消色差谱相位延迟器的光谱特性测试研究

本文应用归一化偏振调制原理建立的测试系统，对常规菲涅耳菱体，改进型菲涅菱体，斜入射型以及直角棱镜组合型的消色差相位延迟的光谱特性进行了测试研究，得到了各延迟器的消色差特性曲线，并对测试结果进行了分析。结果表明改进型菲涅耳菱体以及直色棱镜组合型型消色差相位延迟器，是目前较理想的实用型消色相位延迟器。     

初中生学习化学兴趣的发展趋势

针对目前初中化学教学中学生因缺乏应有的学习兴趣而导致学习动力不足和影响其个性和谐发展的问题，运用现代教育学、心理学的理论，结合初中生的心理特点和化学学科特点，提出把初中生学习化学兴趣提到学生稳定的个性心理品质上来研究，是符合马克思主义关于人的学说和现代教育心理学理论以及初中化学教学实际的；初中生学习化学兴趣的形成和发展是一个立体发生的过程，其纵向趋势为：直感兴趣→解析兴趣→探索兴趣；其横向品质为：指向性、持久性、广泛性和有效性，初中生学习化学兴趣水平的提高应当在有效的教学中进行     

永磁同步直线电机弱磁调速时的设计

从凸极率角度出发，对内部磁极结构电机提出了新的设计方法，为使电机的特性具有可比性，假设电机均运行于相同的基值点，并采取相同的控制策略，着重了研究凸极率（ld/lq)对电机最大可能速度，逆变器功能（VA）和电流控制特性的影响，所得结论对电机及其驱动系统的选择和有积极的参考指导作用。     

关于山东土壤年龄的探讨

我们依据第四纪地质、考古和历史自然地理学资料,通过分析山东各类土壤母质的形成时期,推论各类土壤的成土年龄。认为一般情况下,山东土壤的年龄不大于2400年。     

A Novel Green Preparation of a, a''''-Bis (substituted benzylidene)-cycloalkanones Promoted by FeCl_3 6H-2O in Ionic Liquid

a, a'-Bis(substituted benzylidene)cycloalkanones were efficiently prepared from cycloalkanones and benzaldehydes in [bmim][BF4] by using iron(III) chloride hexahydrate as a catalyst. It is shown that [bmim][BF4] and iron(III) chloride hexahydrate can be quantitatively recovered and be reused effectively for many times. Compared with the known methods, this novel process has the advantage of being an envkonmentally benign process together with good yields and mild reaction conditions.     

Ce(H_2O)_7Al(OH)_6Mo_6O_(18)·4H_2O: A New One-dimensional Zigzag Chainlike Structure of Anderson Cluster Linked by Cerium Ions

IntroductionPolyoxometalates(POMs),as an important familyof metal oxides,have been receiving considerable at-tention in solid-state materials chemistry due to their di-verse topological properties and potential applications incatalysis,photochemistry,electrochemistry,medicineand magnetism[1,2].Recently,one of the intriguingfields in the polyoxometalate chemistry is to find somenovel subunits and then connect them into one-,two-,even three-dimensional(1-,2-,even3-D)extendednetworks,either thro…     

4′-乙酰基苯并-15-冠-5缩氨基硫脲的微波合成及晶体结构

硫脲衍生物主要通过氢键与阴离子相互作用达到识别的目的，冠醚和硫脲两个主体分子亚单元之间的协同作用往往使冠醚和硫脲表现出对某些客体更加优越的络合识别能力，我们在以前工作的基础上，微波辐射下合成了标题化合物并用红外光谱、核磁共振氢谱、元素分析、X射线单晶衍射对其结构进行了表征，欲进一步研究其对阳离子和阴离子识别的双重功效。     

尿中肌酐的流动注射分析

本文提出了一种简便快速的尿中肌酐的测定方法。采用空气整段间隔试样带的流动注射分析体系,在非化学反应平衡的条件下测定,尿样不经手工稀释可直接用于测定。测样频率每小时为90次,相对标准偏差为1.5%。     

利用天然斜发沸石从高离子强度的强碱性溶液中吸附和洗脱K+和Rb+的研究

在80℃下，用间歇法研究了NH4^ 型天然斜发沸石对某厂高离子 强碱性循环液中的K^ 和Rb^ 的吸附，得到不同粒度天然斜发沸石对K^ 和Rb^ 的交换吸附量，用不同浓度的NH4HCO3溶液对沸石进行洗脱再生，是到洗脱速率随着洗脱液浓度增大而增大。本文对沸石与钾含量很高的高离子强度强碱性溶液中碱金属的交换吸附和洗脱过程进行了初步探讨。     

A High Sensitivity Detection Method of Singlet Oxygen and Superoxide Anion

This paper, for the first time, reports a method that can be used as a highly sensitive probe for singlet oxygen (^1O2) and superoxide anion (O2^-) in vitro or in vivo. FCLA(3,7-dihydro-6-{4-[2-(N‘-(5-fluoresceinyl)thioureido)ethoxy]phenyl}-2-methylimidazo{1,2-a}pyrazin-3-one sodium salt), a chemiluminescence (CL) analysis reagent, has been reported to sensitively react with ^1O2 and O2^- to emit photons with a spectral peak of 525nm. In this work,when human serum albumin (HSA) was added into FCLA solution to enhance the CL intensity,approximately 20 times, compared to that without HSA. The enhanced CL had the same 525 nm spectral peak, identical to that without HSA. By gradually reducing the molecular oxygen content in the solution, we find that the auto-oxidation of oxygen molecules dissolved in the solution plays an important role in the CL process. Based on these experimental evidences, we propose a novel and highly sensitive detection method of ^1O2 and O2^- which may have a great potential in chemical and medical applications.