复方单硝酸异山梨酯-阿司匹林双缓释微丸胶囊的研制(Ⅱ)

以乙基纤维素、丙烯酸树脂Ⅱ和丙烯酸树脂Ⅲ为骨架材料分别制备单硝酸异山梨酯和阿司匹林混合骨架缓释微丸，并通过包薄膜衣进一步控制药物的释放。通过测定微丸的释放度对处方工艺进行评价，选择最佳微丸灌装胶囊．胶囊中两种药物均达到良好的缓释效果。符合中国药典对缓释制剂的要求．其体外释放过程同时符合Higuchi方程和一级释药方程，R^2值均在0．995以上。     

A New Pathway to Synthesize Cyclomercurated Ferrocenylimines Containing Heterocyclic Ring

The cyclomercurated ferrocenylimines containing heterocyclic ring were prepared by the condensation of cyclomercuration of acylferrocene with the appropriate heterocyclic amine.This procedure provides an efficient method for the synthesis of cyclomerucurated ferrocenylimines containing heterocyclic ring which are difficultly synthesized by the conventional method.The reaction mechanism is proposed.     

SYNTHESIS OF MACROPOROUS COPOLYMER OF VCA AND DVB

The reactivity ratios of vinyl acetate(VAc) and divinyl benzene (DVB) were calculated from the Q and e values.The possibility of the copolymerization of these two monomers was predicted and the copolymerization was carried out by suspension polymerization technique in the presence of pore producing agent (toluene and gasoine).The relative ratio of acetoxy group and benzene ring in the copolymer were monitored by IR measurement during the polymerization.The variation of pore properties,such as spectific surface area,porosity and average pore diameter,with polymerization time were determined.The copolymers at various polymerization time were alcoholyzed and thus the variation of the hydroxyl group content with polymerization time was studied.     

教学质量的时齐马尔可夫链评估法

本文研究了教学质量评估中的一种定量分析方法──时齐马尔可夫链评估法．阐明了这种方法的理论依据及其实施程序、并指出它较之其他教学质量评估法更显合理．     

不同羧酯化的聚马来酸十八醇酯齐聚物的镉盐LB膜成膜特…

由聚马来酸酐和十八醇合成了一系列不同羧酯比的聚马来酸十八醇酯，并以其为成膜材料，ＣｄＣｌ２水溶液为亚相制备了一系列聚马来酸十八醇酯镉盐ＬＢ膜，借助小角Ｘ射线衍射和红外吸收光谱表征了成膜条件及羧酯比对ＣｄＰＭＡ膜有序结构的影响。在较高膜压和快速提拉条件下，低羧酯比的ＣｄＰＭＡ可得到有序性很高的Ｙ－型ＬＢ多层膜；高羧酯比的ＣｄＰＭＡ得不到高有序性的ＬＢ多层膜。     

浅谈新《高中数学课程标准》对数学的认识

新《普通高中数学课程标准》已颁布 ,新一轮的高中数学教材的编写正在实施 .为了配合中学教师对新课标的学习 ,集广大教育工作者的智慧搞好新教材的建设 ,本刊将特开办“新课标、新教材论坛”专栏 ,欢迎广大读者将对新课标的认识 ,在新课标指导下的教材建设中的问题及处理方法等向本刊赐稿     

α-卤代萘与叔己酮碳负离子在Co(Ⅱ)络合物催化下的自由基链式亲核取代反应产物的薄层色谱定量分析

研究了以Co(Ⅱ)络合物为催化剂,α-卤代萘与叔己酮碳负离子的自由基链式亲核取代反应(SRN1)产物α-萘基叔己酮的薄层色谱扫描定量分析方法;定量分析的线性范围为0～4.4μg,平均回收率99%～101%,异板间相对标准偏差为2.3%,同板相对标准偏差为1.6%.     

丹聂耳电池电动势产生的机理

 1836年,英国化学家丹聂耳(Daniell)发明了一种原理上最简单的化学电池,通常称之为丹聂耳电池。电动势是化学电池的一个重要的性能参数。而电动势等于单位正电荷由负极通过电池内部移到正极时电池内非静电力(化学力)所做的功。它取决于电极材料的化学性质,与电池的大小无关。因此,本文就从物理化学角度来探讨丹聂耳电池电动势产生的机理。丹聂耳电池的结构如图1所示。电池的两个电极锌板和铜板分别浸在ZnSO₄溶液和CuSO₄溶液中。     

THE DIMENSION FOR RANDOM SUB-SELF-SIMILAR SET

In this article,the Hausdorff dimension and exact Hausdorff measure function of any random sub-self-similar set are obtained under some reasonable conditions.Several examples are given at the end.