基于热固振耦合的某附件壳体蠕变-热疲劳寿命预测方法

提出一种基于热固振耦合的某附件壳体蠕变 热疲劳寿命预测方法,主要是基于ANSYS Fluent模块进行流固热耦合,仿真结果得到的附件壳体温度场分布并通过实测数据进行结果验证,再通过温度场数据传递途径结合ANSYS Workbench模块进行附件壳体热固振耦合仿真得到壳体应力应变场,然后基于线性累计损伤理论耦合附件壳体蠕变持久寿命和热疲劳寿命,最终得到其蠕变 热疲劳寿命预测结果。针对附件壳体,一方面对比分析了单纯热疲劳寿命（41 063个循环寿命）与蠕变 热疲劳（39 054个循环寿命）,通过结果得知航空发动机附件系统高热环境下蠕变作用对附件壳体热疲劳寿命是存在显著影响的;另一方面对比分析了基于稳态温度场的蠕变 热疲劳（23 334个循环寿命）与基于瞬态温度场（考虑温变速率）的蠕变 热疲劳（24 545个循环寿命）,结果表明温变速率在一定程度上影响航空发动机附件系统结构的蠕变 热疲劳寿命。     

科技工作者心理健康素养现状

 心理健康素养主要指有助于维护和促进心理健康的知识、行为和意识,是影响心理健康的重要因素。为了解科技工作者心理健康素养的现状,2017年,依托全国调查站点对1.3305万名科技工作者进行心理健康知识调查;2018年,依托网络对2531名科技工作者开展了心理健康素养全面调查。调查发现：中国科技工作者的心理健康素养整体状况较好,高于其他职业人群,但是对心理健康知识的掌握不均衡;科技工作者的心理健康素养水平存在一定的群体差异：女性高于男性,25~44岁年龄组高于其他年龄组,学历越高心理健康素养水平也越高,其中硕士和博士最高,高中及中专以下最低。地区差异方面,东部地区最高,东北和西部地区次之,中部地区最低;北京、上海、广州和深圳等一线城市高于其他省会或直辖市、地县级城市。职业差异方面,教学人员最高,专业技术人员次之,卫生技术人员最低。     

A facile way for preparing tin nanoparticles from bulk tin via ultrasound dispersion

In this paper, we reported a facile and rapid process to prepare tin nanoparticles from bulk tin via ultrasound dispersion. The morphology and structure of synthesized tin nanoparticles were characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD), X-ray photoelectron spectrum (XPS) and thermogravimetric analysis (TGA). The results show that the morphology of tin nanoparticles is spherical and the structure of tin nanoparticles has the same crystal structure as the bulk tin. In addition, the tribological property of tin nanoparticles as additives in oil is evaluated on a four-ball tester and the results show that tin nanoparticles exhibit good performance in wear.     

拉压性能不同材料的几种结构的极限分析

给出了拉压性能不同材料（简称具有Ｓ－Ｄ效应的材料）的几种结构的极限载荷公式。揭示出材料的拉压性能不同对几种结构承载能力的影响规律。所给出的极限载荷公式可供工程设计人员参考。     

拉压性能不同材料全量型本构关系及厚壁筒的应力分析

将经典全量理论作了推广，考虑了应力状态及塑性体积变形对拉压性能不同材料的塑性行为的影响。应用该本构模型分别计算了厚壁筒在内压和外压作用下的应力分布。给出了径向应力、环向应力和轴向应力沿壁厚的分布图。将本文的计算解与拉压性能相同(不考虑体积变形、强化曲线唯一)的幂函数强化材料的厚壁筒的理论解进行了比较。结果表明，材料的拉压性能不同对厚壁筒的环向应力和轴向应力影响较大。因此，对于拉压性能不同材料，考虑到其对应力状态及塑性体积变形敏感时，是不能将其简化成拉压性能相同、体积不可压缩、强化曲线唯一的理想材料。     

Statistical Analysis of the Effect of Intensity Pattern Noise on the Displacement Measurement Precision of Digital Image Correlation Using Self-correlated Images

This paper discusses the effect of intensity pattern noise on the displacement measurement precision of digital image correlation (DIC). Through mathematical deduction, a formula is presented to estimate the displacement measurement error caused by intensity pattern noise. The resulting formula synthetically reflects the effects of the variance of noise, the intensity variance and the subset size on the displacement measurement precision. To verify the correctness of the resulting formula, two experiments are done. The first one is a real self-correlation experiment, and aims to analyze the effect of the subset size, while the second is a numerical self-correlation experiment, and is to analyze to the effect of the different noise levels. The experimental results are in good agreement with the theoretical predictions. The project is supported by the National Science Foundation of China (10572103).     

