6─或8─脂代─7─氧香豆素与二氢呋喃香豆素的NMR，MS研究

对从重齿毛当归（ＡｎｇｅｌｉｃａｐｕｂｅｓｃｅｎｓＭａｘｉｍｆ．ｂｉｓｅｒｒａｔａＳｈａｎｅｔＹｕａｎ）根及根茎中分得的１２种６－或８－脂代－７－氧－香豆素和８种二氢呋喃香豆素衍生物进行了１Ｈ和１３ＣＮＭＲ分析研究．结合文献．做出规律性总结．运用２ＤＮＭＲ技术．对文献中当归醇类化合物碳谱中的个别错误归属给予了纠正，并首次探讨了此类化合物的ＭＳ裂解途径．     

A Pre－lasing Reliable Dynamic Filter Single－longitudinal－mode Q－switched Laser

ＡＰｒｅ－ｌａｓｉｎｇＲｅｌｉａｂｌｅＤｙｎａｍｉｃＦｉｌｔｅｒＳｉｎｇｌｅ－ｌｏｎｇｉｔｕｄｉｎａｌ－ｍｏｄｅＱ－ｓｗｉｔｃｈｅｄＬａｓｅｒＣＨＥＮＣｈａｎｇｍｉｎ（ＤｅｃａｎｔｍｅｎｔｏｆＥｌｅｃｔｒｏｎｉｃａｎｄＩｎｆｏｒｍａｔｉｏｎＴｅｃｈｎ...     

Phase retrieval from spectral interferograms including a stationary-phase point

We report on a simple processing procedure to retrieve the phase from spectral interferograms including a stationary-phase point. First, the numerical simulations are performed to demonstrate high precision of the phase retrieval from the spectral interferogram. Second, the feasibility of the procedure is confirmed in processing the experimental data from a dispersive Michelson interferometer comprising a cube beam splitter and a plate made of BK7 optical glass. From the retrieved spectral phase, the effective thickness of the BK7 optical glass is determined precisely.     

STABILITY ANALYSIS OF NONLINEAR GALERKIN ＆ GALERKIN METHODS FOR NONLINEAR EVOLUTION EQUATIONS

Abstract. Ogr object in this artlcle is to describe tbe Galerkln scheme and nonlin-eax Galerkin scheme for the approximation of nonlinear evolution equations, and tostudy the stability of these schemes. Spatial discretizatlon can be pedormed by eitherGalerkln spectral method or nonlinear Galerldn spectral method; time discretizatlort isdone hy Euler sin.heine wklch is explicit or implicit in the nonlinear terms. According tothe stability analysis of the above schemes, the stability of nonllneex Galerkln methodis better than that of Galexkln method.     

Splitting and pinching for convex sets

We consider noncompact, closed and convex sets with nonvoid interior in Euclidean space. It is shown that if such a set has one curvature measure sufficiently close to the boundary measure, then it is congruent to a product of a vector space and a compact convex body. Related stability and characterization theorems for orthogonal disc cylinders are proved. Our arguments are based on the Steiner-Schwarz symmetrization processes and generalized Minkowski integral formulas.     

Subgraphs of hypercubes and subdiagrams of boolean lattices

In this paper we extensively treat the following problems: When is a given graph a subgraph (resp. induced subgraph) of a hypercube and when is an ordered set a subdiagram (resp. induced subdiagram) of a Boolean lattice? We present characterizations for that in terms of suitable edge-colorings of the graphs and, for ordered sets, of their covering graphs.     

Finding the αn-th largest element

We describe an algorithm for selecting the n-th largest element (where 0<<1), from a totally ordered set ofn elements, using at most (1+(1+o(1))H())·n comparisons whereH() is the binary entropy function and theo(1) stands for a function that tends to 0 as tends to 0. For small values of this is almost the best possible as there is a lower bound of about (1+H())·n comparisons. The algorithm obtained beats the global 3n upper bound of Schönhage, Paterson and Pippenger for <1/3.     

Topological hochschild homology of extensions of ?/p? by polynomials, and of ?[x]/(xn) and ?[x]/(xn?1)

Topological Hochschild homology is calculated for the rings /p[x]/(f(x)) (where p is prime and f(x) /p[x] any polynomial), [x]/(x ⁿ) and [x]/(x ⁿ–1). A spectral sequence argument is used for calculating the homology of the topological Hochschild homology spectrum, from which its stable homotopy structure can be read off since the spectrum is known for a priori reasons to be a restricted product of Eilenberg-MacLane spectra.     

二溴羟基苯基荧光酮荧光熄灭法测定铜

研究了在pH 6 2～ 8 2磷酸二氢钾 磷酸氢二钠缓冲体系中 ,非离子表面活性剂TritonX 10 0存在下 ,铜 (Ⅱ )与二溴羟基苯基荧光酮 (DBH PF)形成 1∶2红色三元混配合物而使荧光熄灭 ,建立了荧光熄灭法测定铜的新方法。配合物的λex=5 3 0nm ,λem=5 60nm ,含量在 0～ 80 μg·L-1范围内有良好的线性关系 ,检测限为 0 2 μg·L-1。体系的灵敏度高 ,选择性好。Al(Ⅲ )、Fe(Ⅲ )、Ti(Ⅳ )的干扰 ,可用氟化钠、苦杏仁酸掩蔽。方法快速简便 ,用于人发、茶叶及水中微量铜的测定与AAS相符 ,RSD(n=5 ) <6 9% ,回收率在 98%～ 10 4 %之间。     

1GHz声表面横波谐振器的研究及应用

本文介绍声表面横波谐振器的设计及制作,并报导了我们研制的频率为１．１ＧＨｚ,插损３ｄＢ,有载Ｑ值大于２０００的声表面横波谐振器及其应用。