西藏牦牛染色体的研究

应用外周血淋巴细胞短期培养法，结合Ｇ显带、Ｃ显带和Ａｇ－ＮＯＲｓ显带技术，研究了西藏耗牛的一般核型、Ｇ带、Ｃ带、Ａｇ－ＮＯＲｓ核型，并对耗牛的Ｙ染色体多态性进行了探讨．     

斜拉桥钢索的振动与张力问题

本文用弦振动理论分析了斜拉桥钢索的简谐振动和强迫振动，结合对钢索在常温下振动频率的测量，计算了常温某一温度的张力．采用线性插值由该张力值推算出其它气温下钢索的张力，并与实际的测量结果作了比较．     

犬复合营养素的研制及饲喂效果试验

试验以研制的由矿物质、微量元素、复合维生素和特殊香料组成的大用复合营养素饲喂２３头小型大和５０头大型犬，收到了明显效果。复合营养素对于预防营养和代谢疾病、佝偻病等有明显作用，亦有益于幼大生长发育及成年犬的繁殖，使用安全、可靠。     

新型稀土电子输运材料Tb(AcA)3·phen

Kido等人在文献[1]中报导,在研究有机电致发光(OEL)器件时发现,斓系化合物不能很好地传输载流子.但是,我们在实验中却现Tb(AcA)3phen·不仅是一种很好的OEL发射材料.而且具有很强的电子输运能力.     

MnBiDy(Sm)永磁膜的结构和磁性

报道了采用真空蒸镀的方法制备的MnBiDy(Sm)永磁膜的结构和磁性.Mn:Bi:Dy(Sm)的投料比为2:1:0.10.薄膜经过退出处理(350—425℃,保温4h)后,具有NiAs型hcp结构,C轴垂直膜面,剩余磁感应强度B=3.4-6.5kG,内禀矫顽力_MH_c≈3-8kOe,最大磁能积(BH)_(max)=13.39MG·Oe.实验发现,薄膜厚度对MnBiDy(Sm)永磁膜的结构和磁性具有很大的影响. 关键词：     

Quadratically constrained minimum cross-entropy analysis

Quadratically constrained minimum cross-entropy problem has recently been studied by Zhang and Brockett through an elaborately constructed dual. In this paper, we take a geometric programming approach to analyze this problem. Unlike Zhang and Brockett, we separate the probability constraint from general quadratic constraints and use two simple geometric inequalities to derive its dual problem. Furthermore, by using the dual perturbation method, we directly prove the strong duality theorem and derive a dual-to-primal conversion formula. As a by-product, the perturbation proof gives us insights to develop a computation procedure that avoids dual non-differentiability and allows us to use a general purpose optimizer to find an-optimal solution for the quadratically constrained minimum cross-entropy analysis.     

山东章丘明水地区二叠系“A”层硬质高岭土的研究

明水地区的硬质高岭土俗称焦宝石,即我国华北石炭二叠纪煤系地层申的“A”层铝土。明水地区的“A”层铝土具有耐火度高,化学成分稳定等特点,广泛用于日用陶瓷、电器、耐火材料等工业部门,是一种重要的工业原料。“A”层铝土在华北石炭二叠系煤系地层中分布普遍,层位稳定,其经济价值不低于煤,应当引起有关部门,特别是煤田地质勘探部门的重视。     

酚醛型吸附树脂对水体系中吡啶和N,N-二甲基苯胺的吸附性能研究

研究了酚醛型吸附树脂在水体系中对吡啶和N，N-二甲基苯胺的静态和动态吸附行为．结果表明，在水中树脂对吡啶和N，N-二甲基苯胺的吸附主要以疏水吸附机理进行；吸附吡啶和N．N-二甲基苯胺的初始阶段，即达到38．3～48．9％平衡吸附时，吸附速率数据和半经验速率方程很吻合：酚醛型吸附树脂等温吸附吡啶和N，N-二甲基苯胺的平衡吸附数据符合Langmuir方程，相关系数在0．99以上，酚醛型吸附树脂吸附吡啶和N，N-二甲基苯胺属单分子层吸附：用80％的乙醇溶液作洗脱剂来洗脱吸附吡啶已达饱和的JDW-2树脂，效果是很理想的．在3．6个床体积内洗脱率达91．52％，4．8个床体积内洗脱率达到94．85％。表明酚醛型吸附树脂具有优良的洗脱性能．     

Iodine(V) reagents in organic synthesis. Part 3. New routes to heterocyclic compounds via o-iodoxybenzoic acid-mediated cyclizations: generality, scope, and mechanism

The discovery and development of the o-iodoxybenzoic acid (IBX) reaction with certain unsaturated N-aryl amides (anilides) to form heterocycles are described. The application of the method to the synthesis of delta-lactams, cyclic urethanes, hydroxy amines, and amino sugars among other important building blocks and intermediates is detailed. In addition to the generality and scope of this cyclization reaction, this article describes a number of mechanistic investigations suggesting a single electron transfer from the anilide functionality to IBX and implicating a radical-based mechanism for the reaction.     

Chemical ionization mass spectrometry of nitrosamines

The mass spectra of eight nitrosamines have been recorded, with excitation by chemical ionization (CI) and electron impact (EI). Comparison of the intensities of the base peaks under CI and El conditions gives intensity ratios in the range 1.4-1.9 for low resolution measurements and up to 10 for high resolution measurements, confirming the enhanced sensitivity available in the CI mode.