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111.
A new ion-exchange adsorbent (IEA) derived from Fe(3)O(4)/SiO(2)-GPTMS-DEAE with paramagnetic properties was prepared. Fe(3)O(4) nanoparticles were firstly prepared in water-in-oil microemulsion. The magnetic Fe(3)O(4) particles were modified in situ by hydrolysis and condensation reactions with tetraethoxysilane (TEOS) to form the core-shell Fe(3)O(4)/SiO(2). The modified particles were further treated by 3-glycidoxypropyltrimethoxysilane (GPTMS) to form Fe(3)O(4)/SiO(2)-GPTMS nanoparticles. Fe(3)O(4)/SiO(2)-GPTMS-DEAE nanoparticles (IEA) were finally obtained through the condensation reaction between the Cl of diethylaminoethyl chloride-HCl (DEAE) and the epoxy groups of GPTMS in the Fe(3)O(4)/SiO(2)-GPTMS. The obtained IEA has features of paramagnetic and ion exchange properties because of the Fe(3)O(4) nanoparticles and protonated organic amine in the sample. The intermediates and final product obtained in the synthesis process were characterized. The separation result of genomic DNA from blood indicated that Fe(3)O(4)/SiO(2)-GPTMS-DEAE nanoparticles have outstanding advantages in operation, selectivity, and capacity. 相似文献
112.
Ding S Luan D Boey FY Chen JS Lou XW 《Chemical communications (Cambridge, England)》2011,47(25):7155-7157
We demonstrate a new hydrothermal method to directly grow SnO(2) nanosheets on a graphene oxide support that is subsequently reduced to graphene. This unique SnO(2)/graphene hybrid structure exhibits enhanced lithium storage properties with high reversible capacities and good cycling performance. 相似文献
113.
Wang Z Luan D Madhavi S Li CM Lou XW 《Chemical communications (Cambridge, England)》2011,47(28):8061-8063
Polycrystalline α-Fe(2)O(3) nanotubes with thin walls have been synthesized by one-step template-engaged precipitation of Fe(OH)(x) followed by thermal annealing. In virtue of the unique structural features, these α-Fe(2)O(3) nanotubes exhibit superior lithium storage capabilities with exceptional high-rate capacity retention as a potential anode material for lithium-ion batteries. 相似文献
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115.
为解决5G环境下高频次位置服务(location based service,LBS)带来的位置隐私暴露问题,分析了5G环境下移动用户位置隐私泄露风险,梳理了已有隐私保护技术,并对3类常见方法进行分析对比,针对5G环境下位置隐私保护面临的新挑战,提出了一种适合5G环境的隐私保护方法,即融合定位隐私保护方法.该方法通过降维初步处理、融合隐私算法及传输加密方法,在不提升复杂度的情况下,处理了从定位维度选择、定位中间过程乃至传输全链路的风险.仿真分析结果表明,该方法能在混合场景下实现高效的隐私保护,适用于5G超密集高频次位置服务. 相似文献
116.
Three-dimensional (3D) image reconstruction of an Hα flare near the solar disk center, is done by a series of line-center and off-line-center filtering observation, according to the physical meaning of contribution function based on the line formation theory. The contribution function represents the contribution from stellar atmospheric layers to the emergent specific intensity and describes the depth distribution of escape photons. In this paper, an Hα flare of 26 March 2001 is used to illustrate the 3D line-of-sight reconstruction and its development 相似文献
117.
The photorefractive planar lens for converting a vertical incident plane wave to a lateral-spread spherical wave and vice versa, is suggested. Using the two-beam coupled-wave theory, the coupled wave equations are derived and their half-analytical solutions are also given in terms of an infinite series. The diffraction properties (beam profiles, diffraction efficiency) of the local volume grating in the lens are presented. And the focusing property of the lens is discussed and compared with that of an ideal convergent spherical wave. It is demonstrated that the suggested photorefractive planar lens shows a good focusing effect. 相似文献
118.
本文阐述了浓香型白酒发酵池窖泥中兼性自养型链霉菌的分离及菌种鉴定的研究情况,对各菌种扩大培养最适液体培养基进行了选择,并探索了不同链霉菌发酵液对已酸梭菌,产酯酵母菌生长的促进作用及代谢的刺激作用。 相似文献
119.
非均质土体稳定性分析的广义极限平衡法及其应用 总被引:2,自引:0,他引:2
非均质土体稳定性分析是岩土工程中十分重要且非常复杂的课题,目前既缺乏严密的理论公式,也无统一的实用方法。本文运用拉格朗日乘子法,有机地将传统的极限平衡法与极限分析上限定理相结合,建立了一种既能考虑土料强度非线性特征,又适用于非均质剖面等的土建筑物及地基稳定性统一分析方法即广义极限平衡法,并比较严密地阐明了方法的物理基础与解答的性质。最后简要介绍了这种方法在非均质土坡稳定性、层状地基承载力与挡土墙土压力等方面应用所取得的一些数值结果与结论。 相似文献
120.