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961.
Xian Tao Ke‐Cheng Shen Qing‐Yun Tang Meng Feng Jiang‐Tao Fang Yu‐Long Wang Ying‐Zhong Shen 《应用有机金属化学》2012,26(7):323-329
New N‐silver(I) acetylbenzamide complexes of type Ln?AgNC9H8O2 (L = PPh3; n = 1, 2a; n = 2, 2b; n = 3, 2c; L = P(OEt)3; n = 1, 2d; n = 2, 2e; n = 3, 2f) were prepared. These complexes were obtained in high yields and characterized by elemental analysis, 1H NMR, 13C{H} NMR, 31P{H} NMR and IR spectroscopy, respectively. The molecular structure of 2b has been determined by X‐ray single‐crystal analysis in which the silver atom is in a distorted tetrahedral geometry and crystallizes as cis–trans. New N‐silver(I) acetylbenzamide complexes have a four‐membered ring, which could influence their chemical and physical properties and modulate volatility. Metal organic chemical vapor deposition experiments were carried out successfully at 400°C and 450°C using 2e as precursor for the deposition of silver films, respectively. The high‐purity silver film obtained at 400°C is dense and homogeneous. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
962.
963.
Adhesive force between two solid surfaces can lead to stiction failure of the micro-electro-mechanical systems (MEMS) device. The competition between the adhesive force and the beam restoring force determines whether the stiction occurs or not. Previous models assume that the stuck beam deforms either as the arc-shape or the S-shape, which causes significant differences in the measurements of adhesion and disputations among researchers. The contact mechanics model presented in this paper shows that the assumptions of the arc-shape and S-shape on the beam deformation over-simplify the problem; both the arc-shaped deformation and S-shaped deformation significantly deviate from the real ones. The previous theories are shown to be incompatible with the recent experimental results. The model presented in this paper attempts to explain those new experimental results and resolve some disputations on the previous models. The instabilities of jump-in during loading process and jump-off during unloading process are also incorporated in this model. 相似文献
964.
Yue Shao Hong-Ping Zhao Xi-Qiao Feng Huajian Gao 《Journal of the mechanics and physics of solids》2012,60(8):1400-1419
Studying the structure–property relation of biological materials can not only provide insight into the physical mechanisms underlying their superior properties and functions but also benefit the design and fabrication of advanced biomimetic materials. In this paper, we present a microstructure-based fracture mechanics model to investigate the toughening effect due to the crack-bridging mechanism of platelets. Our theoretical analysis demonstrates the crucial contribution of this mechanism to the high toughness of nacre. It is found that the fracture toughness of nacre exhibits distinct dependence on the sizes of platelets, and the optimized ranges for the thickness and length of platelets required to achieve higher fracture toughness are given. In addition, the effects of such factors as the mechanical properties of the organic phase (or interfaces), the effective elastic modulus of nacre, and the stacking pattern of platelets are also examined. Finally, some guidelines for the biomimetic design of novel materials are proposed based on our theoretical analysis. 相似文献
965.
选区激光熔化(selective laser melting, SLM)技术具有一体化快速制备复杂和高精度零件的能力,在航空航天等工业生产中有巨大的发展潜力。高强铝合金是近年来在增材制造领域发展迅速,可实现结构轻量化的重要材料,其中Al-Mg-Sc系高强铝合金在结构和性能方面具有极大的潜力。针对增材制造领域Al-Mg-Sc系高强铝合金的应用与发展,结合增材制造工艺技术,从增材制造高强铝合金合金成分、微观组织和力学性能三个方面,全面总结了增材制造Al-Mg-Sc系高强铝合金的研究现状和进展趋势。在增材制造高强Al-Mg-Sc合金领域内,应当重点关注强化元素的多元化、SLM成形合金微观组织调控以及性能特征的多元化研究等方向。 相似文献
966.
Zhou Xingyu Zhang Jiang Liu Yang Xie Yanqing Zhang Ran Zhao Yang He Zhongxiong 《中国工程科学》2004,2(2):88-89
Based on the intelligent decision support system, a new method was presented to defense the catastrophic infectious disease such as SARS, Bird Flu, etc.. By using All Set theory, the decision support system (DSS) model can be built to analyze the noise information and forecast the trend of the catastrophe then to give the method or policy to defend the disease. The model system is composed of four subsystems: the noise analysis subsystem, forecast and simulation subsystem, diagnosis subsystem and second recovery subsystem. They are discussed briefly in this paper. This model can be used not only for SARS but also for other paroxysmal accidences. 相似文献
967.
从结构形式、热处理、材质选择等方面对新型管式浆膜蒸发器运行中出现的引起板片爆裂、泄露进行了研究分析;并就新型板片设计、制造、试验做出探索。 相似文献
968.
969.
970.
利用了GPRS无线通信网络和Internet网络结合,构成路灯远程监控系统,其中GPRS网络主要完成路灯监控系统的控制端主机的数据采集任务,Internet网络主要实现路灯监控系统的主控制器的数据传输任务.两种网络进行结合的方式,能达到远距离数据传输稳定可靠的优点,对于路灯远程监控系统是很好的尝试. 相似文献