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991.
992.
R. S. Dias A. P. Roque D. M. S. S. Vitti 《Journal of Radioanalytical and Nuclear Chemistry》2006,269(3):661-663
Summary The objective of this study was to determine endogenous phosphorus excretion in sheep fed with different diets. Sixteen male
growing sheep, received a basic diet with: 42% hydrolyzed sugarcane bagasse (HSB), 45% lucerne hay (LH) plus 14% hydrolyzed
sugarcane bagasse, and 30% citrus pulp (CTP) plus 40% hydrolyzed sugarcane bagasse. A dose of 7.7 MBq 32P was injected into the left jugular vein of each animal. The P endogenous fecal losses were: 1.69, 2.50, 2.33 and 1.45 g/animal
for treatments HSB, LH, and CTP respectively (P>0.05). The type of diet influenced slight endogenous P excretion but altered
excretion of P in urine. Endogenous P excreted in feces (PF) comes mainly from saliva and represents an important loss of P. The estimation of net requirements of phosphorus (P) for
ruminants includes endogenous losses, which is also essential for calculating true absorption of this mineral. Physical structure
of the feed may influence endogenous losses, altering the metabolism of P and also the demand of this mineral, therefore being
important to know how different feeds affect endogenous P losses. 相似文献
993.
Ngo Quang Huy Trinh Thi Bich Nguyen Van Suc 《Journal of Radioanalytical and Nuclear Chemistry》2006,269(1):129-133
Summary The paper presents a procedure to prepare soil samples for U and Th isotope measurement by alpha-spectrometry after coprecipitation
with LaF3. In this procedure the reduction of U(VI) to U(IV) was performed by Zn metal in 4M HCl solution. The recoveries of chemical
separation equal to eU-chemistry = 78±4% for uranium and eTh-chemistry = 82±4% for thorium. Canberra alpha-spectrometer was used with PIPS detectors of A-1200-37-AM Model of 1200 mm2 active area. The counting efficiency of the measuring system equals to ecounting = 18% and the total efficiencies were eU = ecounting .eU-chemistry = 14.0±0.7% for uranium and eTh = ecounting .eTh-chemistry = 14.7±0.7% for thorium. The recoveries of chemical separation were rather high (about 80%), that leads to the use of a small
weight of soil sample (about 0.5 g). The efficiencies were also stable, that allows analyzing the soil sample without using
radiotracers. They are advantages of the sample preparation procedure of this work. 相似文献
994.
A graphite electrode modified with cobalt hexacyanoferrate by mechanical immobilization was used for amperometric determination of hydrazine. The modified electrode exhibits good catalytic activity for the oxidation of hydrazine at a reduced overpotential with remarkable sensitivity. The modified electrode showed a linear response for hydrazine in the concentration range of 2.0 × 10–5 to 2.8 × 10–4 M. The detection limit was 9.8 × 10–6 M (S/N = 3). The proposed modified electrode was simple, sensitive, rapid, stable and promising. 相似文献
995.
D. P. Kozlenko S. E. Kichanov S. Lee J. -G. Park V. P. Glazkov B. N. Savenko 《JETP Letters》2006,83(8):346-350
The effect of a high pressure (up to 6 GPa) on the crystal and magnetic structure of the hexagonal manganite LuMnO3 is studied by neutron diffraction in the temperature range 10–295 K. It is found that, as the pressure increases, the ordered magnetic moment of Mn ions at T = 10 K decreases noticeably from 2.48 (0 GPa) to 1.98 μB (6 GPa). This decrease is due to an enhancement of the geometrical frustration effects on the triangular lattice. At the same time, the symmetry of the triangular antiferromagnetic state (the irreducible representation Γ2) remains unchanged. A correlation is revealed between the distortion parameter of the triangular lattice formed by Mn ions and the symmetry of the antiferromagnetic state of hexagonal manganites RMnO3. Based on this correlation, a generalized magnetic phase diagram of these compounds is constructed. The obtained phase diagram provides an explanation for the changes observed in the magnetic state of hexagonal manganites caused by high pressure and chemical substitution. 相似文献
996.
