基于偶联反应新极谱法测定痕量亚硝酸根的研究——Ⅱ.以苯酚为偶联试剂

本文研究了苯酚在氨性缓冲溶液中与NO_2~--磺胺重氮盐偶联反应的实验条件,建立了一个灵敏快速测定痕量NO_2~-的新方法。NO_2~-离子浓度在1.0×10~(-10)～4.8×10~(-7)g/ml范围内,与峰高呈良好的线性关系.4000倍量NO_3~-存在不干扰.     

探索学生学习效能的提高--兼数学教学活动

学生学习效能差异很大，这和内外因的各种因素有关，文章着重激发学生学习中的内驱力和教师教学方法等外驱力的作用展开探讨．     

A 2500-year sea level change record in Fildes Peninsula, Antarctica

A detailed record of sea level changes during the last 2500 years is preserved in the northernwest coast of Fildes Peninsula in Antarctica. Fourteen marine alga layers were deposited in the beach with an altitude of 2.80 m, and one diatom layer deposited in the ancient lake on the terrace with an altitude of 6.84 m. A radiocarbon age of 695±70 aBP was obtained for the modern marine alga, and the age was used in correction for the carbon reservoir effect of the marine alga. Sea level fell 4.98 m from the 4th century B.C. to the early 13th century, at an average of -0.31 cm/a, then rose about 0.78 m during the early 13th to the middle 18th century, at an average of 0.14 cm/a. It has risen about 0.16 m since the middle 18th century, at an average of 0.07 cm/a.     

论虚概念

把虚概念理解为“所指称的对象不存在于客观世界的概念”，是不对的，将导致把“理想模型”等本该是实概念的概念纳入其中，也把本该是虚概念的如“地心说”中的概念却排除在外。实际上，对象有虚实，属性也有虚实。实对象、实属性，属于实概念；虚对象、实属性，也属于实概念；实对象、虚属性，属于虚概念；虚对象、虚属性，是虚概念。可见，无论对象虚实，只要所指称的对象的主要特征所反映的属性不是客观的概念就是虚概念。     

拥挤型网络的路流组合及模型求解的搜索法

证明了一个路流组合定理并由此而给出了一个求解网络选址两级模型的算法，讨论了网络的Ｂｒａｅｓｓ性及其在网络规划中的应用前景。     

关于超导机制的一些思考（待续）

对三旋理论应用于超导机制作一些介绍和研究。     

红外光谱法测定乙丙橡胶中丙烯的含量

乙丙胶经热压膜后测定8.65um和13.85um处的吸光度。Ln~(A8.65)/_(A13.85)值与丙烯含量C_3成直线关系,回归方程C_3％=54.43+16.45ln~(A8.65)/_(13.85)。未知样品,A,C,D,F丙烯克分百分数分别为41.0,53.1,40.4和59.7。     

带有不等式约束的全局最优性条件

本文利用不连续罚函数方法将带有不等式约束的全局优化问题的求解转化为 讨论一非线性方程的求根问题,从而得到若干个全局最优性条件.     

民营企业家体育锻炼与生活方式及健康现状的调查分析

对浙江沿海3城市(温州市、宁波市、台州市)208名(25岁～59岁)民营企业家的身体健康状况、体育锻炼情况与生活方式等进行调查,结果表明:浙江沿海3城市民营企业家身体健康状况不容乐观.体质测试总体合格率为65.86%,低于全国的合格率(71.40%)和浙江省的平均水平(79.70%).大多数民营企业家日常生活方式差,参加体育锻炼的人数少.建议民营企业家要养成良好的生活习惯,重视卫生保健知识的自我教育,积极参加体育锻炼.     

Flow-injection spectrophotometric determination of sulfadiazine and sulfamethoxazole in pharmaceuticals and urine.

A rapid and sensitive flow-injection spectrophotometric method is proposed for the determination of sulfadiazine and sulfamethoxazole. This method is based on the diazotization of sulfonamide with sodium nitrite, and a coupling reaction of the diazo-compound with alpha-naphthylamine. The optimum experimental conditions are obtained by using the controlled and weighted centroid simplex method. The linear ranges for the determination of sulfadiazine and sulfamethoxazole are 0.2-20 microg ml(-1) and 0.1-20 microg ml(-1), and their detection limits are 0.06 microg ml(-1) and 0.05 microg ml(-1), respectively, and the sampling frequency is 130 samples per hour. The method has been used to determine sulfadiazine and sulfamethoxazole in pharmaceuticals and urine without separation. The results are in agreement with those obtained by a high-performance liquid chromatograph technique at the 95% confidence level.