氟硅烷自组装单分子膜的制备及其摩擦学性能

利用分子自组装技术制备了全氟辛酰胺丙基硅烷单分子膜,用X射线光电子能谱(XPS)对组装膜的表面元素进行了表征;接触角测试表明,该组装膜具有很好的疏水-疏油性,其对水的接触角高达105°,对正十六烷的接触角为50°.摩擦磨损实验结果表明,全氟辛酰胺丙基硅烷自组装单分子膜可以大大降低基片的摩擦系数,使载玻片的摩擦系数从0.85左右降低到0.14左右,而且低负荷下具有很好的耐磨性.     

Synthesis of triphenylene derivatives by Pd-catalyzed Suzuki coupling/intramolecular CH activation between arylboronic acids and dibromobiphenyls

An efficient and regioselective synthesis of functionalized triphenylenes via palladium-catalyzed Suzuki-Miyaura coupling and subsequent intramolecular CH activation between arylboronic acids and dibromobiphenyls was developed. This methodology showed excellent atomic economy and regiospecificity as well as synthetic feasibility of unsymmetrical triphenylenes.     

Reactive dications: the superacid-catalyzed reactions of alkynes bearing adjacent N-heterocycles or amine groups

A variety of aminoalkynes and related heterocycles are reacted in the Bronsted superacid CF(3)SO(3)H (triflic acid), and products are obtained in generally good yields (69-99%) from Friedel-Crafts-type reactions. The reactions are consistent with the formation of novel dicationic intermediates having a vinyl cationic site and an adjacent protonated N-heterocycle or ammonium cation.     

基于生成对抗网络的渐进式夜视图像彩色化算法

受限于夜景光照不足等影响,夜视成像中的部分内容极易缺失或模糊,导致这部分的彩色化效果不佳.为此,本文提出了一种基于生成对抗网络的夜视图像彩色化算法, 通过对纹理细节的修复来提升图像模糊区域的彩色化效果.首先,在模糊区域修复中,利用下采样操作减少模糊图像块的比例,并用梯度调节预测器对模糊图像块周围的像素值进行预测,以此来不断增强和修复模糊的纹理细节.其次,在彩色化过程中,依托于生成的超分辨率图像和已有的先进对抗网络着色模型,通过最小化亮度和纹理等失真,来生成较为清晰的彩色图像.实验结果表明,经过模糊区域恢复和增强之后,灰度图像的PSNR平均提升0.33 dB.相比之前的夜视图像彩色化方法,本文方法可以赋予灰度夜视图像更丰富、自然的色调,更清楚地表达图像的细节,从而提高目标探测和识别效率.     

A Perturbation Approach to Vector Optimization Problems: Lagrange and Fenchel–Lagrange Duality

Journal of Optimization Theory and Applications - In this paper, we study a general minimization vector problem which is expressed in terms of a perturbation mapping defined on a product of locally...     

Hardy Spaces on the Plane and Double Fourier Transforms

We provide a direct computational proof of the known inclusion where is the product Hardy space defined for example by R. Fefferman and is the classical Hardy space used, for example, by E.M. Stein. We introduce a third space of Hardy type and analyze the interrelations among these spaces. We give simple sufficient conditions for a given function of two variables to be the double Fourier transform of a function in and respectively. In particular, we obtain a broad class of multipliers on and respectively. We also present analogous sufficient conditions in the case of double trigonometric series and, as a by-product, obtain new multipliers on and respectively.     

对“有机化合物命名”中存在问题的商榷

按照《有机化学命名原则》（１９８０）,对目前高校有机化学教材中化合物命名中存在的问题进行了讨论。     

Optimal linear estimators of the unknown mean of a random field observed on a cross

Explicit formulas of minimum-variance linear unbiased estimators of the unknown mean are derived for homogeneous random fields with correlation functions observed on the set (a cross).Translated from Vychislitel'naya i Prikladnaya Matematika, No. 64, pp. 116–121, 1988.     

A sequential multielement separation scheme for determination of As,Mn, Mo,Cu and Zn in human milk by neutron activation analysis

A simple separation scheme for the analysis of As, Mn, Mo, Cu and Zn using neutron activation is described. It has been checked using three standard reference materials, A-11 milk powder (IAEA) and bovine liver and orchard leaves (USNBS) and found to give acceptable results. This scheme was applied for determination of these trace elements in mature human milk samples. The concentrations of As, Mn, Mo, Cu in samples obtained from two socio-economic groups—low and middle incomes—were not significantly different. However, Zn levels in samples obtained from the poor income group were significantly lower than in those obtained from the other group. Work carried out under Research Contract No. 2598/RB of International Atomic Energy, Vienna. Health Physics Division. Analytical Chemistry Division.