烯效唑的气相色谱分析

采用气相色谱分析烯效唑的含量，选用ＱＦ－１固定液，Ｃｈｒｏｍｏｓｏｒｂ Ｗ．Ｈ．Ｐ为担体，以邻苯二甲酸二丁酯为内标物，该方法标准偏差０．１５％，变异系 ０．１７％，烯效唑的平均回收率为９９．５９％．     

High power 1.3414 μm Nd:YAP cw laser

The eigen-oscillation mode of the Nd:YAP cw laser has been analysed. The influence of thermal effects arising from the pumping process on the output character of the 1.3414 μm Nd:YAP cw laser has been discussed. The crack problem of the reflective film at a 1.34 μm dielectric mirror has been solved. Based on the aforementioned work, we have been able to achieve an 82.8 W laser output at 1.3414 μm with a nearly polarized beam from a 5.8 mm diameter by 111 mm Nd:YAP rod. The overall efficiency and the slope efficiency are 1.15% and 2.02% respectively, and the fluctuation of the output power at 62 W is less than 1% during continuous operation for 45 min.     

电极的校正及应用

本文应用EDTA作为钙离子缓冲溶液,对自制涂丝钙离子选择电极(Ca-CWISE)进行了校正,与用标准系列稀释法相比,电极的线性范围扩大了三个数量级。文章还利用自制Ca-CWISE,采用Thomas等所用的简易pH-pM法,测定了柠檬酸钙的浓度稳定常数,IgK_(CaCit~-)=3.86(30℃,I=0.1)。     

基于排队的分销系统费用问题

用排队论的方法对商品分销过程的排队系统进行分析,确定了排队模型.给出统计平衡条件下的主要指标.讨论分销系统费用最优化,并进行实例分析.     

优质铝合金管制造工艺

针对我国用传统工艺（铸造－挤压工艺）生产５６０ｍｍ×７０ｍｍ超大特厚９１９铝合金管出现的多种质量缺陷（如力学性能差，组织中存在光晶和花边等缺陷），提出了一种生产这类超大特厚管的新工艺（由快速铸造、高柱体自由冲扩孔、高温慢速润滑挤压、混合校直等不同种类的加工工艺组合而成），成功地生产出了合格产品，并实现了批量生产     

关于一元线性回归简化计算公式的注记

本文用初等变换方法，给出了一元线性回归预测公式ｙ∧＝ａ＋ｂｘ中参数ａ和ｂ的简化计算公式．     

Growth-induced magnetic anisotropy in YIG

YIG film were grown by LPE and the substrate was carefully removed by grinding. From the⁵⁷Fe Moessbauer spectrum the orientation of magnetization was determined and the growth-induced magnetic anisotropy constant deduced. For (111) orientation YIG, the magnetic uniaxial anisotropy constant Ku was determined to be 2.3×10³ erg cm^–3.     

圆锥螺旋铣刀的铣削力仿真

应用微分几何理论，给出了圆锥螺旋赞和何特性，据此导出了三维非线性铣削力模型，继而采用非线性规划识别切削力系数。     

杜诗评解志疑（续）

唐诗的解释工作历来做的人很多，而且十分深入，这也是一笔丰富的文学遗产。本文就杜甫诗若干名篇名句的评解提出讨论，归综诸说，较论异同，断以己见，供阅读和研究参考。     

An X‐shaped π‐conjugated polymer comprising of fluorene units and anthracene units with high efficiency. Synthesis and optical and electrochemical properties

A new X‐shaped π‐conjugated monomer comprising of fluorene units and anthracene units was synthesized, and it was used to fabricate the new X‐shaped π‐conjugated polymers and investigate the properties of the new polymers. Using different molar ratios between such monomer and a fluorene monomer gave three polymers that showed higher absolute PL quantum yields than the linear polyfluorene (PF) in the solid state. After thermal annealing at 200 °C for 4 h, the linear PF showed an additional bathochromic emission at about 550 nm, whereas such red‐shifted emission was fully eliminated for the X‐shaped polymers. The electroluminescent devices based on the X‐shaped polymers with a configuration of ITO/PEDOT:PSS/polymer/LiF/Ca/Al displayed blue emission with low turn‐on voltage and high brightness. © 2008 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 46: 5616–5625, 2008