新型金属杂冠醚配合物18-MC-6[Mn6(4-Amashz)6(DMF)6]·12DMF的合成

合成了一种新型金属杂冠醚配合物[Mn6(4-amashz)6(DMF)6]·12DMF,并用X射线衍射法对其结构进行了表征.研究了该化合物修饰金电极催化氧还原的性质,结果表明,该化合物具有平面碟状结构,对在碱性溶液中的氧有显著的催化还原作用.     

Relativistic Electromagnetic Solitary Wave in a Cylindrical Magnetized Plasma

In the presence of an applied static and uniform magnetic field, a cylindrical Kadomtsev-Petviashivili equation is derived for a relativistic electromagnetic solitary wave propagating in collisionless plasma consisting electrons, positrons, and ions in the case of weak relativistic limit. This equation is solved in a stationary frame to obtain explicit expression for the velocity, amplitude and width of solitons. The amplitude of the solitary wave has a maximum value at a critical αc of the ratio of the ion equilibrium density to the electron one, and it increases as the applied magnetic field becomes larger.     

Effect of Nonradiative Recombination on Carrier Dynamics in GaInNAs/GaAs Quantum Wells

The nonradiative recombination effect on carrier dynamics in GalnNAs/GaAs quantum wells is studied by timeresolved photoluminescence （TRPL） and polarization-dependent TRPL at various excitation intensities. It is found that both recombination dynamics and spin relaxation dynamics strongly depend on the excitation intensity. Under moderate excitation intensities the PL decay curves exhibit unusual non-exponential behaviour. This result is well simulated by a rate equation involving both the radiative and non-radiative recombinations via the introduction of a new parameter of the effective concentration of nonradiative recombination centres in the rate equation. In the spin dynamics study, the spin relaxation also shows strong excitation power dependence. Under the high excitation power an increase of spin polarization degree with time is observed. This new finding provides a useful hint that the spin process can be controlled by excitation power in GaInNAs systems.     

Web-Based Information Extraction Technology

Information extraction techniques on the Web are the current research hotspot. Now many information extraction techniques based on different principles have appeared and have different capabilities. We classify the existing information extraction techniques by the principle of information extraction and analyze the methods and principles of semantic information adding, schema defining,rule expression, semantic items locating and object locating in the approaches. Based on the above survey and analysis,several open problems are discussed.     

催化动力学光度法测定痕量铝

痕量铝在硝酸介质中能催化加速过氧化氢和高碘酸钾与二甲苯胺兰FF之间的褪色反应。研究了反应的最佳实验条件,建立了测定痕量铝的新方法。方法检出限为6.1×10-10gAl3+/mL,检测范围为0-1.0μgAl3+/25mL。本方法具有高灵敏度,选择性较好,操作简便,快速的特点。用以测定水样中的痕量铝,获得满意结果。     

一类仓库货物储存模型经典解的存在唯一性

文章用特征线法给出一类仓库货物储存模型解的递推表达式,并证明其光滑性从而得到了经典解的存在唯一性。     

辽宁男排跳发球技术分析

跳发球是现代排球比赛中一项攻击力很强的发球技术,为当今世界强队所广泛采用.采用高速摄影法和影片解析法,对在1997~1998年和1998~1999年全国排球联赛中两次获得最佳发球奖的李铁鸣的跳发球技术进行运动学分析,旨在揭示其技术的运动学特征,探讨影响动作效果的有关因素,为今后的教学和训练提供参考.     

斐索梯度折射率光纤透镜传感实验

采用LD泵浦的单纵模Nd：YVO4倍频激光器、梯度折射率光纤透镜等器件构成斐索梯度折射率光纤透镜传感实验仪．本文介绍了实验装置和实验原理，并给出了实验结果。     

体效应振荡器特性观测与使用实验教学研究

探讨了体效应振荡器特性观测与使用实验中，编写实验原理要应用能带结构解释负阻特性并通过对偶极畴生长和运动过程的描述说明振荡原理，提出了实验教学方案，从教学效果上分析了开设此实验的意义及合理性。     

脑膜瘤的CT、MRI表现与病理对照研究

目的：探讨脑膜瘤的CT、MRI表现与病理分型之间的关系．方法：收集经CT、MRI诊断和手术病理证实的脑膜瘤185例，CT和MRI检查均采用增强前后常规扫描，病理为手术巨检和切片光镜下所见．结果：典型脑膜瘤多为过渡型或纤维母细胞型脑膜瘤，密度(信号)均匀，明显均匀强化，15％～20％伴有钙化，无或轻度瘤周水肿．不典型脑膜瘤以合胞体和血管母细胞瘤型脑膜瘤为主，密度(信号)不均匀，无或不均匀强化，瘤周水肿较重．恶性脑膜瘤为混杂密度(信号)肿块，强化不均匀，形状不规则，瘤周水肿明显，伴有骨质破坏．结论：CT、MRI平扫 增强是诊断脑膜瘤的最主要方法，准确率为95％，在一定程度上可提示脑膜瘤的病理学分型，为术前选择手术方案及判定预后提供信息．