Liquid phase oxidation of p-chlorotoluene to p-chlorobenzaldehyde over cobalt-doped mesoporous titania with a crystalline framework

Cobalt-doped mesoporous titania with a crystalline framework synthesized by surfactant templating method presented highly selective (99%) and reasonable conversion rate (49%) of catalytic oxidation of para-chlorotoluene to para-chlorobenzaldehyde in acetic acid using aqueous hydrogen peroxide as oxidant for the first time. Recycling of the catalyst indicates that the catalyst can be used a number of times without losing its activity to a greater extent. By contrast, cobalt-doped mesoporous titania without a crystalline structure and cobalt doped the commercial titania, Degussa P25 prepared by impregnation method with the similar concentration of cobalt were found inactive. The effects of catalyst concentration, reaction time, reaction temperature, and solvents on the performance of the catalyst were also investigated.     

网络时代下对高校思想政治教育的几点思考

网络技术的发展,对学生行为方式、思想品德的形成、心理和人格的健康发展产生深刻的影响。网络的普及对传统模式教育方法提出了新挑战,对思想政治教育工作既有有利的因素也有负面影响。本文探讨了网络时代如何面对思想政治教育工作中的新问题。     

High Voltage Pulse Power and the Technics for the Capacitor Power-Storage Type

Lower hybrid wave （LHW）, electro cyclotron （EC） and neutral beam injection （NBI） etc. are the important methods of auxiliary heating. They would be devoted to the HL-2A tokamak step by step. In order to satisfy the debug of each system and the need of the experiment, the system should be equipped with high voltage pulse power （HVPP） according to the requirement.     

开放式微波消解与干灰化法消解测量食品中铅的方法比较

对开放式微波消解法与干灰化法消解测量食品中铅的方法进行了比较，试验表明，前者操作简易，试验周期短，在测量精度和加标回收率方面两种方法无显著性差别。     

水切割机中超高压预应力复合缸体研究

针对水切割机中高压缸经常爆裂的现象,本文研究了预应力缸体、高压缸的失效原因及预应力缸体的基本特点,最后进行了缸体疲劳实验。     

一种适合于B/S和C/S应用的经济型实体鉴别公钥密码器

针对我国电子政务发展的需求,提出一种适合于B/S和C/S应用的经济型实体鉴别公钥密码器方案,研究出相关密码算法,并论证了其安全性.与采用现有公钥密码算法的密码器相比,这种密码器能有效降低对硬件运算能力的需求,从而降低造价,若在居民身份卡系统等社会信任服务系统中推广,可为国家节省大量资金.     

现浇框架结构梁、柱、板协同工作体系的有限元方法及其内力特征

应用多种单元集成总刚的有限元法，分析现浇梁、柱、板结构体系在不同工况下的内力分布及组合设计内力，从理论分析角度揭示一些设计计算及构造上值得重视的特征。     

单摆测重力加速度的研究

本文分析了单摆测重力加速度的误差主要来源，在测量装置，测量工具和测量方法上进行改进，从而有效地提高了测量精度。     

Efficient Synthesis of the Oxadiazole Biphenyl Tetrazoles

Since the discovery of losartan[1](DUP 753), the leading non-peptide AT1 antagonist, several highly potent AT1 selective antagonists bearing heterocycles have been reported. [2] The tetrazole group is a common acidic functionpresent in many these antagonists.     

单件小批生产系统下模糊优化的动态随机投入产出模型

本文针对单件小批量生产系统 ,建立了模糊优化的动态随机投入产出模型 ,同时给出了该模型的递推解法 ,并用此模型对某单件小批企业在生产计划期的商品量进行了规划