Fabrication of high temperature moiré grating and its application

The fabrication technique of high temperature moiré grating has been presented, which combines thermal nanoimprint process method and high temperature transferring technique. And the quality of grating was evaluated by analyzing its configuration through the Atomic Force Microscope (AFM) images. From the analysis, it was found that the optimal depth of grating will cause different stress condition in the process of vacuum deposition, and thicker deposited metal film on the grating may enhance the oxidation resistant ability. However, with the increase of the thickness of the metal film, cracks may occur in the film, In order to avoid this mechanical failure, the optimization of the depth of grating was performed. The optimized depth was obtained by analyzing the stress intensity using Finite Element Method (FEM). In order to verify the reliability of high temperature grating, the tensile experiment of high temperature alloy (GH3030) at 650 °C was carried out, and the experimental results demonstrated that fabricated high temperature grating was feasible.     

Displacement modal identification method of elastic system under operational condition

Modal identification of engineering structure in operation deals with the estimation of modal parameters from vibration data obtained in working conditions rather than laboratory conditions. After one structure destruction during a flight test, it was strongly required to carry out full-scale model testing to acquire the low-frequency vibration acceleration data of the investigated rocket (its structural dynamic properties could be represented by a beam). These vibration data were used to assess the modal properties of the modified structure. In this paper, a new modal identification method based on vibration displacement is suggested. The displacements of the measured points on the rocket are obtained by the integration of the low-frequency vibration accelerations during free flight test. In the method, the data are filtered through wavelet transform. For comparison, several methods are used to extract the modal frequencies of the investigated beam. In terms of the results of standard deviation of identified frequencies, it is believed that the generalized displacement-based modal identification method is more practicable in modal identification for similar problems.     

总体电路瞬态浪涌抑制

航天系统设备多,负载特性复杂,产生的瞬态浪涌电流通常对航天飞行器电气系统总体电路的危害很大。为了解决航天飞行器电气系统中瞬态浪涌如何有效抑制的问题,本文从瞬态浪涌形成的原理、影响及测量方法出发,在电气系统总体设计角度,分别从浪涌抑制电路、负载分配策略、负载休眠唤醒工作模式三方面提出了串电阻法、软启动法、负载休眠唤醒法等多种解决方案,通过搭建仿真试验平台和实物试验平台开展了相应的试验验证,瞬态浪涌电流得到了有效抑制。     

氮气开关流柱形成过程的理论研究

使用蒙特卡罗-粒子模拟方法对氮气开关中的流柱形成过程进行模拟, 并结合计算结果对其进行理论分析. 发现在流柱击穿发生前(即空间电荷场远小于本底电场), 等离子体的电离频率、电子平均能量及其迁移速度等都近似为常数, 因此可以解析求解电子数密度方程对等离子体的演化行为进行分析. 在击穿发生后, 随机碰撞过程会破坏初始等离子体区域分布的对称性, 并出现分叉的等离子体区域结构. 在放电过程中, 随着等离子体密度增加, 其内部基本保持电中性且电场不断减小, 靠近阴阳极两端电荷分离产生的净电荷密度不断增加, 场强也不断增加, 且靠近阳极端的电荷密度(绝对值)和场强都大于阴极端. 通过改变极板间电压发现, 平均电子能量随极板间场强增加而增加, 电子迁移速度随着场强近似线性增加, 电离频率随场强的变化快慢介于E⁴与E⁵之间.     

A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride

<正>2,4,6-Trichloroborazine has been recognized as a desirable monomer for the preparation of high-performance boron nitride fibers through polymer derived ceramics route.So a high yield and facile synthesis of 2,4,6-trichloroborazine is essential in practice. Using boron trichloride-dimethylsulfide complex((CH_3)_2S·BCl_3) and ammonium chloride(NH_4Cl) as starting materials and toluene(C_6H_5CH_3) as solvent,the synthesis of 2,4,6-trichloroborazine to give high yield is reported.     

