新型全固态铁离子敏感电极研究

采用稀土电极材料六硼化镧制备了一种新的全固态铁离子敏感电极。研究了该敏感电极在常见介质中对Ｆｅ３＋的响应行为。结果表明，该铁离子敏感电极在１．５ｍｏｌ／ＬＨ３ＰＯ４介质中的线性响应范围、检测下限和响应斜率分别为１．０×１０－５～１．０×１０－１ｍｏｌ／ＬＦｅ３＋，６．０×１０－６ｍｏｌ／ＬＦｅ３＋和６０ｍＶ／ｐＣ，且具有较好的选择性。     

独立不同分布随机变盆序列的部分和的增量有多小

关于独立同分布随机变量部分和的增量有多小问题，目前已有了著名的结果.本文通过与独立同分布情形时完全不同的途径，讨论了独立不同分布情形时相应的问题.在矩母函数存在的条件下，获得了与同分布情形相近的结论.     

界面反射偏振象差分析

在光学没计中,一般认为在同一光波面上,光束具有相同的振幅和偏振状态。事实上,光束经过许多光学元件后,偏振状态会发生变化,特别是入射角和光程的不同,会导致出射光波面上偏振分布不再均匀,形成偏振象差。本文主要就轴上物点发出的光束经过界面反射后的偏振象差方面进行了分析。     

彩电中I2C总线系统调整

介绍了彩电中 I2 C总线系统的控制和调整原理 ,以及实例机型的调整方法 .     

三峡二期围堰工程几个问题的研究及实践

三峡工程二期围堰是三峡工程最重要的临时建筑物之一，大江截流水深大，流量大；防渗墙深度大，工程量大，工期紧，且还要穿过各种复杂地层，通过试验，研究，采取有效地对策确保大江安全，顺利截流，基坑按三峡总工期目标要求抽干，检查渗漏量仅为设计估计量的1／10。     

轻质页岩脱色性能的研究

本文研究了轻质页岩的脱色性能，其最佳活化温度为６００～７００℃。最佳活化时间为０．５ｈ，并获得了有意义的结论。     

关于毛泽东的反对错误倾向的分析与思考

毛泽东关于反对错误倾向的思想是非常深刻、非常系统的。完全可以说,毛泽东关于反对错误倾向的思想是一整套严密的理论。我们应该学习和继承这一理论。但在反对错误倾向的问题上,毛泽东有沉重的经验教训值得我们记取。     

Two differential equation systems for equality-constrained optimization

This paper presents two differential systems, involving first and second order derivatives of problem functions, respectively, for solving equality-constrained optimization problems. Local minimizers to the optimization problems are proved to be asymptotically stable equilibrium points of the two differential systems. First, the Euler discrete schemes with constant stepsizes for the two differential systems are presented and their convergence theorems are demonstrated. Second, we construct algorithms in which directions are computed by these two systems and the stepsizes are generated by Armijo line search to solve the original equality-constrained optimization problem. The constructed algorithms and the Runge–Kutta method are employed to solve the Euler discrete schemes and the differential equation systems, respectively. We prove that the discrete scheme based on the differential equation system with the second order information has the locally quadratic convergence rate under the local Lipschitz condition. The numerical results given here show that Runge–Kutta method has better stability and higher precision and the numerical method based on the differential equation system with the second information is faster than the other one.     

局部对称共形平坦黎曼流形中的极小子流形

对局部对称共形平坦黎曼流形中具有平坦法丛的极小子流形作了一些讨论，得到了极小子流形是全测地的两个充分条件。     

2‐Cyanoprop‐2‐yl dithiobenzoate mediated reversible addition–fragmentation chain transfer polymerization of acrylonitrile targeting a polymer with a higher molecular weight

The reversible addition–fragmentation chain transfer (RAFT) polymerization of acrylonitrile (AN) mediated by 2‐cyanoprop‐2‐yl dithiobenzoate was first applied to synthesize polyacrylonitrile (PAN) with a high molecular weight up to 32,800 and a polydispersity index as low as 1.29. The key to success was ascribed to the optimization of the experimental conditions to increase the fragmentation reaction efficiency of the intermediate radical. In accordance with the atom transfer radical polymerization of AN, ethylene carbonate was also a better solvent candidate for providing higher controlled/living RAFT polymerization behaviors than dimethylformamide and dimethyl sulfoxide. The various experimental parameters, including the temperature, the molar ratio of dithiobenzoate to the initiator, the molar ratio of the monomer to dithiobenzoate, the monomer concentration, and the addition of the comonomer, were varied to improve the control of the molecular weight and polydispersity index. The molecular weights of PANs were validated by gel permeation chromatography along with a universal calibration procedure and intrinsic viscosity measurements. ¹H NMR analysis confirmed the high chain‐end functionality of the resultant polymers. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 1272–1281, 2007