Uniform persistence and flows near a closed positively invariant set

In this paper, the behavior of a continuous flow in the vicinity of a closed positively invariant subset in a metric space is investigated. The main theorem in this part in some sense generalizes previous results concerning classification of the flow near a compact invariant set in a locally compact metric space which was described by Ura-Kimura (1960) and Bhatia (1969). By applying the obtained main theorem, we are able to prove two persistence theorems. In the first one, several equivalent statements are established, which unify and generalize earlier results based on Liapunov-like functions and those about the equivalence of weak uniform persistence and uniform persistence. The second theorem generalizes the classical uniform persistence theorems based on analysis of the flow on the boundary by relaxing point dissipativity and invariance of the boundary. Several examples are given which show that our theorems will apply to a wider varity of ecological models.     

Determination of diflubenzuron and chlorbenzuron in fruits by combining acetonitrile‐based extraction with dispersive liquid–liquid microextraction followed by high‐performance liquid chromatography

In this study, a simple and low‐organic‐solvent‐consuming method combining an acetonitrile‐partitioning extraction procedure followed by “quick, easy, cheap, effective, rugged and safe” cleanup with ionic‐liquid‐based dispersive liquid–liquid microextraction and high‐performance liquid chromatography with diode array detection was developed for the determination of diflubenzuron and chlorbenzuron in grapes and pears. Ionic‐liquid‐based dispersive liquid–liquid microextraction was performed using the ionic liquid 1‐hexyl‐3‐methylimidazolium hexafluorophosphate as the extractive solvent and acetonitrile extract as the dispersive solvent. The main factors influencing the efficiency of the dispersive liquid–liquid microextraction were evaluated, including the extractive solvent type and volume and the dispersive solvent volume. The validation parameters indicated the suitability of the method for routine analyses of benzoylurea insecticides in a large number of samples. The relative recoveries at three spiked levels ranged between 98.6 and 109.3% with relative standard deviations of less than 5.2%. The limit of detection was 0.005 mg/kg for the two insecticides. The proposed method was successfully used for the rapid determination of diflubenzuron and chlorbenzuron residues in real fruit samples.     

High-internal-phase-emulsion polymeric monolith coupled with liquid chromatography–electrospray tandem mass spectrometry for enrichment and sensitive detection of trace cytokinins in plant samples

High-internal-phase-emulsion polymers (polyHIPEs) show great promise as solid-phase-extraction (SPE) materials because of the tremendous porosity and highly interconnected framework afforded by the high-internal-phase-emulsion (HIPE) technique. In this work, polyHIPE monolithic columns as novel SPE materials were prepared and applied to trace enrichment of cytokinins (CKs) from complex plant samples. The polyHIPE monoliths were synthesized via the in-situ polymerization of the continuous phase of a HIPE containing styrene (STY) and divinylbenzene (DVB) in a stainless column, and revealed highly efficient and selective enrichment ability for aromatic compounds. Under the optimized experimental conditions, a method using a monolithic polyHIPE column combined with liquid chromatography–electrospray tandem mass spectrometry (LC–MS–MS) was developed for the simultaneous extraction and sensitive determination of trans-zeatin (tZ), meta-topolin (mT), kinetin (K), and kinetin riboside (KR). The proposed method had good linearity, with correlation coefficients (R ²) from 0.9957 to 0.9984, and low detection limits (LODs, S/N?=?3) in the range 2.4–47 pg mL^?1 for the four CKs. The method was successfully applied to the determination of CKs in real plant samples, and obtained good recoveries ranging from 68.8 % to 103.0 % and relative standard deviations (RSDs) lower than 16 %.