that reason, we regard perfect families as part of the hereby defined translation designs, which comprise and slightly generalise many structures already existing in the literature. The geometric context allows
some suggestive additional definitions. The main result of the paper is the construction of two infinite classes of d-families. Furthermore, we provide two sporadic examples and show that a d-family may exist only if d≡0,3,8,11 (mod 12). 相似文献
56.
A scheme for vehicle density and velocity estimation in a stretch of highway based on a modified cell transmission model [C.
F. Daganzo, Transportation Research, Part B, 28B(4),269–287, 1994. Elsevier is presented. The scheme is intended for use with on-ramp metering control algorithms, providing
local knowledge of densities and velocities that is helpful to improve on-ramp metering control performance. Estimation of
density is obtained by nonlinear estimators, while velocity estimation is obtained by gradient algorithms. There is one density–velocity
estimator for free traffic flow and other for congested traffic flow. Both estimator schemes work in parallel. The final estimation
of density and velocity results from a convex combination of the predictions of the two estimators. This combination depends
on occupancy or density measurements at the boundaries of the stretch and is produced by a fuzzy inference system. Stability
and convergence of the density and velocity estimation scheme is proved by Lyapunov based techniques. Simulation results comparing
measured and estimated traffic data are presented. They confirm good performance of the estimators.
Research sponsored by grants UNAM PAPIIT IN110403 and CONACYT 47583. 相似文献
57.
We examine the problem of building or fortifying a network to defend against enemy attacks in various scenarios. In particular,
we examine the case in which an enemy can destroy any portion of any arc that a designer constructs on the network, subject
to some interdiction budget. This problem takes the form of a three-level, two-player game, in which the designer acts first
to construct a network and transmit an initial set of flows through the network. The enemy acts next to destroy a set of constructed
arcs in the designer’s network, and the designer acts last to transmit a final set of flows in the network. Most studies of
this nature assume that the enemy will act optimally; however, in real-world scenarios one cannot necessarily assume rationality
on the part of the enemy. Hence, we prescribe optimal network design algorithms for three different profiles of enemy action:
an enemy destroying arcs based on capacities, based on initial flows, or acting optimally to minimize our maximum profits
obtained from transmitting flows. 相似文献
58.
物理实验课程考核、评估体系初探 总被引:4,自引:0,他引:4
对物理实验课程考核、评估方法进行了探讨,提出了物理实验课程考核、评估体系及实施细则.重点介绍了体系中的核心部分——正规的物理实验课程考试. 相似文献
59.
60.
小长径比垂直管气液两相流动特性分析 总被引:1,自引:0,他引:1
实验观察了小长径比垂直上流管内流型及特点,并对管入口处的压力波动特性和系统的压差波动特性进行了试验研究.结果表明:小长径比(L/D)垂直管内流型表现为泡状流、塞状流、乳沫状流、环状流和液束环状流;分别增加管线中的气量、液量,或者同时增加气液流量,均会造成垂直管入口处压力波动的均值和最大压力的增加;压力信号的概率密度(PDF)大部分呈双峰分布,也存在单峰和多峰分布;差压信号的概率密度符合正态分布,其功率谱密度同压力信号相比具有频率波动范围宽、幅值小的特点. 相似文献