临近铁路深基坑开挖防护技术

考虑到周边建筑物安全及在动荷载下施工人员和机械设备的安全,选择了防护桩方案并进行了设计及计算,为临近铁路深基坑施工提供了参考。     

Samples Selection for Artificial Neural Network Training in Preliminary Structural Design

An artificial neural network (ANN) is applied in the preliminary structural design of reticulated shells. Major efforts are made to enhance the generalization ability of networks through well-selected training samples. Number-theoretic methods (NTMs) are adopted to generate samples with low discrepancy, i.e.uniformly scattered in the domain, where discrepancy is a quantitative measurement of the uniformity. The discrepancy of the NTM-based sample set is 1/6-1/7 that of samples with equal spacing. In a case study,networks trained by NTM-based samples are compared with those trained by equal-spaced samples in generalizing performance. The results show that both the computational precision and stability of the former ANNs are more satisfactory than those of the latter. It is concluded that the flexibility of ANNs in generalizing can be effectively increased by use of uniformly distributed training samples rather than simply piling data.More reliable uniformity should be obtained, however, through NTMs instead of equal-spaced samples.     

鲁北地区商周时期的海盐业

采用XRD和XRF分析测试方法，研究了山东省渤海湾地区滨州市阳信县李屋遗址和寿光市大荒北央遗址出土的商代晚期的陶器——盔形器及附着土壤．样品的Na元素和Cl元素XRF分析结果表明：李屋遗址和大荒北央遗址出土的盔形器的含盐量明显高于其他样品，显示这二地的盔形器与早期海盐生产有关．李屋遗址出土的盔形器表面附着土样用去离子水过滤后，滤液结晶体的XRD分析结果，进一步表明该盔形器是商周时期渤海湾地区海盐生产的器物．大荒北央遗址出土的盔形器的内壁沉淀物与长江三峡中坝遗址出土的花边陶釜的内壁沉淀物具有基本相同的物相，这进一步表明其与海盐生产有关．     

SACD中的DSD技术和数据无损压缩算法

SACD是对现有CD的改进，它利用直接数字流（DSD）技术，和DST无损压缩方法，对数据进行存储。它可以存储2声道或6声道的声音数据。由于采用了全新的技术来记录声音，使它可以产生更好的声音质量，必将成为新一代的声音记录格式。本文详细介绍了1比特DSD编码技术的原理，和DST无损压缩方法的原理。     

对新疆群众体育场地设施投资现状的探讨

文章从经济学的角度出发,分别从投资政策、资金来源、运营性质和影响群众体育场地设施投资的客观因素对新疆目前群众体育场地设施的投资状况进行分析,指出阻碍新疆群众体育场地设施投资的关键所在.从理论和实践上解释体育场地设施投资缺乏的原因,力求为群众体育场地设施的投资工作提供可靠依据.     

PHASE INVERSION AND ITS MECHANICAL MODEL STUDIES FOR THE TWO-PHASE POLYMER BLEND SYSTEMS (Ⅱ)——DYNAMIC VISCOELASTIC RESPONSE

The dynamic viscoelastic response of the two-phase polymer blend systems shows the characteristics of the thermorheologically complex materials. In this paper theoretical equations for describing the dynamic viscoelastic response of such polymer blend systems have been established by means of the mechanical modeling technique. The dynamic viscoelastic response of the blend systems at any blend composition can be predicted theoretically by using the equations established, provided that the dynamic viscoelastic response of the two pure components and the mechanical model parameters are known in advance. Thus, we provide an effective method for studying the dynamic mechanical properties and the molecular relaxation characteristics of the two-phase polymer blend systems.     

毛细管离子分析法测定人发中钙和锌

适量人发试样经洗涤、冲洗,并于60℃干燥至恒重后称取1.000 g于600℃灰化后用盐酸(1+1)溶解残渣,溶液定容为100 mL供CIA分析。在10 mmol.L-1咪唑、10 mmol.L-1α-羟基乙酸、pH 4.0的电泳介质中,两离子在10 min内实现了分离。以间接紫外法检测(214 nm),外标法定量。钙(Ⅱ)及锌(Ⅱ)的峰面积与其质量浓度之间在0.5~40 mg.L-1范围内呈线性关系,相关系数分别为0.999 1和0.998 9,检出限(S/N=3)为0.1和0.2 mg.L-1,回收率在97.9%~102.5%之间,相对标准偏差小于2.5%。     

新型萃取剂杯[4]冠－6的合成与表征

研究了新型萃取剂1，3－交替构象的二烷氧基杯[4]冠－6化合物系列的合成方 法，对合成的中间体和目标产物进行了详细表征。合成的化合物对铯离子有较高的 选择性。     

新型氮芥和卤代烷基哌嗪芳香醛的合成

通过对Vilsmeier反应、烷基化反应和氯化反应的改进提出了以简单易得的苯胺和苯基哌嗪为原料制备氮芥和哌嗪芳香醛的方法. 采用该改进的方法合成了8个氮芥和哌嗪芳香醛, 其中7个为新化合物. 它们的结构均经质谱、红外光谱、核磁共振谱和元素分析确证.     

磷钼酸铵-孔雀绿-PVA分光光度法测定钽粉中磷

提出了以磷钼酸铵-孔雀绿-PVA三元络合物体系测定金属钽粉中磷的方法,该体系表观摩尔吸光系数ε=8.19×104L.mol-1.cm-1,加标回收率为:99.3%~105%,方法的RSD为:5.9%。有效地解决了目前高纯钽粉中磷的分析难题,方法已应用于实际产品的分析中。