Determination of lead by selective chelatometric titration with HEDTA after separation as its sulphate by an improved method of precipitation

A selective titrimetric determination of Pb after separation by a modified method of precipitation as its sulphate is proposed. Pb(II), present as the perchlorate, is precipitated by gentle boiling in 3.6M H(2)SO(4) presaturated with PbSO(4) and free from any extraneous anions. The customary time-consuming evaporation to fumes of sulphuric acid is dispensed with. The precipitate is collected, and dissolved in excess of HEDTA, the surplus of which is back-titrated with Zn(II) at pH 5.0-5.5. Use of Catechol Violet and Xylenol Orange as a mixed indicator gives a sharper end-point. The standard deviation of the proposed method for 60 mg of lead is 0.35 mg. The method has been successfully used to determine Pb in non-ferrous alloys.     

化工过程能量综合知识表示的方法研究

剖析了人类专家进行化工过程能量综合的过程,简述了几种知识表示方法的优、缺点。分析了化工过程能量综合领域知识的种类和特点,提出了题域知识的“面向对象”表示方法。     

贵阳地区蝗虫的危害与防治

论述了贵阳地区（5区1镇）7科17属23种蝗虫的生活习性,危害情况,并提出了防治措施。     

江西大青属药用植物资源及开发利用

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Preparation and optical properties of solid solution semiconductor (Zn x Cd1−x S) doped silica glasses

Semiconductor(Zn_xCd_1−x S) doped silica glasses were prepared by Sol-Gel process andin situ growth technique. The structure of the materials was characterized by X-ray diffraction technique, the particle size of semiconductor crystallites from X-ray patterns was estimated less than 10 nm. From absorption spectra, it is obtained that the absorption edges shifted to short wavelength direction when Zn contents increased, and the absorption edge can be adjusted from 2.46 eV to 2.96 eV by controlling Zn contents. The third-order nonlinear optical susceptibility was studied at 532 nm with 8 ns pulse laser by degenerate four wave mixing (DFWM) technique.     

瓶盖加工模具的失效分析

对瓶盖加工模具在生产使用中突然出现的裂纹及崩刃等现象进行了分析,指出失效的主要原因是原热处理工艺不当使其硬度偏高所致．鉴于此,本文对其进行了实验研究,并制定了新工艺．     

X2105柴油机连杆轴承故障的理论分析和振动实验研究

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甘薯开花规律的观察

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