超高效液相色谱-串联质谱法同时测定水产调味品中的罗丹明B、结晶紫和孔雀石绿

1引言罗丹明B常被违法用于调味品的染色,孔雀石绿和结晶紫因具有消毒和杀菌作用而常被违法应用于水产品养殖中。三者结构类似,都具有高毒、高残留和致癌、致畸、致突变等特点,色谱分离较难,且由于食品基质复杂,对质谱检测影响较大。目前,单独检测3种物质的方法分别有高效液相色谱法[1]、气相色谱-质谱法[2]、液相色谱-质谱法[3]和液相色谱-     

一个(3+1)维非线性方程的B(a)cklund变换和精确解

利用双Bell多项式方法构造了一个(3+1)维非线性方程的双线性形式,得到了该方程的双线性Bcklund变换和相应的Lax对.同时利用Riemann theta函数,获得了该方程的周期波解.     

4×4B-型KdV方程族

基于sl(4,(C))的loop代数的非平凡李代数分裂,构造了5类新的孤子方程族.这些代数分裂通过构造从正李子代数到负李子代数的线性箅子B统一得到.对所有可能的线性箅子B进行分类,证明存在5类4×4仿射B-型KdV方程族.利用Adler- Konstant- Symes理论获得了这些方程族的Hamilton结构,并利用loop群方法得到其B(a)cklund变换.     

Bcklund Transformation and Conservation Laws for the Variable-coefficient N-Coupled Nonlinear Schrdinger Equations with Symbolic Computation

Considering the integrable properties for the coupled equations, the variable-coefficient N-coupled nonlinear Schrdinger equations are under investigation analytically in this paper. Based on the Lax pair with the nonisospectral parameter, a Bcklund transformation for such a coupled system denoting in the Γ functions is constructed with the one-solitonic solution given as the application sample. Furthermore, an infinite number of conservation laws are obtained using symbolic computation.     

反相液相色谱中动力学因素对肽谱影响规律研究

研究了用反相色谱模式, 在不同流动相流速条件下所得到的细胞色素C的肽谱图. 发现在低流速时, 保留弱的肽谱峰增多, 而在高流速时保留强的肽谱峰增多, 未发现溶质分子质量与溶质相对保留值(RRT)之间存在有特定的变化关系. 然而却发现了两种变化规律, 即溶质相对保留值(RRT)与流动相流速之间的双对数线性关系(1) log RRT＝a＋blog ν, 及所得该二线性参数, a与b之间的线性关系(2) a＝c＋db. 预计该结果可能会在液相色谱指纹图谱研究和蛋白质组学中分离低丰度蛋白时有潜在的应用价值.     

Numerical simulation of solid tumor angiogenesis with Endostatin treatment： a combined analysis of inhibiting effect of anti-angiogenic factor and micro mechanical environment of extracellular matrix

To investigate the influence of anti-angiogenesis drug Endostatin on solid tumor angiogenesis, a mathematical model of tumor angiogenesis was developed with combined influences of local extra-cellular matrix mechanical environment, and the inhibiting effects of Angiostatin and Endostatin. Simulation results show that Angiostatin and Endostatin can effectively inhibit the process of tumor angiogenesis, and decrease the number of blood vessels in the tumor. The present model could be used as a valid theoretical method in the investigation of anti-angiogenic therapy of tumors.     

A method to determine Young＇s modulus of soft gels for cell adhesion

A convenient technique is reported in this note for measuring elastic modulus of extremely soft material for cellular adhesion. Specimens of bending cylinder under gravity are used to avoid contact problem between testing device and sample, and a beam model is presented for evaluating the curvatures of gel beams with large elastic deformation. A self-adaptive algorithm is also proposed to search for the best estimation of gels＇ elastic moduli by comparing the experimental bending curvatures with those computed from the beam model with preestimated moduli. Application to the measurement of the property of polyacrylamide gels indi- cates that the material compliance varies with the concentrations of bis-acrylamide, and the gels become softer after being immersed in a culture medium for a period of time, no matter to what extent they are polymerized.     

两指标B值强鞅空间的强原子分解

定义了两指标B值强鞅空间和强原子,利用Banach空间的光滑性建立了两指标B值强鞅空间s~∑α^p的强原子分解定理,应用强原子分解定理证明了一些两指标B值强鞅不等式.     

两层液体Bénard-Marangoni对流的实验研究

采用粒子图像测速技术(PIV)对两层流体B(en)ard-Marangoni对流进行了实验研究.研究了各种不同厚度比下的临界对流模式,同时研究了在温差变大时向超临界对流模式转化过程.实验结果表明,界面张力对各种对流模式的形成和转变具有重要的作用.     

Numerical investigation on evolution of cylindrical cellular detonation

Cylindrical cellular detonation is numerically investigated by solving two- dimensional reactive Euler equations with a finite volume method on a two-dimensional self-adaptive unstructured mesh. The one-step reversible chemical reaction model is applied to simplify the control parameters of chemical reaction. Numerical results demonstrate the evolution of cellular cell splitting of cylindrical cellular detonation explored in experimentas. Split of cellular structures shows different features in the near-field and far-field from the initiation zone. Variation of the local curvature is a key factor in the behavior of cell split of cylindrical cellular detonation in propagation. Numerical results show that split of cellular structures comes from the self-organization of transverse waves corresponding to the development of small disturbances along the detonation front related to detonation instability.