冠醚酮酸和烷酸的合成

本文介绍了在PPA存在下，由B15C5和DB18C6同过量的二羧酸发生酰化作用，得到酮酸1a～e和3a～c。再把所得相应的酮酸1a～e和3a～c利用黄鸣龙法制得4'-(ω－羧基多亚甲基)苯并-15-冠-5(2a～e)和4',4'(5')-二(ω-羧基多亚甲基)二苯并-18-冠-6(4a～c)等一系列ω-冠醚酮酸。     

芳基-芳基偶联反应的研究进展

综述了近年来芳基-芳基偶联反应的研究进展, 包括不同类型芳基-芳基偶联反应的特点、机理和应用, 尤其是对立体选择性和区域选择性的偶联方法进行了重点介绍.     

Physico-chemical Characterization of Mo-Hβ Zeolite Catalysts

A series of Mo-impregnated Hβ samples, with MoO3 loading in Hβ zeolite in the mass fraction range of 0. 5%-6.0%, were studied by means of XRD and IR in order to characterize their structures. Mo/Hβ sampies‘ crystallinity almost linearly decreases with increasing the amount of MoO3 loaded, The IR spectra and XRD patterns suggest that the progressive destabilization of the Hβ zeolite structure is caused by increasing Mo loading in (MoO3 Hβ zeolite). During the calcination, Al2(MoO4)3 formed from the dealumination of Hβ zeolite, causes the substantially partial breakdown of the zeolite framework when the Mo loading in MoO3 Hβ is relatively high.     

笃斯茎中六种无机元素含量分析

应用原子吸收光谱法测定了内蒙古地产的笃斯茎、叶中的Cu,Fe,Zn,Mn,Ca,Mg等六种人体必需微量元素及宏量元素的含量。从而为评价笃斯的品质及其药理、药效提供了具有一定价值的数据。     

单氧代-二硒烷基-1, w-二氧取代杯[4]衍生物的合成,结构及萃取性能研究

Novel macrocyclic monooxa-diselkylene-1,ω-dioxy substituted calix[4]arene derivatives 1a-5a were synthesized by the reaction of calix[4]arene dibromides 1-5 with the disodium salt of bis（2-selenylethyl）ether in the yields between 28% and 64%. Their structures were characterized by proton and carbon NMR spectra. X-Ray structure analysis of la further confirmed the cone conformation of compounds 1a-5a. An interesting host-guest complex of la with dichloromethane via CH/π and C1/π interactions was elucidated. Extraction experiments showed that these novel monooxa-diselkylene-1,ω-dioxy substituted calix[4]arene derivatives 1a-5a had strong extraction ability towards mercury ion. The interaction of Hg^2＋with the calix ligand has also been investigated by 1^H NMR titration.     

先进文化与东北老工业基地的振兴

老工业基地要实现振兴与发展，必须要有先进文化的指引，先进文化为企业提供振兴与发展的强大精神力量。先进文化有力地冲击旧体制、旧机制下形成的旧的思想观念，激发强烈的自主竞争意识，焕发创造潜能，营造以创新求发展的氛围。以先进文化为指引，企业才能获得有长久生命力的价值观，才能实现可持续发展。     

试论电子出版物呈缴制度设计的若干问题

通过对国外电子出版物呈缴制度建设特点和经验的分析,阐述了我国电子出版物呈缴制度的设计问题.     

萘与草酰氯反应机理的探讨

研究在N2气氛和无水AlCl3存在的条件下，萘与草酰氯反应。反应混合物GC／MS，GC／FTIR检测结果表明，该反应经历了碳正离子亲电取代-自由基取代反应历程，并讨论了催化剂AlCl3量对产物组成的影响。     

论大学英语情感教学

情感因素对大学英语课堂教学氛围有很大的影响,积极的情感和良好的氛围将有助于课堂教学效果的提高。在论述情感教学理论依据的基础上,分析了焦虑、自尊心、动机和移情等情感因素,对大学英语课堂教学的影响及教学策略,并对优化情感教学提出了四条建议。     

义务教育课程标准实验教科书·化学两版(人民教育出版社,上海教育出版社)之比较

义务教育课程标准实验教科书.化学是根据新课程标准编写而成的,并实行“一纲多本”,由人民教育出版社和上海教育出版社出版,并同时在全国不同的实验区供九年级学生使用。文章就两版教科书在内容,体系,版面设计,探究性等方面进行探讨和对比,得出结论:两版教科书都较好地体现了课程标准的思想,但就探究性而言,人教版的设计更为仔细,真正做到了以学生为主体。