日本菊花螺Siphonaria Japonia化学成分的研究(I)

近年来相继从菊花螺属(Siphonaria)海洋软体动物中分离出一系列聚丙酸酯(Polypropi-onate)类化合物.这类化合物在自然界罕见,被认为是菊花螺属软体动物的典型代谢产物.本文实验所用的菊花螺采自福建省湄洲湾莲城半岛.该动物味很苦,有清凉解毒之功.     

高粘度十二烯基琥珀酸淀粉钠理化性质的研究(Ⅱ)——颗粒形貌和乳化性质

原玉米淀粉经十二烯基琥珀酸酐（DDSA）酯化后，颗粒形貌发生变化。经研究认为：化学反应首先发生在淀粉颗凿表面的无定形区；酯化后淀粉的乳化能力明显增强，不同取代度产品的亲水亲油平衡（HLB）值均大于10，表明它为亲水型乳化稳定剂。     

技术视野下的人与自然关系

为构建人与自然的和谐相处,现代技术的“双刃剑”效应需要人们理性的思考和认真的对待。本文从马克思主义哲学的角度阐述了技术不同于科学的内涵、负面效应及人的责任;从分析技术悲观主义、技术乐观主义与技术现实主义的基础上审视技术价值观的选择,实施可持续发展的生态文明模式;并要求在意识、科教、法律与道德和国际合作等方面采取措施,促进人与自然关系的和谐发展。     

Damage and fracture evaluation of granular composite materials by digital image correlation method

This paper presents the applications of digital image correlation technique to the mesoscopic damage and fracture study of some granular based composite materials including steelfiber reinforced concrete, sandstone and crystal-polymer composite. The deformation fields of the composite materials resulted from stress localization were obtained by the correlation computation of the surface images with loading steps and thus the related damage prediction and fracture parameters were evaluated. The correlation searching could be performed either directly based on the gray levels of the digital images or from the wavelet transform (WT) coefficients of the transform spectrum. The latter was developed by the authors and showed higher resolution and sensitivity to the singularity detection. Because the displacement components came from the rough surfaces of the composite materials without any coats of gratings or fringes of optical interferometry, both surface profiles and the deformation fields of the composites were visualized which was helpful to compare each other to analyze the damage of those heterogeneous materials. The project supported by the National Natural Science Foundation of China (10125211 and 10072002), the Scientific Committee of Yunnan Province for the Program of Steel Fiber Reinforced Concrete, and the Institute of Chemical Materials, CAEP at Mianyang     

自然数同次幂级数求和的方法

本文利用微积分方法，推导出自然数同政幂级数的求和公式。     

带观测器的电液力伺服变极点数控系统的设计

本文在阐述变极点最优控制原理及其在电液力伺服系统中的实施之基础上，又进行了变极点控制的离散化处理和离散降维观测器对系统的状态重构，解决了系统稳定性与响应速度的矛盾，为该系统微机控制软、硬件的实观奠定了理论基础     

半参数模型约束条件下估计量的统计诊断

利用最小惩罚二乘原理构造加权惩罚平方和，导出了约束条件下，半参数模型中正规化矩阵正定时半参数平差的计算方法，用直接法得到了参数和半参数的估计量，并将此方法引入测绘领域，给出了相应的公式。     

氨基膦酸羧酸螯合树脂的合成及其对痕量镧系稀土富集分离性能的研究

简要叙述了氨基膦酸羧酸树脂的合成路线 ,用 ICP- AES对其富集分离痕量镧系稀土元素进行了研究 ,讨论了吸附酸度、洗脱、吸附流速以及共存离子干扰等的影响 ,并进行了实际样品的分析 ,获得了满意的结果 .     

Isolation and Structure Elucidation of Nortriterpenoids from Schisandra rubriflora

Seven new highly oxygenated nortriterpenoids, rubriflorins D–J ( 1 – 7 ), were isolated from the leaves and stems of Schisandra rubriflora, and their structures were elucidated on the basis of extensive analysis of spectroscopic data. These new compounds feature the opening of ring A compared with related known nortriterpenoids isolated from the genus Schisandra and showed weak activity against HIV‐1.     

Studies on the chemical constituents of the South China Sea sponge Phacellia fusca

Three pyrrololactam alkaloids have been isolated from the marine sponge Phacellia fusca Schmidt collected from the South China Sea, and their structures were determined as 1–3 , on the grounds of spectral data. This is the first report of these compounds from this sponge. The structure of 1 was confirmed by X-ray analysis.