石英玻璃分子动力学模拟中的原子电荷转移与系综选择

介绍了SiO2体系分子动力学模拟中的Si、O原子电荷转移问题;采用Morse势函数研究了原子电荷转移对石英玻璃模拟的影响,发现原子电荷转移在影响模型密度的同时,还直接影响着原子的最近邻距离.NPT和NVT系综下的模拟结果对比显示,系综对模型中原子最近邻情况影响不大,但在NVT系综下模拟结果表明实际玻璃中存在的较大的空隙结构,找到了以往模拟中密度结果偏高的原因,提出了一种较好的石英玻璃分子动力学建模的方法.该方法不但解决了在调整电荷时维持原子最近邻距离与保证模型密度之间的矛盾,而且可以很好地描述石英玻璃在远程结构上密度不均、存在较大空隙的无序结构.此外,原子自扩散系数的计算结果展示了空隙结构在石英玻璃扩散性质研究中的作用.     

考虑蜂窝高度效应的蜂窝夹芯板稳定性分析

蜂窝芯层等效弹性参数因受表板影响与其高度紧密相关,而传统蜂窝夹芯板稳定性模型未对其加以考虑。本文基于精化锯齿层合板理论,建立了蜂窝夹芯板稳定性模型。模型借助于解析均匀化方法获取蜂窝芯层等效模量,并因引入该方法而能够反映由蜂窝高度改变引起的蜂窝芯子等效模量变化对屈曲载荷产生的影响,即捕捉到了蜂窝芯子的高度效应。以四边简支蜂窝夹芯方板受单向面内压缩载荷作用为例进行了算例分析。算例结果表明,蜂窝芯子高度效应在蜂窝高度较低时明显,随着蜂窝高度增加,高度效应逐渐减弱。此外,高度效应在蜂窝芯层厚度比例较大时明显,随着蜂窝芯层厚度比例的持续下降,高度效应减弱直至消失。     

基于修正的Craig-Bampton法的大长径比助推器分离特性研究

在芯级周围布置助推器是提升运载能力的有效手段。对于长径比较高的助推器,结构呈现明显的局部弹性效应,这将对助推器分离的安全性产生影响。针对传统Craig-Bampton方法无法适用于大范围运动弹性体的不足,本文采用修正的Craig-Bampton法获得系统的正则化模态,使研究对象的所有模态与频率一一对应,实现分离体大范围刚体运动与弹性变形的有效耦合。基于该方法开展柔性多体动力学仿真,获得了不同模态阶数和结构刚度的弹性助推器分离系统的分离特性。研究结果表明,与传统的刚体模型相比,考虑助推器弹性效应的分离动力学模型更加贴近真实飞行情况。基于此,获得了各阶模态和结构刚度对分离安全边界的影响规律,其中以一阶横向模态最为敏感。通过研究弹性助推器的分离特性,为运载火箭助推器分离系统的工程实际应用提供理论参考和研究支撑。     

Discrete models of liquid-vapour phase change phenomena in porous media

This survey presents recent developments in the modelling of liquid-vapor phase change phenomena in porous media within the framework of the discrete approach. The pore network (or discrete) approach is first illustrated through the example of the evaporation at low capillary number of a pure liquid from a capillary porous medium. In particular, it is shown that invasion percolation patterns characterise the phase distribution. Then first results concerning the vaporisation of a liquid within the porous wick of a capillary evaporator are presented. These results show that capillary fingering patterns can be expected within the wick.     

A new proposed mechanism for the cathodic reduction of a carbon–chlorine bond in 2-acetylphenyltrichloroacetate

The cathodic reduction of 2-acetylphenyltrichloroacetate at a controlled potential of −0.5 V (vs SCE) yields 3,3-dichloro-4-hydroxy-4-methyl-3,4-dihydrocoumarin. The charge consumption is 1e⁻/substrate molecule, which is in agreement with a non-conventional R–X→R⁻+X mechanism.