二茂铁有机锡衍生物的13C,119Sn NMR研究

本文测定了几种二茂铁有机锡衍生物的¹¹⁹Sn,¹³C NMR谱。对其中几种衍生物的¹³C NMR谱进行了归属,从而进一步验证了这类化合物的结构。着重讨论了结构如化合物中取代基X的改变对¹¹⁹Sn化学位移的影响。并对结构如 类化合物N→Sn异侧配位的问题进行了讨论。     

一类多线性振荡奇异积分算子的有界性

考虑了一类多线性振荡奇异积分算子并获得了其在一维Lebesgue空间Lp(R)(1＜p＜∞)的有界性.并通过迭代方法,将这种有界性推广到高维的Lebesgue空间Lp(Rn)(1＜p＜∞)上.     

基于C/S结构的机房管理系统的设计与实现

介绍了机房管理系统的设计方法，给出了工作流程和功能模块以及出入口管理的功能和实现技术．     

电能质量问题及对策

概述了电能质量问题的产生及日益引起关注的原因，介绍了国际电工委员会(IEC)和电气与电子工程师协会(IEEE)对电能质量的定义，并针对电能质量问题提出了具体对策。     

试论黄帝文化的形成

黄帝文化是中华民族的宝贵财富，黄帝时期所创造出来的物质财富和精神文化对后世有重大影响。春秋至战国中期，人们对始祖的尊崇使得黄帝文化得以形成并且发扬光大，而道教的兴起和发展以及对黄帝的神化也推动着黄帝文化的形成。黄帝个人的影响在春秋战国时期达到较高的程度，对于黄帝的认识，在战国时期也非常完备清晰。     

中性磷萃淋树脂吸附铼的性能和机理研究ⅢCL－P＿（350）－KReO＿4－HNO＿3体系

本文报道四甲基膦酸二甲庚酸萃淋树脂（ＣＬ－Ｐ＿（３５０）从硝酸溶液中吸附鳞的性能和机理研究。实验结果表明，吸附平衡服从Ｌａｎｇｍｕｉｒ经验等温式。测得吸附物分子中Ｐ（３５０）与Ｒｅ（Ⅶ）的摩尔比为２：１。Ｒｅ（Ⅶ）是以形式被树脂吸附，其吸附机理属于综合反应：并测定了吸附过程的热力学函数。     

ROOM TEMPERATURE LIGHT-THERMO-DETECTOR MADE OF HIGH-Tc SUPERCONDUCTOR

Based on the anisotropic Seebeck tensor coefficients, a light-thermo-radiation detector made of high-T_c superconductor (YBa₂Cu₃O_7-δ) was fabricated, which can function at room temperature. The induced voltaic signals at various modulation frequencies for radiation from He-Ne laser and from a 500 K black body were measured. The noise ratio for detecting He-Ne laser radiation and the D^* for black body were evaluated. Compared with bolometer made of high-T_c superconductor which functions at liquid nitrogen, and with pyroelectric detector, it was found that the advantages of this new device are that the device can work at room temperature with very low noise and very fast response. Although having a lower D^* value than that of bolometer for the present device construction, we point out the possibility and the direction for improving the D^* value, hence the promising prospect of this kind of device.     

高职院校中技能教学的探讨

本文论述高职教育中的技能训练与科技进步及科研之间的关系。     

泡沫分离,带溶剂萃取和沉淀法提取庆大霉素

研究了用文题法从水相中分离砂大霉素的各种操作因素对分离过程的影响。在最适条件下，种方法对庆大霉素配制液的收率分别为７２％，８８％，８７％，无机盐能使沉淀收率提高。将上述３法用于发酵液时，泡沫法和萃取法的收率均有显著降低，而沉淀法依然能达到很高的收率，ψ＝捍沉淀率约为１００％．     

The honeycomb network structure of poly[[[μ2‐1,3‐bis(1H‐benzimidazol‐2‐yl)benzene‐κ2N3:N3′](μ2‐terephthalato‐κ2O:O′)zinc(II)] ethanol solvate]

The terephthalate dianion and the bis(imidazolyl)benzene ligand of the title compound, {[Zn(C₈H₄O₄)(C₂₀H₁₄N₄)]·C₂H₆O}_n, each bridges two adjacent zinc centers, resulting in a layer‐type coordination polymer; the zinc center shows tetrahedral coordination. The disordered ethanol solvent molecules occupy the spaces between the layers and are hydrogen bonded to the layers. The two symmetry‐independent dianions lie on different inversion sites.