Field-induced functions of porous Si as a confined system

Electroluminescent porous Si (PS) diodes exhibit various useful functions under a high-electric field. The experimental PS diodes are composed of thin semitransparent metal films, PS layers (about 500 nm thick in minimum), p- or n-type Si substrates and ohmic back contacts. Definite nonlinear electrical behavior (negative resistance and nonvolatile bistable memory effects) and cold electron emission phenomena appear in these PS diodes associated with the EL emission. Both the negative resistance and memory effects are related to the charging of Si nanocrystallites by field-induced carrier injection. The electron emission observed in the PS diodes formed on n+–Si substrates is caused by hot electrons tunnelling through the top contact. By an appropriate structural control of PS, the effective drift length under a high-field conduction is significantly increased, and then electrons are emitted ballistically. These functions reflect the activity of PS as a nanocrystalline confined system.     

非晶合金条带的爆炸焊接

 报道了利用爆炸焊接技术对铁基、铁镍基非晶合金条带（厚度约25 μm）进行单层和多层爆炸焊接的结果。金相分析结果表明，条带间相互结合良好；X光衍射结果说明，焊接后的条带仍保持非晶态，即使采用表面已有部分晶化德条带进行焊接，焊接后仍转化为非晶态。这说明在焊接过程中条带表面已发生熔化，且冷却速度也可达10⁶ K/s量级。     

Calorimetric and nuclear byproduct measurements in electrochemical confinement of deuterium in palladium

We present the results of a new experiment with our multicell set-up implemented with mass spectrometric measurements of⁴He and a highly improved neutron detector. The excess heat measured is comparable with the results of other laboratories, but no neutrons were found and the tritium excess was lower than expected from the power excess. ⁴He has been measured in the electrolysis gases and a tentative correlation of ⁴He with excess power is presented and discussed.     

紫花地丁中汞的原子荧光法测定

利用还原气化的非色散型装置，以湿法消解的方式，建立了原子荧光测定紫花地丁中痕量汞的测定方法，同时比较了不同玻璃仪器的洗涤方法和不同的定量方法，试验回收率在86．9％－110．8％之间，误差＜8．5％，通过对实际样品的测定，得到了满意的结果。     

Analysis of volatile organic compounds in polymers by dynamic headspace and gas chromatography/mass spectrometry

An experimental method for the analysis of volatile organic compounds in polymers is described. The technique involves dynamic headspace sampling, collection, and concentration of the volatiles in a cold trap, followed by capillary column gas chromatography/mass spectometry. Flow switching is carried out by the Deans switching technique. Four technical polymers used as pharmaceutical packaging materials have been analyzed in order to demonstrate the method.     

The Loewner differential equation and slit mappings

We show that the Loewner equation generates slits if the driving term is Hölder continuous with exponent 1/2 and small norm and that this is best possible.

     

Cold trap/reinjection interface for two-dimensional gas chromatography

The construction and evaluation of an interface for two-dimensional gas chromatography is described. The interface consists of commercially available components and is attachable to available gas chromatographs without any major modifications. The interface has been constructed so as to permit “heartcutting” as well as solute band concentration. Trapping is performed in a simple cold trap of fused silica. Flow switching is accomplished by Deans switching. Factors of the over-all chromatographic performance are examined.     

Optical Measuring Method for Quality Monitoring Purpose in Laser Welding of Tin－plates

ＯｐｔｉｃａｌＭｅａｓｕｒｉｎｇＭｅｔｈｏｄｆｏｒＱｕａｌｉｔｙＭｏｎｉｔｏｒｉｎｇＰｕｒｐｏｓｅｉｎＬａｓｅｒＷｅｌｄｉｎｇｏｆＴｉｎ－ｐｌａｔｅｓ￥ＬＵＯＨｏｎｇ；ＨＵＬｕｎｊｉ；ＨＵＡＮＧＳｈｕｈｕａｉ；ＬＩＺｈｉｙｕａｎ；ＨＵＸｉｙｕａｎ（Ｈ...     

简易毛细管气相色谱冷柱头进样法

介绍了一种在无冷柱头进样器和特殊注射器情况下简便可行的冷柱头进样技术。以海洛因、秋水仙碱、正三十烷醇为研究对象，考察了本方法的定性、定量偏差，提出两种溶质聚焦方法。