Characteristics of black carbon aerosol in Jiaxing,China during autumn 2013

We conducted measurements of black carbon（BC） aerosol in Jiaxing,China during autumn from September 26 to November 30,2013.We investigated temporal and diurnal variations of BC,and its correlations with meteorological parameters and other major pollutants.Results showed that hourly mass concentrations of BC ranged from 0.2 to 22.0 μg/m³,with an average of 5.1 μg/m³.The diurnai variation of BC exhibited a bimodal distribution,with peaks at 07:00 and 18:00.The morning peak was larger than the evening peak.The mass percentages of BC in PM_2.5 and PM₁₀ were 7.1%and 4.8%,respectively.The absorption coefficient of BC was calculated to be 44.4 Mm^-1,which accounted for 11.1%of the total aerosol extinction.BC was mainly emitted from local sources in southwestern Jiaxing where BC concentrations were generally greater than 11 μg/m³ during the measurement period.Correlation analysis indicated that the main sources of BC were motor vehicle exhaust,and domestic and industrial combustion.     

注重内涵,以创新求跨越,持续发展,建设国家物理学基础科学人才培养基地——中国科学技术大学国家物理学基础科学人才培养基地建设总结

介绍了中国科学技术大学国家物理学基础科学人才培养基地的建设经验.基地传承了“科学与技术、科研与教学、理论与实践”相结合的中国科学技术大学办学特色,充分发挥基地物理学科门类齐全、学风优良、师资力量雄厚的综合优势,以培养具有宽厚知识、创新能力和探索精神的创新人才为目标,对物理理论课和物理实验课课程体系、教学内容、教学方法等方面作了全面的改革,取得了显著成果.     

Gd2O3:Eu纳米晶的制备及其光谱性质研究

以EDTA为络合剂，聚乙二醇为有机分散剂，用络合溶胶—凝胶法制备出Gd2O3:Eu纳米晶。用XRD，SEM，X—射线能量色散谱仪(EDS)，荧光分光光度计等分析手段对Gd2O3:Eu的纳米晶结构、形貌、组分的均匀性以及发光特性进行了研究。结果表明：EDTA—M凝胶仅在800℃焙烧即可得到颗粒细小、组分均匀、纯立方相的Gd2O3:Eu纳米晶，颗粒基本呈球形，粒径为30nm左右。对样品的激发光谱、发射光谱测定表明：Gd2O3:Eu纳米晶在269nm光激发下发红光，发射光谱谱峰在611nm，与体材料基本相同；激发光谱中电荷迁移带(CTB)明显红移，从体材料的255nm移至269nm，移动了约14nm；猝灭浓度从体材料的6％提高到8％。     

制备介孔复合环境材料的酸洗刻蚀工艺

探索了一种制备介孔复合环境材料的方法--破坏式造孔与有机复合相结合,使最终产品可大量吸附污染水体中的各种污染物并具有一定的杀菌功能.该方法通过酸洗刻蚀,达到了去除原材料中的杂质和刻蚀孔径的目的,所制备的中间产品24h吸湿率为原材料的2倍,染料吸附量为原材料的1.6倍.     

利福平菌丝体厌氧生化处理的研究

制药厂生产利福平过程中产生大量的利福平菌丝体,可严重污染环境。用厌氧消化法处理利福平菌丝体,消化温度40℃,反应器容积负荷2KgCOD/m~3·d,液料滞留期(SRT)14～20天,取得了良好的处理效果。COD去除率稳定在90％左右,BOD_5去除率达到95％以上,产气率达到0.49m~3/去除KgCOD。     

常温条件下颗粒污泥处理含铅废水

对未经驯化的颗粒污泥处理含铅废水进行了初步实验研究.结果表明,颗粒污泥对含铅废水具有较高的去除能力,铅去除率在95%以上.颗粒污泥的加入量、废水酸度、沉降时间是影响处理效果的主要因素.通过对20mg/L的含铅试水进行处理,铅达到了排放标准.     

Degradation of 4-chlorophenol in aqueous solution by γ-radiation and ozone oxidation

The application of radiation technology in the en-vironmental protection was listed as one of the mostimportant research fields by the International AtomicEnergy Agency (IAEA) for the peaceful use of nuclearenergy. It has great research value and potential appli-cation. Because of their broad-spectrum antimicrobialproperties, Cholophenols (CPs) have been used aspreservative agents for wood, paints, vegetable fibersand leather and as disinfectants. In addition, they havebeen widely employed…     

A Novel Green Preparation of a, a''''-Bis (substituted benzylidene)-cycloalkanones Promoted by FeCl_3 6H-2O in Ionic Liquid

a, a'-Bis(substituted benzylidene)cycloalkanones were efficiently prepared from cycloalkanones and benzaldehydes in [bmim][BF4] by using iron(III) chloride hexahydrate as a catalyst. It is shown that [bmim][BF4] and iron(III) chloride hexahydrate can be quantitatively recovered and be reused effectively for many times. Compared with the known methods, this novel process has the advantage of being an envkonmentally benign process together with good yields and mild reaction conditions.     

尿中肌酐的流动注射分析

本文提出了一种简便快速的尿中肌酐的测定方法。采用空气整段间隔试样带的流动注射分析体系,在非化学反应平衡的条件下测定,尿样不经手工稀释可直接用于测定。测样频率每小时为90次,相对标准偏差为1.5%。     

利用天然斜发沸石从高离子强度的强碱性溶液中吸附和洗脱K+和Rb+的研究

在80℃下，用间歇法研究了NH4^ 型天然斜发沸石对某厂高离子 强碱性循环液中的K^ 和Rb^ 的吸附，得到不同粒度天然斜发沸石对K^ 和Rb^ 的交换吸附量，用不同浓度的NH4HCO3溶液对沸石进行洗脱再生，是到洗脱速率随着洗脱液浓度增大而增大。本文对沸石与钾含量很高的高离子强度强碱性溶液中碱金属的交换吸附和洗脱过程进行了初步探讨。