氢化－原子吸收法测定钢铁中砷量

本文应用连续蒸汽产生系统的氢化－原子吸收法，以王水溶解试样，加硫酸驱除过量硝酸。采用邻菲啉有效地掩蔽干扰元素，在适当的盐酸酸度和硼氢化钾浓度下，测定钢铁中砷量。采用本法准确度与精确度均能获满意结果，方法简便、快速。     

One-dimensional perturbations of the shift

The structure of isometries on a Hilbert space are well studied. In this paper we study contractions which are one-dimensional perturbations of isometries, in particular, perturbations of the shift operator onH ².     

Excitation of analytes and enhancement of emission intensities in a d.c. plasma jet: a critical review leading to proposed mechanistic models

Experimental data and theoretical criteria are used to critically review existing models for analyte emission enhancement in the 3-electrode d.c. plasma (DCP). The analytical zone is characterized as a non-optically thin recombining plasma in partial thermodynamic equilibrium (PTE). Spectrochemical excitation the authors ascribe largely to: (1) argon resonance line radiative transport; (2) inversion of optically pumped argon states; (3) inversion of analyte populations by Franck-Condon collisions with argon; (4) energy cascading in analytes via a multitude of channels. Adding an easily ionized element (EIE): (1) induces additional resonance line radiative transfer; (2) raises electron densities in cooler, analyte-rich plasma margins; (3) locally increases argon optical absorption cross sections via Stark broadening; (4) redistributes ohmic heating. Coupling between the proposed mechanisms is non-linear. Relationships between radiative transfer and collisional redistribution and (1) background suppression by EIE and (2) analyte emission enhancement by helium are also examined. Similarities between DCP and inductively coupled plasma (ICP) excitation mechanisms are noted and practical implications are addressed.     

Multiple points of trajectories of multiparameter fractional Brownian motion

Consider 0<α<1 and the Gaussian process Y(t) on ℝ ^N with covariance E(Y(s)Y(t))=|t|^2α+|s|^2α−|t−s|^2α, where |t| is the Euclidean norm of t. Consider independent copies X ¹,…,X ^d of Y and␣the process X(t)=(X ¹(t),…,X ^d (t)) valued in ℝ ^d . When kN≤␣(k−1)αd, we show that the trajectories of X do not have k-multiple points. If N<αd and kN>(k−1)αd, the set of k-multiple points of the trajectories X is a countable union of sets of finite Hausdorff measure associated with the function ϕ(ɛ)=ɛ ^{k N /α−( k −1) d} (loglog(1/ɛ)) ^k . If N=αd, we show that the set of k-multiple points of the trajectories of X is a countable union of sets of finite Hausdorff measure associated with the function ϕ(ɛ)=ɛ ^d (log(1/ɛ) logloglog 1/ɛ) ^k . (This includes the case k=1.) Received: 20 May 1997 / Revised version: 15 May 1998     

What must and what need not be contained in a graph of uncountable chromatic number?

We investigate the following problem: What countable graphs must a graph of uncountable chromatic number contain? We define two graphsΓ andΔ which are very similar and we show thatΓ is contained in every graph of uncountable chromatic number, whileΔ is (consistently) not.     

Proper fibrations with Hilbert cube manifold fibers

The main result of this paper asserts that any proper fibration over a finite-dimensional ANR with Hilbert cube manifold fibers is a locally trivial bundle.     

Free products of kω-topological groups with normal amalgamation

It is shown in this paper that if A is a closed normal subgroup of k_ω-topological groups G and H, then the free product of G and H with A amalgamated, G1_AH, exists, is Hausdorff and indeed a k_ω-group.     

Countably compact extensions of topological spaces

We study the question whether a topological space X with a property $\text{P}$ can be embedded in a countably compact space X? with the same property $\text{P}$.