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21.
Bi12TiO20纳米粉体的制备及其光吸收特性研究 总被引:3,自引:0,他引:3
以钛酸四丁酯和硝酸铋为原料 ,利用化学溶液分解法制备了Bi12 TiO2 0 纳米多晶粉体 .采用XRD和TEM对其结构和形貌进行了表征 .结合热重 差热 (TG DTA)分析 ,探讨了Bi12 TiO2 0 晶相的形成机理 .通过UV Vis漫反射谱的测定 ,研究了Bi12 TiO2 0 纳米晶粉体的光吸收特性 .结果显示 ,从组成为化学计量比的前驱液中可以很容易制得纯Bi12 TiO2 0 纳米晶粉体 ,该Bi12 TiO2 0 纳米晶粉体呈现了在很宽的波长范围内 (5 6 0~ 385nm )对光的吸收的特性 . 相似文献
22.
Parameters of Gaussian multivariate models are often estimated using the maximum likelihood approach. In spite of its merits, this methodology is not practical when the sample size is very large, as, for example, in the case of massive georeferenced data sets. In this paper, we study the asymptotic properties of the estimators that minimize three alternatives to the likelihood function, designed to increase the computational efficiency. This is achieved by applying the information sandwich technique to expansions of the pseudo-likelihood functions as quadratic forms of independent normal random variables. Theoretical calculations are given for a first-order autoregressive time series and then extended to a two-dimensional autoregressive process on a lattice. We compare the efficiency of the three estimators to that of the maximum likelihood estimator as well as among themselves, using numerical calculations of the theoretical results and simulations. 相似文献
23.
We study a generalized Crank–Nicolson scheme for the time discretization of a fractional wave equation, in combination with
a space discretization by linear finite elements. The scheme uses a non-uniform grid in time to compensate for the singular
behaviour of the exact solution at t = 0. With appropriate assumptions on the data and assuming that the spatial domain is convex or smooth, we show that the
error is of order k
2 + h
2, where k and h are the parameters for the time and space meshes, respectively. 相似文献
24.
Summary.
This paper is concerned with a high order convergent
discretization for the semilinear reaction-diffusion problem:
,
for , subject to ,
where .
We assume that on
, which
guarantees uniqueness of a solution to
the problem. Asymptotic properties of
this solution are discussed. We consider a
polynomial-based three-point
difference scheme on a simple piecewise
equidistant mesh of Shishkin type.
Existence and local uniqueness of a solution
to the scheme are analysed. We
prove that the scheme is almost fourth order
accurate in the discrete maximum
norm, uniformly in the perturbation parameter
. We present numerical
results in support of this result.
Received February 25, 1994 相似文献
25.
A robust and efficient adaptive reweighted estimator of multivariate location and scatter 总被引:1,自引:0,他引:1
Daniel Gervini 《Journal of multivariate analysis》2003,84(1):116-144
This article proposes a reweighted estimator of multivariate location and scatter, with weights adaptively computed from the data. Its breakdown point and asymptotic behavior under elliptical distributions are established. This adaptive estimator is able to attain simultaneously the maximum possible breakdown point for affine equivariant estimators and full asymptotic efficiency at the multivariate normal distribution. For the special case of hard-rejection weights and the MCD as initial estimator, it is shown to be more efficient than its non-adaptive counterpart for a broad range of heavy-tailed elliptical distributions. A Monte Carlo study shows that the adaptive estimator is as robust as its non-adaptive relative for several types of bias-inducing contaminations, while it is remarkably more efficient under normality for sample sizes as small as 200. 相似文献
26.
We deal with the q-numerical radius of weighted unilateral and bilateral shift operators. In particular, the q-numerical radius of weighted shift operators with periodic weights is discussed and computed. 相似文献
27.
Runge–Kutta based convolution quadrature methods for abstract, well-posed, linear, and homogeneous Volterra equations, non
necessarily of sectorial type, are developed. A general representation of the numerical solution in terms of the continuous
one is given. The error and stability analysis is based on this representation, which, for the particular case of the backward
Euler method, also shows that the numerical solution inherits some interesting qualitative properties, such as positivity,
of the exact solution. Numerical illustrations are provided. 相似文献
28.
A fictitious domain approach to the numerical solution of PDEs in stochastic domains 总被引:1,自引:0,他引:1
We present an efficient method for the numerical realization of elliptic PDEs in domains depending on random variables. Domains
are bounded, and have finite fluctuations. The key feature is the combination of a fictitious domain approach and a polynomial
chaos expansion. The PDE is solved in a larger, fixed domain (the fictitious domain), with the original boundary condition
enforced via a Lagrange multiplier acting on a random manifold inside the new domain. A (generalized) Wiener expansion is
invoked to convert such a stochastic problem into a deterministic one, depending on an extra set of real variables (the stochastic
variables). Discretization is accomplished by standard mixed finite elements in the physical variables and a Galerkin projection
method with numerical integration (which coincides with a collocation scheme) in the stochastic variables. A stability and
convergence analysis of the method, as well as numerical results, are provided. The convergence is “spectral” in the polynomial
chaos order, in any subdomain which does not contain the random boundaries. 相似文献
29.
Effect of Deborah number and phase difference on peristaltic transport of a third-order fluid in an asymmetric channel 总被引:1,自引:0,他引:1
The effect of a third-order fluid on the peristaltic transport in an asymmetric channel is studied. The wavelength of the peristaltic waves is assumed to be large compared to the varying channel width, whereas the wave amplitudes need not be small compared to the varying channel width. The channel asymmetry is produced by choosing the peristaltic wave train on the walls to have different amplitudes and phase. The flow is investigated in a wave frame of reference moving with velocity of the wave. The effects of Deborah number, phase difference, varying channel width and wave amplitudes on the pumping characteristics, streamline pattern and trapping phenomena are investigated. It is observed that the trapping regions increase as the channel becomes more and more symmetric and the trapped bolus volume decreases for increasing Deborah number, phase difference and varying channel width whereas it increases for increasing flow rate and wave amplitudes. Furthermore, the obtained results could also have applications to a range of peristaltic flows for a variety of non-Newtonian fluids such as aqueous solutions of high-molecular weight polyethylene oxide and polyacrylamide. 相似文献
30.
Michèle Audin 《manuscripta mathematica》2007,124(4):533-550
In this paper, we investigate symplectic manifolds endowed with a Morse–Bott function with only two critical submanifolds,
one of which is Lagrangian while the other one is symplectic. 相似文献