Research progress on thermal protection materials and structures of hypersonic vehicles

Hypersonic vehicles represent future trends of military equipments and play an important role in future war. Thermal protection materials and structures, Which relate to the safety of hypersonic vehicles, are one of the most key techniques in design and manufacture of hypersonic vehicles. Among these materials and Structures, such as metallic temperature protection structure, the temperature ceramics and carbon/carbon composites are usually adopted in design. The recent progresses of research and applica- tion of ultra-high temperature materials in preparation, oxidation resistance, mechanical and physical characterization are summarized.     

离子色谱法测定沙坦类药物中的叠氮酸根

选用IonPac AS18离子色谱柱分离,利用在线淋洗液发生器自动产生氢氧化钾梯度淋洗液,以抑制电导降低淋洗液的背景电导进行沙坦类药物中叠氮化钠含量的测定.该方法可以将药物中的各类杂质有效分离,简化了样品的预处理,提高了测定的灵敏度.研究表明:叠氮根的检出限(S/N=3)为0.23/μg·L-1,检测的线性范围在0.001～20 mg·L-1,其相关系数为r2>0.999 2.采用该方法测定了厄贝沙坦,氯沙坦试样及中间体保护基溴化物中的叠氮化钠含量,结果令人满意.     

基于环境可信的关键档案保护系统的设计与实现

提出并实现了基于windOWS NTFS和FAT32文件系统的关键档案保护系统.该系统采用权限验证、环境可信验证,数据完整性验证和透明加解密等技术手段,对系统的环境信息进行检测并生成环境可信证书保存于USBKEY中.通过权限认证的可信用户只能访问相应权限的档案;木马和病毒无法对关键档案进行访问;脱离可信环境的档案由于无法进行认证将无法使用,从而实现了对关键档案的保护.测试结果表明,该系统能够很好地满足关键档案机密性、完整性以及防泄漏等需求,具有较好的可行性和实用性.     

Preservation of Linear Constraints in Approximation of Tensors

For an arbitrary tensor (multi-index array) with linear constraints at each direction, it is proved that the factors of any minimal canonical tensor approximation to this tensor satisfy the same linear constraints for the corresponding directions.     

苯并寡聚乙二氧链螺旋体的合成

以对甲氧基苯酚、对苄氧基苯酚、对苯二酚和四乙二醇二磺酸酯这些简单化合物为原料,通过磺酸酯与酚的亲核取代反应及苄基保护、钯碳氢化去保护策略制备得到了4种新颖的苯并寡聚乙二氧链螺旋体化合物.     

烯丙基保护基在多羟基化合物中的应用

烯丙基保护基由于能够在温和的反应条件下,在羟基、氨基等基团中引入和脱除,并且具有很好的区域选择性和化学选择性,因此被广泛应用于有机合成中。本文介绍了烯丙基保护基的发展历史,综述了烯丙保护基对多羟基化合物中不同羟基的选择性保护应用,并阐述了烯丙保护基的引入和脱除的机理及方法。     

An efficient quantum secure direct communication scheme with authentication

In this paper an efficient quantum secure direct communication (QSDC) scheme with authentication is presented, which is based on quantum entanglement and polarized single photons. The present protocol uses Einstein--Podolsky--Rosen (EPR) pairs and polarized single photons in batches. A particle of the EPR pairs is retained in the sender's station, and the other is transmitted forth and back between the sender and the receiver, similar to the `ping--pong' QSDC protocol. According to the shared information beforehand, these two kinds of quantum states are mixed and then transmitted via a quantum channel. The EPR pairs are used to transmit secret messages and the polarized single photons used for authentication and eavesdropping check. Consequently, because of the dual contributions of the polarized single photons, no classical information is needed. The intrinsic efficiency and total efficiency are both 1 in this scheme as almost all of the instances are useful and each EPR pair can be used to carry two bits of information.     

基于羟基保护的百里酚催化加氢合成薄荷醇

薄荷醇;薄荷酮;百里酚;羟基保护;催化加氢;反应机理     

诊断中性束加速电源打火检测与保护电路的研究与设计

通过检测打火短路过程中产生较大的di/dt 和du/dt 来实现高压电源的打火短路保护。在研究了中性束加速电源控制和保护特点的基础上, 设计了诊断中性束加速电源在打火短路过程中的di/dt 和du/dt 的检测电路和相应的保护电路, 实现提前对加速器高压电源打火短路的保护。     

巨豆三烯酮的合成及表征

采用这种合成方法的优点是原料易得,反应条件温和,操作比较简单,主要步骤产率较高,是合成目标产物的一种新方法,国内外未见文献报道。根据拟定的合成路线,通过实验对各步反应进行了研究,部分中间体经过折光率、红外(IR)、核磁共振(HNMR)、质谱(MS)等分析确定了其结构。实验证明该合成方法简单可行,目标产物的产率达24.3%,具有一定的继续研究开发价值。