2-碘-N-甲基苯磺酰胺的合成新方法和分子结构

选用新方法合成了2-碘—N-甲基苯磺酰胺，通过^1H NMR,^13C NMR,^13C DEPT NMR(Distortionless Enhancement by Polarization Transfer NMR)和MS确证的其结构。     

Indriect Determination of CTMAB with Sodium Chloride and Ammonium Thiocyanate by Floatation and Separation of Zine

A new method for indirect determination of cetyl-trimethyl ammonium bromide (CTMAB) with NaCl and NH4SCH by floatation and separation of zinc has been studied.The study shows that Zn(Ⅱ） can associate with NH4SCN and CTMAB to form insoluble ternary ion-association complex,and the precipitate can float on the surface of the liquid phase.A good linear relationship is observed between the floatation yield(E%) of Zn(Ⅱ） and the amount of CTMAB.On the ground,CTMAB Can be indirectly determined by determining E% of Zn(Ⅱ）.The results were satisfactory.     

X波段盘圈加速结构热阴极微波电子枪的研究

介绍了采用盘圈(DAW)加速结构在11.43GHz下研制的热阴极微波电子枪注入器，分析了注入器中DAW加速结构支撑杆对于微波特性的影响以及加速结构中的模式重叠问题. 针对该结构的强腔间耦合以及次临近耦合不能忽略的特点，对其调谐方法进行了分析研究.给出了该长腔链热阴极微波电子枪注入器的物理设计及粒子动力学计算结果，电子能量为5—6MeV，脉冲流强为40mA，电子束发射度为3.4πmm.mrad. 该微波电子枪的加工焊接已经完成，文中给出了其冷测结果.     

Proton Fraction in Neutron Star Matter and Three-Body Force Effects

The three-body force effects on the equation of state and its iso-spin dependence of asymmetric nuclear matter and on the proton fraction in neutron star matter have been investigated[1] within Brueckner Hartree-Fock (BHF) approach by using a microscopic three-body force. It is shown that, even in the presence of the three-body force, the empirical parabolic law of the energy per nucleon vs. isospin asymmetry β=(N-Z)/A is fulfilled in the whole asymmetry range 0 ≤β ≤1 and also up to high density. The three-body force provides a strong enhancement of symmetry energy at high density in agreement with relativistic approaches. Thecalculated proton fraction in β stable neutron star matter is given in Fig.l, where the thick solid line is the BHF prediction using AV18 TBF, while the dotted one is the BHF result using AVis. The thin solid line is the prediction of the Dirac-Brueckner approach taken from Ref.[2]. The results extracted according to the phenomenological paramete rizations of the symmetry energy suggested in Ref.[3] are also plotted. It is seen from     

三包层WⅠ和WⅡ型单模光纤波导色散特性的研究

研究了三包层WⅠ和WⅡ型单模光纤的波导色散特性。结果发现在相同条件下，三包层WⅠ和WⅡ型单模光纤零色散点的调节范围比传统的双包层W型单模光纤明显增大。详细分析了几何参量P、Q和光学参量R1、R2对单模传输时的波导色散特性和低次模截止频率的影响。所得的研究结果为获得更为理想的色散补偿、色散平坦光纤及设计新型无源光器件提供了重要的依据。计算波导色散的方法可推广到多包层光纤。     

烷烃类分子对NC0（A^2∑^＋）自由基的猝灭

采用激光光解—激光诱导荧光(LP—LIF)的方法，用266nm激光光解CHBr3分子产生CH自由基，再与N2O继续反应作为NCO自由基的产生源，用438．6nm激光将电子基态X^2∏i(00^10)的NCO激励到激发态A^2∑^+(00^00)上，通过检测激发态NCO时间分辨荧光信号，测得室温(298K)下NCO(A^2∑^+)被烷烃类分子猝灭的实验结果，获得了A^2∑^+(00^00)态猝灭速率常数．实验发现，随着烷烃分子中C—H键数增加，其猝灭截面也近线性增加，但随着分子体积增大，这种增加趋缓．     

炉液倾动重心近似计算的数学分析

为给转炉设计提供依据,需要计算炉液倾动的重心.利用数学方法将实际问题进行简化,通过分析炉液倾动过程中变量间的相互关系,来确定每个倾动角度对应情况下的液面位置.利用数学中三重积分的有关应用,进一步得出转炉在每个倾动角度为α∈(0,π2)时的重心计算方法及相关结论,在理论上为工程计算重心的方法提供参考.     

“先重后单”法用于求空间曲面所围立体的体积

学生在用三重积分求体积时，当体积由比较复杂的空间曲面所围成，同学们由于对这样的空间曲面缺乏了解，作图也比较困难，所以通常做起来会感到束手无策，但是如果曲面为绕某一轴的旋转曲面，通过使用“先重后单”的方法，并且充分利用初等数学的公式，可使问题得到大量的简化。下面我们举几个具体例子。例1求曲面（x2＋y2＋z2）2＝a2（x2＋y2－z2）所界体积。分析与解：实际上这个曲面是WZ平面上双纽线（y2＋z2）2＝a2（y2－z2）绕z轴旋转一周而成。过X轴一点D作平行于Xoy平面的平面截旋转体得一圆环，如图1所示，内半径DA，外半径DB，…