约束梁柱构件抗火性能研究进展

约束构件抗火性能和抗火设计是近年国内外相关学者关注的热点之一.笔者简要介绍了约束构件(包括约束梁、约束柱)抗火性能所取得的成果,总结了约束构件在火灾下的工作行为、抗火性能研究以及抗火设计方法的进展,指出了约束构件抗火研究目前存在的主要问题,并对下一步工作进行了展望.     

次条纹积分干涉计量

叙述了次条纹积分干涉干时的原理，仅用一幅光载频干涉纹图获取全部位相信息。先用分段积分法求出条纹初始位相，再由最小二乘原理，迭代出信息的位相解。并讨论了条纹位相的算法，误差修正和测量面形的应用。     

Characteristics of deep penetration laser welding of dissimilar metal Ni-based cast superalloy K418 and alloy steel 42CrMo

Experimental trials of autogenous deep penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 5.0 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser output power, welding velocity and defocusing distance on the morphology, welding depth and width as well as quality of the welded seam were investigated. Results show that full keyhole welding is not formed on both K418 and 42CrMo side, simultaneously, due to the relatively low output power. Partial fusion is observed on the welded seam near 42CrMo side because of the large disparity of thermal–physical and high-temperature mechanical properties of these two materials. The microhardness of the laser-welded joint was also examined and analyzed. It is suggested that applying negative defocusing in the range of Raylei length can increase the welding depth and improve the coupling efficiency of the laser materials interaction.     

非共轴激光雷达几何因子分析与测量

介绍了非共轴激光雷达几何因子的物理意义,分别通过理论分析和试验测量给出了求解几何因子的方法。结合自行研制的CSY-1便携式能见度激光雷达,将两种方法得到的几何因子进行对比,讨论了系统参数对几何因子的影响,从而实现了对激光雷达系统优化设计的可能性。     

晶体X射线衍射实验的数据分析模式

针对粉末X射线衍射谱分析软件CSM的特点,利用CSM软件附带的用户程序库功能,实现了固溶体的物相分析和固溶度的定量计算,扩展了CSM软件的使用范围,提高了物相分析的准确程度.     

Effects of initial crystal size of diamond powder on surface residual stress and morphology in polycrystalline diamond (PCD) layer

Polycrystalline diamond compacts (PDC) were synthesized using diamond powder of average crystal size 3-20 μm by the Ni 70 Mn 25 Co 5 alloy infiltration technique at high temperature and high pressure (HPHT).The surface residual stress of polycrystalline diamond (PCD) layer was measured using micro-Raman spectroscopy with hydrostatic stress model and X-ray diffraction (XRD).Measurements of the stress levels of PCDs show that the residual compressive stresses range from 0.12 to 0.22 GPa,which increase with th...     

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of γ-FeCr_0.29Ni_0.16C_0.06 austenite solid solution dendrites as the dominant and very small amount of super-fine dispersed Ni₃Al γ′ phase and Laves particles as well as MC needle-like carbides distributed in the interdendritic regions. Although the microhardness of the laser-welded seam was lower than that of the base metal, the strength of the joint was equal to that of the base metal and the fracture mechanism showed fine ductility.     

Theoretical study of the electronic ground states and low-lying singlet excited states of thiophene-based spirofluorenes

The electronic structures and optical properties of oligothiophene substituted spirofluorenes are investigated theoretically with semi-empirical quantum chemical calculations. A theoretical investigation of the interaction between two perpendicular π-systems of various oligothiophene substituted spirofluorenes is conducted. The results demonstrate that the interaction between two perpendicular branches is reduced by oligothiophene substitutions. Photoexcitation induced relaxation is mainly located on one of...     

Polaron effect dependence of thermopower in organic semiconductors

A unified physical model for thermopower was presented in organic semiconductors, based on the Marcus theory and variable-range hopping theory. According to the proposed model, the characteristic of charge carrier thermoelectric transport in organic semiconductors has been investigated. In particular, polaron effects, energetic disorder, and carrier density dependence of the thermopower have been discussed in detailed. The calculation also shows a good agreement with the experimental data in organic semiconductors.