草酸生产水洗塔设计

对目前国内合成法生产草酸所用水洗塔,采用加大水量到50m~3/h,提高塔板开孔率到19.55%(一般推荐6%～12%),降低溢流堰高为25mm,增大降液管到下层塔板间距为95mm 的办法,使洗涤后的气体达到要求。     

Average Atom Model in Hot Plasmas

Ａｖｅｒａｇｅ　Ａｔｏｍ　Ｍｏｄｅｌ　ｉｎ　Ｈｏｔ　ＰｌａｓｍａｓＡｖｅｒａｇｅＡｔｏｍＭｏｄｅｌｉｎＨｏｔＰｌａｓｍａｓ￥ＹｕａｎＪｉａｎｈｕｉ；ＳｕｎＹｏｎｇｓｈｅｎｇ；ＺｈｅｎｇＳｈａｏｔａｎｇ（ＩｎｓｔｉｔｕｔｅｏｆＡｐｐｌｉｅｄＰｈｙｓｉｃ...     

苯乙烯基取代的缩杂环卓酮化合物的合成

探讨了３－肉桂酰基酚酮及其亲电取代产物与盐酸羟氨和盐酸苯肼的反应，合成了１０个苯乙烯基取代的缩杂环酮新化合物，并用元素分析及光谱分析证实了它们的结构。     

Ga1-xInxAs/InAsyP1-y/InP异质结的MOCVD生长及表征

Ga1-xInxAs(x>0.53)材料是未来长距离低损耗光纤通信的理想光源材料和探测器材料之一.我们采用水平常压MOCVD系统,在InP衬底上成功地生长了Ga1-xInxAs(x>0.53)/InAsyP1-y/Inp异质结材料.其中InAs1-yPy为组份阶梯变化的多层结构.由样品的(400)面X光衍射结果测定了各层组份.由二次离子质谱(SIMS)得到了样品剖面组份变化结果,证明InAs1-yPy层组份为阶梯状变化的.通过对光致发光结果和X光衍射结果比较,可以看到,InAsyP1-y层通过位错和弹性畸变二种方式来释放或积累Ga1-xInxAs与InP间的失配应力,从而减少了Ga1-xInxAs中的失配位错.有效地改善了Ga1-xInxAs的质量.已获得了x高达0.94表面光亮的Ga1-xInxAs/InAs1-yPy/InP异质结材料.     

Complexes in polymers IV. FTIR microscopic characterization of thin organic polymer films containing embedded transition-metal carbonyl complexes

Thin films of polystyrene (PS), poly(methyl methacrylate) (PMMA) and polystyrene-polyacrylonitrile copolymer (PS-AN), containing various embedded transition-metal complexes, have been studied by FTIR microscopy. The spatial distributions of the transition-metal carbonyl complexes throughout the thin organic polymer films have been determined by a two-dimensional IR mapping procedure. The spectral variations observed in the distribution of the metal carbonyls throughout the different polymer films are discussed. The IR data show that the technique used to prepare the organometallic-embedded thin films (viz. freeze-drying of solutions followed by hot mechanical pressing of the residues) does in general lead to homogeneous films which may eventually find industrial application, e.g. as membrane sensors for small molecules.     

一类二维非线性Schrodinger方程的吸引子及其维数

本文研究了一类二维非线性Ｓｃｈｒｏｄｉｎｇｅｒ方程解的有限维行为，我们得到了此方程存在吸引子，并得到了此吸引子维数的上界估计     

Millimeter wave beams diffracted from reflecting gratings

According to the angular-spectrum method, a radiation beam of an antenna horn in the Fresnal region is decomposed into the plane waves with the fast Fourier transform algorithm and the waves diffracted from a reflection grating are superposed as a diffracted beam. Compared with the reflected beam from the same size mirror, the radiation half width of the diffracted beam from a grating is narrower and its lateral shape is shift. These performances have been experimentally verified at Ka-band by: (1). The relative diffraction efficiencies in the first order with two triangular gratings which is put along propagating direction of a beam produced by a conical lens-horn. (2). H-plane lateral width with power—3dB lapsed of the focus beam from a grating and a mirror in a grating spectrometer for millimeter waves (25–100 GHz).     

在BBO中产生217.3-2 21.4nm高功率和频输出

用Q-YAG激光的三次谐波(355nm)与调谐的Rh·6G染料激光在β-BaB2O4(BBO)晶体中和频,获得217.3～221.4nm连续调谐输出,和频输出的最大能量为250μJ,转换效率为11%.我们还讨论了获取最大和频输出能量的一些实验条件.     

物理实验"十要十不要"

一要明确实验目的、原理和步骤;不要目的不明,原理不清,做一步想一步。 二要会从多种器材中选用精度要求和量程符合的器材;不要随意选用精度和量程不符合实际要求的仪器。