牛血清白蛋白在NVP/HEMA无规共聚物水凝胶上的吸附研究

合成了不同含水量的N-乙烯吡咯烷酮(NVP)／甲基丙烯酸-β-羟乙酯(HEMA)共聚物水凝胶．研究了温度、pH值，蛋白质初浓度及离子强度等因素对牛血清白蛋白吸附性能的影响．采用紫外分光光度法测定BSA的吸附量．结果表明，蛋白质初浓度越高．温度越高，离子强度越大；蛋白质内部更多的疏水性氧基酸残基暴露于外部．吸附量增加：在等电点pH=4．7附近蛋白质沉积量最大．     

Determination of lead by selective chelatometric titration with HEDTA after separation as its sulphate by an improved method of precipitation

A selective titrimetric determination of Pb after separation by a modified method of precipitation as its sulphate is proposed. Pb(II), present as the perchlorate, is precipitated by gentle boiling in 3.6M H(2)SO(4) presaturated with PbSO(4) and free from any extraneous anions. The customary time-consuming evaporation to fumes of sulphuric acid is dispensed with. The precipitate is collected, and dissolved in excess of HEDTA, the surplus of which is back-titrated with Zn(II) at pH 5.0-5.5. Use of Catechol Violet and Xylenol Orange as a mixed indicator gives a sharper end-point. The standard deviation of the proposed method for 60 mg of lead is 0.35 mg. The method has been successfully used to determine Pb in non-ferrous alloys.     

后交联型St-DVB大孔吸附树脂对低级醇类的吸附性能研究

分别在静态和动态条件下研究了Friedel—Crafs后交联型聚苯乙烯-二乙烯基苯(St-DVB)大孔吸附树脂对水溶液中多种低级一元醇的吸附性能，测定静态吸附等温线和动态吸附曲线，并分别按照Langmuir和Freundlich模型进行拟合．结果显示，树脂对水中低浓度低级一元醇的吸附过程属于放热的物理吸附过程，树脂吸附能力随着一元醇碳原子数的增加，即分子内疏水基团质量的增加而增加；树脂对直链醇的吸附能力稍强于同分异构的支链醇．     

变压器绕组短路故障多特征融合诊断

绕组匝间短路是变压器最常见的初期故障类型之一.为了提高轻度故障的诊断准确率,考虑绕组短路电流、绕组温度、电流密度和磁通偏移特征,提出了变压器绕组短路故障的多特征融合诊断方法.首先建立了变压器绕组短路的COMSOL空间模型,将仿真结果和理论计算结果进行对比,证明空间模型的正确性.然后,对变压器轻度故障时进行了故障模拟和故障特征分析,提取其电流特征参量、温度特征参量、电流密度偏移率和磁通偏移率作为故障特征.采用BP网络进行故障识别.变压器的工程诊断实例验证了本文方法的有效性.     

化工过程能量综合知识表示的方法研究

剖析了人类专家进行化工过程能量综合的过程,简述了几种知识表示方法的优、缺点。分析了化工过程能量综合领域知识的种类和特点,提出了题域知识的“面向对象”表示方法。     

贵阳地区蝗虫的危害与防治

论述了贵阳地区（5区1镇）7科17属23种蝗虫的生活习性,危害情况,并提出了防治措施。     

江西大青属药用植物资源及开发利用

介绍了江西大青属（赤贞桐属）（ＣｌｅｒｏｄｅｎｄｒｕｍＬ．）药用植物种类、地理分布以及临床疗效等,同时对该属药用植物种类进行了本草考证,对该属资源的合理开发利用提出了建议。     

Preparation and optical properties of solid solution semiconductor (Zn x Cd1−x S) doped silica glasses

Semiconductor(Zn_xCd_1−x S) doped silica glasses were prepared by Sol-Gel process andin situ growth technique. The structure of the materials was characterized by X-ray diffraction technique, the particle size of semiconductor crystallites from X-ray patterns was estimated less than 10 nm. From absorption spectra, it is obtained that the absorption edges shifted to short wavelength direction when Zn contents increased, and the absorption edge can be adjusted from 2.46 eV to 2.96 eV by controlling Zn contents. The third-order nonlinear optical susceptibility was studied at 532 nm with 8 ns pulse laser by degenerate four wave mixing (DFWM) technique.