橙皮素A的NMR研究

橙皮素A是从中药北沙参(Glehnia littoralis Fr. Schmidt ex Miquel)的正丁醇萃 取物中分离得到的一种8-O-4′-型异木脂素苷类化合物. 通过化学方法和波谱分析鉴 定了该 化合物的结构. 采用2D NMR技术对其NMR信号进行了全归属. DMSO-d₆代替CD₃OD作为溶剂，并利用重水交换，能准确读出偶合常数J_7,8值.      

寻找异面直线所成角的着眼点

异面直线所成角的问题,是空间“三大角”问题之一,历来是考试的重点内容。异面直线所成角的大小是用过空间一点分别引它们的平行线所成的锐角(或直角)来定义的,准确地定位角的顶点,平移直线构造三角形是解题的关键。下面通过举例谈谈寻找异面直线所成角的几种方法,请大家重点体会寻找异面直线所成角的几个着眼点。     

Tokamak Experiment and Tokamak Engineering——Development of the Plasma Diagnostics on HL-2A Tokamak

The main mission the HL-2A tokamak is of the experiments on to explore the divertor physics and to investigate the plasma confinement, transport and instabilities with high power auxiliary heating and advanced fuelling, it is necessary to develop more new diagnostics and increase the spatial and temporal resolutions of the measurements for exist system. Up to now, about 30 diagnostic systems have been moved from HL-1M to HL-2A tokamak. Other 10 diagnostic systems are being designed and installed on the device. In developed in last 2 years, will be presented.     

The First Results of Supersonic Molecular Beam Injection in the HL-2A Tokamak

HL-2A tokamak, the first tokamak with divertor in China, has been constructed and put into operation in 2002. The main parameters are R=1.65 m, a=0.4 m, BT=2.8 T, Ip = 0. 48 MA. The divertor of HL-2A is unique, because it is characterized with a large closed divertor chamber. The device has double divertor chamber, but now it is operating with lower single null configuration to study the physics of divertor for the next step design of a divertor. Supersonic molecular beam injection （SMBI） system with LN2 cooling trap was first installed and demonstrated on the HL-2A tokamak in 2004. The first results of SMBI into HL-2A plasma are to demonstrate the function of the HL-2A divertor and to observe the cold pulse propagation during multi-pulse SMBI on HL-2A Tokamak.     

回归模型中异方差或变离差检验问题综述

回归模型的异方差或变离差检验是统计诊断的重要课题。本文系统介绍了普通回归模型、广义回归模型和基于纵向数据的随机效应或自相关回归模型的异方差检验或变离差检验的研究概况和最新进展；同时介绍了作者关于非线性回归模型的相应工作，最后指出了若干有有待进一步研究的问题。     

二阶Melnikov函数及其应用

在Ｍｅｌｎｉｋｏｖ函数的种种应用中，目前常见到的仅是一阶形式。本文具体推导了二阶Ｍｅｌｎｉｋｏｖ函数的分析表达，提出了临界情况下考察双曲鞍点的稳定流形与不稳定流形相对位置的二阶判据，并成功地用于环面ｖａｎｄｅｒＰｏｌ方程的研究中。     

智能型表面测振系统

本文采用加速度传感器测量振动频谱的原理，对表面振动测量系统的实现进行了较为详细的描述，并用所研制的测振系统进行了实际测量，得到较为理想的实验结果．     

山东中生代晚期脉翅目昆虫一个新科

本文记述了一种化石蛉类,采自山东莱阳上侏罗统莱阳组,标本保存完好,其前、后翅的形状、大小和脉序特征差别十分显著,属于一个罕见的特化的类型,据此,建立了脉翅目一个新科,并就其亲缘关系和演化上的问题进行了讨论。     

雨水中微量银的萃取无焰原子吸收光谱测定

碘化银人工增雨水样以及天然雨雪中微量银的无焰原子吸收测定通常要采用离子交换,二乙基二硫代氯氨基甲酸二乙铵溶于甲基异丁酮萃取,双硫腙——四氯化碳萃取,阴离子树脂分离后再用吡咯烷二硫代甲酸铵水溶液萃取,硫代磷酸三辛酯——甲基异丁酮萃取,再以盐酸反萃,吡咯烷二硫代甲酸铵水溶液——甲基异丁