SURFACE METALLIZATION OF CENOSPHERES AND PRECIPITATORS BY ELECTROLESS PLATING

This paper reports the use of a colloidal Pd^0 catalysis system to metallize the surface of precipitators separated from coal fly-ash, and metals such as Cu, Ni etc. are deposited on the precipitators surface. Alternatively, according to the characteristic surface of cenospheres, an Ag coating catalysis system is adopted to first deposit Ag on the cenospheres surface, followed, if necessary, by the deposition of other metals such as Cu, Ni, etc. on the Ag coating to produce monolayer and multilayer metal-coated cenospheres. The surface characteristics and the morphologies of the metal coatings are examined in detail with scanning electron microscopy (SEM), energy dispersive spectroscopy (EDX) and X-ray photoelectron spectroscopy (XPS) techniques. It can be shown that the quality of metal coatings derived from the Aa coatina catalysis system, is better than that of the colloidal Pd^0 catalysis system.     

超短脉冲激光微束对细胞作用的研究

本文详细地介绍了我们自己设计和安装的一个Nd:YAG超短脉冲激光微束系统,该系统分成二个部分:激光源和显微镜。由电光调Q非稳腔Nd:YAG激光倍频后得到355nm紫外光进入显微镜并由物镜聚焦。同时,这超短脉冲激光微束照射在细胞上并且在细胞上产生一个可以自恢复的小孔。在文中我们还讨论了超短脉冲激光微束与细胞之间作用效应及机理。     

Angular momentum effect in prescission particle multiplicities for a light system by diffusion model

The effect of angular momentum on the competition between fission and particle emission during light system fission process was studied via fission diffusion model. The prescission particle multiplicities were found to increase with decreasing angular momentum. The experimental prescission proton and α particle multiplicities can be fitted for 10.6 MeV/nucleon ⁸⁴Kr(²⁷Al,binary fission) reaction with this model. Entrance channel effect found in [1] is proved to be angular momentum effect.     

X-ray evidence for the absence of 90°-domains in polycrystalline PbTiO3 thin films with grains below a critical size

3 thin films is systematically studied by using X-ray diffraction (XRD). The PbTiO₃ thin films with different average grain sizes were prepared on various substrates by a sol-gel process. The films on NaCl and fused glass are randomly grain-oriented, while those on (111)Pt/Ti/SiO₂/Si are highly {100} cubic index grain-oriented . It is found from the XRD patterns of the films on NaCl that with decreasing average grain size from 230 to 80 nm, the intensities of high h index (h>l) peaks (hkl), such as (100), (110), (200), (201), (210), (211), etc., decrease rapidly and ultimately disappear, whereas another set of peaks (lkh), including (001), (002), (102), (112), etc., are still intense. This interesting result suggests that at grain size below a certain critical size an increasing number of grains no longer show 90°-domains, which is confirmed by TEM observations. Meanwhile, X-ray evidence of such a grain-size-related absence of 90°-domains is also found for PbTiO₃ films on Pt(111) and fused-glass substrates. The volume fractions of single-domain grains (without 90°-domains) in the films are estimated from their XRD patterns. By combining SEM and TEM investigations, the critical grain size for the formation of 90°-domains is further determined to be near 200 nm. Received: 19 December 1996/Accepted: 24 March 1997     

压水堆控制棒导向筒结构改进对落棒的影响

为改善横向水力载荷对控制棒导向筒的作用，对靠近上腔室出口管嘴附近的控制棒导向筒（对称的４组：０２－２６，０３－２５，１１－２９，１２－２８）加设了保护套．在秦山核电站压水堆上腔室１４的可视化模拟体中，以水为介质进行了实验研究，把结果与未加设保护套的实验结果作了分析比较，得到了对靠近上腔室出口管嘴附近的控制棒导向筒加设保护套有助于改善流场对控制棒导向筒的水力载荷作用和确保控制棒能按指令在导向筒中自由升降和快速下插的结论．     

θ*r,s,t-图与唯一2-列表染色图的特征化

如果一个图G存在一个k-列表安排使得G具有一个唯一列表染色,则称 G是唯一列表可染色图,简称UkLC图．我们称图G具有M(k)性质当且仅当G不 是UkLC图．本文在借鉴θr,s,t-图概念的基础上引入θr,s,t-图的定义,并证明:除了 r=s=t=2以外,θr,s,t-图都是U2LC图．利用如上结果我们给出M．Mahdian and E．S．Mahmoodian对U2LC图所作特征化的一个简单证明．     

Template atom transfer radical polymerization of a diaminopyrimidine‐derivatized monomer in the presence of a uracil‐containing polymer

Uracil‐derivatized monomer 6‐undecyl‐1‐(4‐vinylbenzyl)uracil and diaminopyrimidine‐derivatized monomer 2,6‐dioctanoylamido‐4‐methacryloyloxypyrimidine (DMP) were synthesized and polymerized by atom transfer radical polymerization (ATRP). A well‐defined, highly soluble, uracil‐containing polymer, poly[6‐undecyl‐1‐(4‐vinylbenzyl)uracil] (PUVU), was prepared in dioxane at 90 °C with CuBr/1,1,4,7,10,10‐hexamethyltriethylenetetramine as the catalyst and methyl α‐bromophenylacetate as the initiator. PUVU was further used as a template for the ATRP of DMP. The enhanced apparent rate constant of the DMP polymerization in the presence of PUVU indicated that the ATRP of DMP occurred along the PUVU template. The template polymerization produced a stable and insoluble macromolecular complex, PUVU/poly(2,6‐dioctanoylamido‐4‐methacryloyloxypyrimidine). An X‐ray diffraction study confirmed that the complex had strandlike domains. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 6607–6615, 2006     

双折射双频激光器偏振特性的分析

用激光原理和晶体光学原理分析了腔内加旋光晶体的激光器输出光的偏振特性，实验和分析表明，激光器输出两束不同频率的垂直线偏振光，激光器两端输出光的偏振面有一夹角ａ，且此夹角与晶轴和传光方向的夹角θ有关。理论计算结果在双折射双频激光器的实验结果符合很好。     

800nm激光泵浦掺Nd^3＋的氟化物玻璃光纤正向双程超荧光分析

从实验上探讨了掺Ｎｄ＾３＋的氟化物玻璃光纤正向双程超荧光基本特性，包括输入－输出特性、输出－带宽特性以及输出－波长（激发）特性。并给出了理论上的拟合公式，实验表明利用氟化物玻璃光纤有望获得性能优异的有应用前景的低相干度集成化光源。     

锻炼对老年人肺通气功能影响的研究

本文采用电子肺活量计对218名老人进行了肺通气功能的测试。测试结果表明:体育锻炼对老年人肺通气功能有良好影响。本文为老年人肺通气功能的研究、评价及老年人体育运动的研究提供了实验性依据。