D. Liu Y. Li R. An Y. Dou H. Yang Q. Gong 《Applied Physics A: Materials Science & Processing》2006,84(3):257-260
We studied the influence of focusing depth on the index change threshold and damage threshold of silica glass irradiated by a focused 120 fs laser beam. Both thresholds increased with the focusing depth. The aspect ratio of the waveguide cross section can be selected by changing the focusing depth. A 5 mm long waveguide was written at the depth of 2100 μm, which was single mode at 632.8 nm and exhibited propagation loss of 0.56 dB/cm. The refractive index change was calculated to be ∼2.47×10-3. The influence of the focusing depth should be considered in multi-layer devices as shown in the fabrication of a 3×3 waveguide array. PACS 42.62.-b; 42.82.Et; 81.05.Kf 相似文献
997.
P. F. Mantica Jr. B. D. Kern B. E. Zimmerman W. B. Walters J. Rikovska N. J. Stone 《Hyperfine Interactions》1992,75(1-4):415-421
The performance of two external plastic scintillator detectors has been tested in an off-line mode using a source of106RuFe at UNISOR/NOF. The measurement of beta asymmetries at various temperatures has resulted in the reproduction of the previously-determined
magnetic dipole moment for the 1+ ground state of106Rh and in addition the conclusion that the sign of this moment is positive. 相似文献
998.
Summary Cold neutrons at the external neutron guide laboratory (ELLA) of the KFA Jülich are used to demonstrate their profitable application
for multielement characterization of biological materials. The set-up and experimental conditions of the Prompt Gamma Cold
Neutron Activation Analysis (PGCNAA) device is described in detail. Results for C, H, N, S, K, B, and Cd using synthetic standards
and the “ratio” technique for calculation are reported for several reference materials and prove the method to be reliable
and complementary with respect to the elements being determined by INAA.
IAEA fellow at the KFA from 6. 3. 91 to 2. 9. 91 on contract No. VIE/9016R. 相似文献
999.
Numerical methods for ordinary initial value problems that do not depend on special properties of the system are usually found in the class of linear multistage multivalue methods, first formulated by J.C. Butcher. Among these the explicit methods are easiest to implement. For these reasons there has been considerable research activity devoted to generating methods of this class which utilize independent function evaluations that can be performed in parallel. Each such group of concurrent function evaluations can be regarded as a stage of the method. However, it turns out that parallelism affords only limited opportunity for reducing the computing time with such methods. This is most evident for the simple linear homogeneous constant-coefficient test problem, whose solution is essentially a matter of approximating the exponential by an algebraic function. For a given number of stages and a given number of saved values, parallelism offers a somewhat enlarged set of algebraic functions from which to choose. However, there is absolutely no benefit in having the degree of parallelism (number of processors) exceed the number of saved values of the method. Thus, in particular, parallel one-step methods offer no speedup over serial one-step methods for the standard linear test problem. Although the implication of this result for general nonlinear problems is unclear, there are indications that dramatic speedups are not possible in general. Also given are some results relevant to the construction of methods.Work supported in part by National Science Foundation grants DMS 89 11410 and DMS 90 15533 and by US Department of Energy grant DOE DEFG02-87ER25026. Work of the second author was completed while at the University of Illinois. 相似文献
1000.
A. Ouardaoui D. M. Martino C. A. Steren H. van Willigen 《Applied magnetic resonance》1997,13(3-4):275-284
The mechanism of 4-chlorophenol (4CP) photolysis was investigated with the aid of Fourier Transform Electron Paramagnetic Resonance (FT-EPR) and pulsed-laser photolysis combined with High Performance Liquid Chromatography (HPLC) detection-of stable (diamagnetic) products. With FT-EPR transient free radicals produced by pulsed-laser excitation of solutions of 4CP in alcohols could be identified. Time profiles of the FT-EPR spectra provided information on reaction kinetics and Chemically Induced Dynamic, Electron Polarization (CIDEP) effects. It was found that 4CP photolysis in alcohols leads to the simultaneous formation of the phenoxyl radical and radicals produced by hydrogen abstraction from the solvent. CIDEP patterns establish that these radicals are formed in a reaction sequence involving a triplet state precursor and radical pair intermediate. Results of earlier transient optical absorption measurements indicate that the triplet precursor must be the carbene 4-oxocyclohexa-2,5-dienylidene. This assignment is supported by the finding that photolysis of quinone diazide in a hydrogen-donating solvent gives the same free radical products as those obtained from 4CP. The formation of the phenoxyl radical intermediate accounts for the finding that photolysis of deoxygenated solutions of 4CP in alcohols gives phenol as stable diamagnetic product. By contrast, photolysis of aerated and deoxygenated aqueous solutions of 4CP produces benzoquinone and hydroquinone as primary products, respectively. 相似文献