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81.
微波消解-原子吸收法测定氧化铝为载体的钯催化剂中钯 总被引:2,自引:0,他引:2
报道了微波消解-AAS法测定氧化铝为载体的钯催化剂中钯的新方法,试验了微波消解溶样条件(溶解试剂、压力、时间和功率等),研究了测定介质的影响,通过在样品测定液中加入铝基体至铝浓度为4 mg/mL,消除了铝对钯测定的干扰.该法测定结果与光度法的结果一致,相对标准偏差小于1.5%(n=5). 相似文献
82.
Vsevolod K. Malinovskii 《Acta Appl Math》1994,34(1-2):261-281
Edgeworth expansions for the distribution of a sequential least squares estimator in the random coefficient autoregressive (RCA) model are derived. The regenerative approach to second-order asymptotic analysis of Markov-type statistical models is developed. 相似文献
83.
Multiderivations of Coxeter arrangements 总被引:3,自引:0,他引:3
Hiroaki Terao 《Inventiones Mathematicae》2002,148(3):659-674
Let V be an ℓ-dimensional Euclidean space. Let G⊂O(V) be a finite irreducible orthogonal reflection group. Let ? be the corresponding Coxeter arrangement. Let S be the algebra of polynomial functions on V. For H∈? choose α
H
∈V
* such that H=ker(α
H
). For each nonnegative integer m, define the derivation module D
(m)
(?)={θ∈Der
S
|θ(α
H
)∈Sα
m
H
}. The module is known to be a free S-module of rank ℓ by K. Saito (1975) for m=1 and L. Solomon-H. Terao (1998) for m=2. The main result of this paper is that this is the case for all m. Moreover we explicitly construct a basis for D
(m)
(?). Their degrees are all equal to mh/2 (when m is even) or are equal to ((m−1)h/2)+m
i
(1≤i≤ℓ) (when m is odd). Here m
1≤···≤m
ℓ are the exponents of G and h=m
ℓ+1 is the Coxeter number. The construction heavily uses the primitive derivation D which plays a central role in the theory of flat generators by K. Saito (or equivalently the Frobenius manifold structure
for the orbit space of G). Some new results concerning the primitive derivation D are obtained in the course of proof of the main result.
Oblatum 27-XI-2001 & 4-XII-2001?Published online: 18 February 2002 相似文献
84.
François Métayer 《Archive for Mathematical Logic》1994,33(3):169-188
This work defines homology groups for proof-structures in multiplicative linear logic (see [Gir1], [Gir2], [Dan]). We will show that these groups characterize proof-nets among arbitrary proof-structures, thus obtaining a new correctness criterion and of course a new polynomial algorithm for testing correctness. This homology also bears information on sequentialization. An unexpected geometrical interpretation of the linear connectives is given in the last section. This paper exclusively focuses onabstract proof-structures, i.e. paired-graphs. The relation with actual proofs is investigated in [Gir1], [Gir2], [Dan], [Ret] and [Tro]. 相似文献
85.
多目标分数变分问题的对偶性 总被引:1,自引:0,他引:1
本文利用参数逼近在函数广义(F,ρ)-凸的条件下,建立了一类多目标式变分问题关于有效解的对偶理论。 相似文献
86.
Denis V. Osin 《Archiv der Mathematik》2007,88(5):403-412
The aim of this paper is to show that free Burnside groups of sufficiently large odd exponent are non-amenable in a certain
strong sense. More precisely their left regular representations are isolated from the trivial representation uniformly on
finite generating sets. It follows that free Burnside groups are of uniform exponential growth. This answers a question of
de la Harpe.
This work has been partially supported by the NSF grant DMS-0605093 and by the RFBR Grant # 05-01-00892.
Received: 25 April 2006 相似文献
87.
W.T. Ingram 《Topology and its Applications》2006,153(10):1530-1539
88.
Michael J. Puls 《Archiv der Mathematik》2007,88(6):500-506
Let p be a real number greater than one. In this paper we study the vanishing and nonvanishing of the first L
p
-cohomology space of some groups that have one end. We also make a connection between the first L
p
-cohomolgy space and the Floyd boundary of the Cayley graph of a group. We apply the result about Floyd boundaries to show
that there exists a real number p such that the first L
p
-cohomology space of a nonelementary hyperbolic group does not vanish.
Received: 4 August 2006 Revised: 2 November 2006 相似文献
89.
Yuval Z. Flicker 《Mathematische Annalen》1993,297(1):199-219
90.
R. Souzy B. Ameduri B. Boutevin 《Journal of polymer science. Part A, Polymer chemistry》2004,42(20):5077-5097
The radical co‐ and terpolymerization of 4‐[(α,β,β‐trifluorovinyl)oxy]bromo benzene (TFVOBB) with 1,1‐difluoroethylene (or vinylidene fluoride, VDF, or VF2), hexafluoropropene (HFP), perfluoromethyl vinyl ether (PMVE), and chlorotrifluroroethylene (CTFE) is presented. Although TFVOBB could be thermocyclodimerized, it could not homopolymerize under radical initiation. TFVOBB could be copolymerized in solution under a radical initiator with VDF or CTFE comonomers, while its copolymerization with HFP or PMVE were unsuccessful. The terpolymerization of TFVOBB with VDF and HFP, or VDF and PMVE, or VDF and CTFE also led to original fluorinated terpolymers bearing bromoaromatic side‐groups. The conditions of co‐ and terpolymerization were optimized in terms of the nature of the radical initiators, and of the nature of solvents (fluorinated or nonhalogenated). Various monomer concentrations in the co‐ and terpolymers were assessed by 19F and 1H‐NMR spectroscopy. The thermal and physico chemical properties were also studied. © 2004 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 42: 5077–5097, 2004 相似文献