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951.
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954.
以碳酸钾为催化剂分别将1(4),8(11),15(18),22(25)-四(4-羧基苯氧基)酞菁锌(1)和卜(4-羧基苯氧基)酞菁锌(2)与溴代乙酰糖基(乳糖、麦芽糖和葡萄糖)偶联,得到5种糖基酞菁偶联衍生物,IR,MS和UV—Vis光谱证实羧基酞菁与糖基成功偶联.糖基过量时,由1主要获得糖基二取代产物.溶解性和稳定性研究表明:5种偶联衍生物易溶或可溶于DMF、丙酮、THF、氯仿和甲醇中,不溶于水,它们在DMF中避光均能稳定存在.在DMF、丙酮、THF、甲醇和氯仿中它们显示相似的酞菁单体的电子吸收光谱,在体积分数O.1%DMF的水中出现聚集,这些体系中的Q带特征吸收峰位于670~690nm;在DMF和含O.1%DMF的水中的荧光量子产率分别为0.358-0.721与0.121~O.198,为原酞菁(1和2)的2~3倍和3~5倍. 相似文献
955.
Lijing Shao 《Physica A》2010,389(16):3109-3116
The occurrence of the nonzero leftmost digit, i.e., 1,2,…,9, of numbers from many real world sources is not uniformly distributed as one might naively expect, but instead, the nature favors smaller ones according to a logarithmic distribution, named Benford’s law. We investigate three kinds of widely used physical statistics, i.e., the Boltzmann-Gibbs (BG) distribution, the Fermi-Dirac (FD) distribution, and the Bose-Einstein (BE) distribution, and find that the BG and FD distributions both fluctuate slightly in a periodic manner around Benford’s distribution with respect to the temperature of the system, while the BE distribution conforms to it exactly whatever the temperature is. Thus Benford’s law seems to present a general pattern for physical statistics and might be even more fundamental and profound in nature. Furthermore, various elegant properties of Benford’s law, especially the mantissa distribution of data sets, are discussed. 相似文献
956.
Zhi-Hai Zhang Kang-Xian GuoBin Chen Rui-Zhen WangMin-Wu Kang Shuai Shao 《Superlattices and Microstructures》2010
The optical absorption coefficients and the changes in the refractive index in GaAs/AlGaAs parabolic quantum dots(QDs) with applied electric and magnetic fields are studied in detail. Analytical expressions for the linear and nonlinear intersubband absorption coefficients and refractive index changes are obtained by using a compact density matrix approach and an iterative procedure. Finally, the calculated results show the incident optical intensity, the frequencies of the confined potential of the QDs and the applied electric and magnetic fields have a great influence on the optical absorption coefficients and refractive index changes in this system. 相似文献
957.
Lei Shi Hui Zhang Yan-Feng Meng Jin-Sheng Su Guo-Liang Shao 《Applied magnetic resonance》2010,38(4):431-442
The objective of this study is to determine differential diagnostic value of diffusion tensor imaging (DTI) in high-grade
brain astrocytomas, brain solitary metastases and brain abscesses. 53 patients with cerebral solitary lesions which showed
ring enhancement on contrast-enhanced T
1-weighted images were enrolled in this study. Brain tissues were examined pathologically from 49 patients to confirm the cerebral
occupational diseases. Four patients have been diagnosed with primary cancer plus brain solitary metastasis. DTI measurements
were obtained from regions of interest placed on central cavity, white matter of the immediate peritumoral region (IPR) and
cerebral white matter of the normal side. The cavity of high-grade astrocytoma and brain metastases displayed hypointense
signals; most of the brain abscess cavities displayed high signal intensity except for one case with uneven signal intensity.
Mean diffusivity (MD) and fractional anisotropy (FA) values could be used for differentiation between tumor and abscess in
brain. The brain abscess cavities showed restricted diffusion and anisotropy [MD = (0.604 ± 0.13) × 10−3 mm2/s, FA = 0.185 ± 0.03], whereas the central portion of high-grade astrocytoma [MD = (2.76 ± 0.26) × 10−3 mm2/s, FA = 0.069 ± 0.02] and solitary brain metastases [MD = (2.82 ± 0.29) × 10−3 mm2/s, FA = 0.064 ± 0.02] showed unrestricted diffusion and isotropy. Brain abscess could be differentiated by MD and FA values
in their cavities from brain tumors (P < 0.01). The IPRs were all depicted as hyperintense or isointense signals on diffusion-weighted imaging. The difference between
FA values in the IPR of high-grade brain astrocytomas and other groups was statistically significant (P < 0.01). In conclusion, our results suggested the potential role of the cavity MD and FA values in the differential diagnoses
of brain tumors and brain abscesses; meanwhile, high-grade astrocytomas could be distinguished from solitary metastases and
abscesses by evaluating their corresponding FA values in the IPR on brain magnetic resonance imaging (MRI). Combined with
conventional MRI, DTI may help radiologists to facilitate the differential diagnosis of ring-enhancing cerebral lesions in
clinical practice. 相似文献
958.
In this work, optical wavelet de-noising with several different types of wavelets such as db4, coif4 and dmey wavelet was applied at the end of the 40 Gbit/s multi-span intensity-modulated fiber communication systems. The results of numerical simulations carried out in different fiber links demonstrated that the optical wavelet de-noising method could remove the random amplitude fluctuation induced by the interaction of EDFA’s ASE noise and optical fiber’s dispersion and nonlinearity. The SNR and BER curves of the optical bit sequence without and with optical wavelet de-noising in dispersion compensation fiber link were plotted to show the effectiveness of the wavelet de-noising in the fiber-optic communication systems and wavelet de-noising with demy wavelet can achieve better result than with other type wavelet. 相似文献
959.
Laser conditioning of high-reflective and anti-reflective coatings in vacuum environments 总被引:1,自引:0,他引:1
Laser conditioning effects of the dielectric mirror coatings in vacuum environments were investigated. The laser-induced damage thresholds (LIDT) in vacuum environments before and after laser conditioning were compared. It is found that laser conditioning in vacuum environments decrease the LIDT of the component. Laser conditioning effects in vacuum and atmosphere environments were also compared and investigated. The negative effects of laser conditioning in vacuum environments were discussed and analyzed with defect statistical model, energy dispersive X-ray analysis and absorption measurements. 相似文献
960.
Based on studying the propagation states of electromagnetic waves in heterostructure coupled waveguides produced by appropriately modulating the refractive index of rods, the realization of photonic-crystal switch is analyzed and the position effect of the heterostructure coupled waveguides on the switch function is investigated. The simulation results show that the output state is the result of the integral effect of different coupling regions; therefore, the switch function is independent on the distribution of heterostructure coupled waveguides. This property will bring great flexibility to fabricate photonic-crystal switch in practice. 相似文献