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191.
Introduction A welded structure must be inspected to guarantee that the weld quality meets the design requirements to as- sure safety and reliability. However, X-ray image analyses and defect recognition are very complex. Most difficulties lie in finding … 相似文献
192.
Shang Chen Chenyan Ren Yuan Ji Dongke Liu Xinke Zhang Fengshan Wang 《Molecules (Basel, Switzerland)》2022,27(13)
Thymus immunosuppressive pentapeptide (TIPP) is a novel anti-inflammatory peptide with high efficacy and low toxicity. This study aims to establish a selective LC-MS/MS method for analyzing the analyte TIPP in biological samples, laying the foundation for further PK and PD studies of TIPP. Protein precipitation was conducted in acetonitrile supplemented with 2% formic acid and 25 mg/mL dithiothreitol as a stabilizer, which was followed by backwashing the organic phase using dichloromethane. The chromatographic separation of TIPP was achieved on a C18 column with a gradient elution method. During positive electrospray ionization, TIPP was analyzed via multiple-reaction monitoring. The linear relationships between the concentration of TIPP and peak area in murine plasma cell lysates, supernatants, and the final cell rinse PBS were established within the ranges of 20–5000 ng/mL, 1–200 ng/mL, 10–200 μg/mL, and 0.1–20 ng/mL, respectively (r2 > 0.99). Validated according to U.S. FDA guidelines, the proposed method was proved to be acceptable. Such a method had been successfully applied to investigate the pharmacokinetics of TIPP in mice via subcutaneous injection. The plasma half-life in mice was 5.987 ± 1.824 min, suggesting that TIPP is swiftly eliminated in vivo. The amount of TIPP uptake by RBL-2H3 cells was determined using this method, which was also visually verified by confocal. Furthermore, the effective intracellular concentration of TIPP was deduced by comparing the intracellular concentration of TIPP and degrees of inflammation, enlightening further investigation on the intracellular target and mechanism of TIPP. 相似文献
193.
姚渊 《青海师范大学学报(自然科学版)》2006,(3):15-17
对苏步青教授在文[1]中介绍的改良后的Hurwitz方法再作一些改进,先对Wirtinger引理进行推广,再用推广后的Wirtinger不等式很自然而简洁地推出了等周不等式. 相似文献
194.
主要研究了Hilbert空间H上全体幂等算子关于左星序的性质, 其中左星序(left-star order)A*≤B定义为A*A=A*B且R(A)⊆R(B)。设A和B是幂等算子, 给出了A*≤B的等价条件和算子矩阵形式表示。同时, 当A*≤B时, 讨论了星序的上、下确界A∧B和A∨B的存在性及其表示。 相似文献
195.
Shunli Ni Sheng Ma Yuhang Zhang Jie Yuan Haitao Yang Zouyouwei Lu Ningning Wang Jianping Sun Zhen Zhao Dong Li Shaobo Liu Hua Zhang Hui Chen Kui Jin Jinguang Cheng Li Yu Fang Zhou Xiaoli Dong Jiangping Hu Hong-Jun Gao Zhongxian Zhao 《中国物理快报》2021,(5):133-137
We systematically measure the superconducting(SC) and mixed state properties of high-quality CsV_3 Sb_5 single crystals with T_c~3.5 K.We find that the upper critical field H_(c2)(T) exhibits a large anisotropic ratio of H_(c2)~(ab)/H_(c2)~c~9 at zero temperature and fitting its temperature dependence requires a minimum two-band effective model.Moreover,the ratio of the lower critical field,H_(c1)~(ab)/H_(c1)~c,is also found to be larger than 1,which indicates that the in-plane energy dispersion is strongly renormalized near Fermi energy.Both H_(c1)(T) and SC diamagnetic signal are found to change little initially below T_c~3.5 K and then to increase abruptly upon cooling to a characteristic temperature of ~2.8 K.Furthermore,we identify a two-fold anisotropy of in-plane angular-dependent magnetoresistance in the mixed state.Interestingly,we find that,below the same characteristic T~2.8 K,the orientation of this two-fold anisotropy displays a peculiar twist by an angle of 60° characteristic of the Kagome geometry.Our results suggest an intriguing superconducting state emerging in the complex environment of Kagome lattice,which,at least,is partially driven by electron-electron correlation. 相似文献
196.
197.
Shaochuan Li Caiping Liu Qihui Chen Feilong Jiang Daqiang Yuan Qing-Fu Sun Maochun Hong 《Chemical science》2022,13(31):9016
Coordination hosts based on flexible ligands have received increasing attention due to their inherent adaptive cavities that often show induced-fit guest binding and catalysis like enzymes. Herein, we report the controlled self-assembly of a series of homo/heterometallic coordination hosts (Me4enPd)2n(ML)n [n = 2/3; M = Zn(ii)/Co(ii)/Ni(ii)/Cu(ii)/Pd(ii)/Ag(i); Me4en: N,N,N′,N′-tetramethylethylenediamine] with different shapes (tube/cage) from a flexible tetraazacyclododecane-based pyridinyl ligand (L) and cis-blocking Me4enPd(ii) units. While the Ag(i)-metalated ligand (AgL) gave rise to the formation of a (Me4enPd)4(ML)2-type cage, all other M(ii) ions led to isostructural (Me4enPd)6(ML)3-type tubular complexes. Structural transformations between cages and tubes could be realized through transmetalation of the ligand. The buffering effect on the ML panels endows the coordination tubes with remarkable acid–base resistance, which makes the (Me4enPd)6(ZnL)3 host an effective catalyst for the CO2 to CO32− conversion. Control experiments suggested that the integration of multiple active Zn(ii) sites on the tubular host and the perfect geometry match between CO32− and the cavity synergistically promoted such a conversion. Our results provide an important strategy for the design of adaptive coordination hosts to achieve efficient carbon fixation.A series of coordination hosts were prepared and their applications in CO2 fixation were studied. 相似文献
198.
幽默是文学的一种表现形式,其产生的原因有很多。合作原则是语用学的重要原则之一,很多幽默的产生源于对合作原则的违反。文章从语用学角度,通过大量实例,探讨违反合作原则产生的幽默效果。 相似文献
199.
袁为民 《上海交通大学学报》1995,29(2):148-151
通用多边形覆盖算法及图形分解软件袁为民(南洋信息与控制工程公司)关键词算法,多边形覆盖,掩膜图形分解中留法分类号TP3171文献回顾和算法简述针对集成工艺中所涉及的掩膜图形的多样性和复杂性,本文提出一种通用性较强的多边形覆盖算法,并已实现为图形分解软... 相似文献
200.
面向网格简化的STL拓扑信息快速重建算法 总被引:10,自引:0,他引:10
以STL模型为研究对象,针对网格简化要求的显式、完整拓扑关系,提出了一种快速构建拓扑信息的新算法.在优化选取拓扑信息构建顺序的基础上,一方面针对各种几何元素的特点选取有效的数据结构,在数据组织层次上保证顶点归并的效率和几何元素的检索效率;另一方面,充分利用顶点与其邻接点和邻接面的关系,将边归并的比较范围控制在顶点的邻域,并在全局遍历时选择数据规模最小的顶点.算法具备优良的时间效率性,提高了网格简化预处理的效率. 相似文献