欧洲鳗鲡血细胞显微和超微结构的观察

欧洲鳗鲡血细胞按形态分为红细胞、嗜中性粒细胞、单核细胞、淋巴细胞和血栓细胞５种,描述了这些细胞的显微和超微结构,为动物学、鳗鲡疾病防治等提供基础资料。     

毫米波调频步进雷达运动补偿方法研究

毫米波调频步进（chirp-step frequency , Chirp-SF）雷达是一种距离高分辨率雷达,但是存在严重的距离 速度耦合问题,所以实现运动目标的距离高分辨必须进行运动补偿。文章提出了一种把脉冲多普勒（Pulse Doppler）测速和基于Chirp-SF信号的时域相关法测速相复合的方法。仿真结果表明该方法测速精度高,算法简单,速度快。     

环(L-苯丙-L-缬)二肽的合成

以L-（＋）-苯丙氨酸甲酯盐酸盐和L-（＋）-缬氨酸为原料,经氨基保护、援基活化等措施合成了新型催化剂环（苯丙-缬）二肽．     

交流调速系统课程理实环节的整体优化研究

介绍我院电气类专业《交流调速系统》课程的现状及存在的问题;介绍了为此进行调研的方法及分析;课程理论与实践环节整合的具体方法及实施效果。     

LC Determination of Ketorolac in Human Plasma and Urine for Application to Pharmacokinetic Studies

A simple, specific and sensitive liquid chromatographic method has been developed for the assay of ketorolac in human plasma and urine. The clean-up of plasma and urine samples were carried out by protein precipitation procedure and liquid–liquid extraction, respectively. Separation was performed by a Waters sunfire C₁₈ reversed-phase column maintained at 35 °C. The mobile phase was a mixture of 0.02 M phosphate buffer (pH adjusted to 4.5 for plasma samples and to 3.5 for urine samples) and acetonitrile (70:30, v/v) at a flow rate of 1.0 mL min^?1. The UV detector was set at 315 nm. Nevirapine was used as an internal standard in the assay of urine sample. The method was validated over the concentration range of 0.05–8 and 0.1–10 μg mL^?1 for ketorolac in human plasma and urine, respectively. The limits of detection were 0.02 and 0.04 μg mL^?1 for plasma and urine estimation at a signal-to-noise ratio of 3. The limits of quantification were 0.05 and 0.1 μg mL^?1 for plasma and urine, respectively. The extraction recoveries were found to be 99.3 ± 4.2 and 80.3 ± 3.7% for plasma and urine, respectively. The intra-day and inter-day standard deviations were less than 0.5. The method indicated good performance in terms of specificity, linearity, detection and quantification limits, precision and accuracy. This assay demonstrated to be applicable for clinical pharmacokinetic studies.     

急性鱼胆中毒并消化道大出血1例报告

介绍１例因生食鱼胆引起急性中毒（胃肠及肝、肾功能损害）并消化道大出血患者的治疗过程。提出,对于急性鱼胆中毒,在治疗急性肾衰护肝的同时,应考虑有可能出现消化道出血。并予以预防。同时应广泛宣传生食鱼胆的危险性。     

福建汉,畲,回族ABO血型分布的研究

本文作者于１９９１～１９９３年间．调查了福建省籍城乡居民汉族１４９８８、畲族６４１人和回族４５９人的ＡＢＯ血型分布。统计分析了三个民族ＡＢＯ血型的民族指数、表现型、基因频率和遗传距离。为我国的血型研究、群体遗传学研究提供基础资料。     

LC Determination of Ketorolac in Human Plasma and Urine for Application to Pharmacokinetic Studies

A simple, specific and sensitive liquid chromatographic method has been developed for the assay of ketorolac in human plasma and urine. The clean-up of plasma and urine samples were carried out by protein precipitation procedure and liquid–liquid extraction, respectively. Separation was performed by a Waters sunfire C₁₈ reversed-phase column maintained at 35 °C. The mobile phase was a mixture of 0.02 M phosphate buffer (pH adjusted to 4.5 for plasma samples and to 3.5 for urine samples) and acetonitrile (70:30, v/v) at a flow rate of 1.0 mL min⁻¹. The UV detector was set at 315 nm. Nevirapine was used as an internal standard in the assay of urine sample. The method was validated over the concentration range of 0.05–8 and 0.1–10 μg mL⁻¹ for ketorolac in human plasma and urine, respectively. The limits of detection were 0.02 and 0.04 μg mL⁻¹ for plasma and urine estimation at a signal-to-noise ratio of 3. The limits of quantification were 0.05 and 0.1 μg mL⁻¹ for plasma and urine, respectively. The extraction recoveries were found to be 99.3 ± 4.2 and 80.3 ± 3.7% for plasma and urine, respectively. The intra-day and inter-day standard deviations were less than 0.5. The method indicated good performance in terms of specificity, linearity, detection and quantification limits, precision and accuracy. This assay demonstrated to be applicable for clinical pharmacokinetic studies.

     

N掺杂碳纳米管环吸附Fe原子的第一性原理研究

采用基于密度泛函理论的CASTEP程序研究N掺杂碳纳米管环结构在变形作用下,外壁对Fe原子的吸附能力.结果表明,构造出的新型纳米结构的结合能为负值,具有稳定存在的可能性;N掺杂碳纳米管环显著提高外壁对Fe原子的吸附能力,这是因为掺杂体系的活度增大,易与Fe原子间形成Fe-N共价结合键.线性增加拉伸和压缩变形幅度,结构外壁对Fe原子的吸附能呈抛物线式快速下降.相比之下,吸附能对拉伸变形更加敏感.