广西防城港市的族群认同(下)

从污名认同、中华民族认同、国家认同、政治政策认同、地域认同等方面对防城港市各族群的特殊认同方式进行了论述。     

配体二吡啶胺单氧化物的配位多样性(英文)

本文报道了以二吡啶胺单氧化物为配体的三个铜配合物的合成和X-射线衍射数据分析。在不同配位条件下,二吡啶胺单氧化物显示了配位多样性,配体酰胺上的氢原子发生转移或者消除,分子骨架在顺式和反式之间变换。此外,还发现了一个不同寻常的分子构型转换现象。     

化学镀法合成纳米Ag包覆Al_2O_3复合粉

以平均直径约为200nm的Al2O3粉为原料,以氨基溶液为镀液,硝酸银为初始材料,在反应过程中,控制最佳的还原剂浓度、反应时间等参量,使Al2O3表面获得均匀的金属Ag涂层·以HRTEM,XRD,EDS等手段研究了化学镀银所获得的Ag Al2O3复合粉的结构·结果表明,所有的Ag Al2O3复合粉具有壳 核结构,壳层由纳米非晶银和纳米银晶体颗粒构成,尺度分别是5nm和10nm·     

各向异性岩体破坏过程声发射测量及其定位实验研究

应用改进后的声发射设备,实验测量了花岗岩试样在单轴压缩加载条件下变形破坏过程中声发射现象;讨论分析了该试样损伤破坏过程中的诱发微裂纹相互作用、积累等.同时采用对速度结构依赖较少的相对定位方法,对非均质岩石试验中的声发射事件进行了定位研究.结果表明,相对定位方法可用于复杂试样和工程岩体的声发射事件定位,其可靠性及精度比以往有所提高,能够初步定量分析岩石在外载荷作用下的破坏过程的定位问题,对于工程岩体破坏问题分析具有很好的借鉴意义.     

An on-line scaling method for improving scalability of a database cluster

The explosive growth of the Internet and database applications has driven database to be more scalable and available，and able to support on-line scaling without interrupting service. To support more client’s queries without downtime and degrading the response time，more nodes have to be scaled up while the database is running. This paper presents the overview of scalable and available database that satisfies the above characteristics. And we propose a novel on-line scaling method. Our method improves the existing on-line scaling method for fast response time and higher throughputs. Our proposed method reduces unnecessary network use，i.e.，we decrease the number of data copy by reusing te backup data. Also，our on-line scaling operation can be processed parallel by selecting adequate nodes as new node. Our performance study shows that our method results in significant reduction in data copy time.     

广州夏季大气中碳气溶胶浓度水平及污染特征

2002年6-7月于广州市3个采样点采集PM10和PM25样品,测定了PM10,PM25以及元素碳(EC)和有机碳(OC)的浓度.PM10和PM2.5平均浓度分别为124.77μg@m-3及78.13μg@m-3.PM10和PM2.5中的OC浓度分别为22.3μg@m-3和15.80μg@m-3,EC浓度分别为7.78和5.90μg@m-3,其中73.8%的OC和77.7%的EC存在于PM25中.在3个采样点PM10和PM25中,OC/EC比值均大于2.0,表明广州夏季大气存在二次污染.各种气象条件对OC、EC浓度及其比值的变化都有不同程度的影响,其中降水和风速是OC、EC浓度变化的主要气象因素.     

裂变碎块角分布与鞍点结构

从Jacob和Wick所推导的具有自旋粒子的散射矩阵元一般表示式出发,采用适当近似后,分析了中子引起Th²³⁰,Th²³²,U²³⁴,U²³⁶,U²³⁸裂变的阈能附近碎块角分布的实验数据。分析结果说明:1)阈能附近碎块角分布可以用裂变是通过鞍点上少数转动带(每一带具有确定的宇称)来解释;2)这些转动带与Nilsson的渐近能谱图所预言的基本上一致。同时利用对称裂变鞍点比非对称裂变鞍点高的观点,讨论了裂变碎块角分布各向异性与质量比之间的关系。     

Enhanced Survivin siRNA Delivery Using Cationic Liposome Incorporating Fatty Acid-modified Polyethylenimine

We described a novel approach for survivin siRNA cellular delivery via a cationic liposome incorporating fatty acid-modified polyethylenimine. A linoleic acid derivative of branched polyethylenimine(PEI, M_w=25 kDa), PEI-LA, was synthesized and incorporated into the liposome. The properties of the liposome, cytotoxicity, cellular uptake of cancer cells for survivin siRNA, survivin protein downregulation levels were investigated. PEI-modified liposome showed a lower cytotoxicity and delivered survivin siRNA into HeLa cells and A549 cells efficiently compared with PEI-25kDa.     

金刚石钻进能量与花岗岩地层风化程度的关系

基于钻进过程监测系统在充填土-风化花岗岩地层中对液压旋转钻进的监测数据,对金刚石钻进系统的能量进行了分析.结果表明,钻进系统的能量分布与在普通风化花岗岩地层中的结果一致,黏滞能、动能以及钻进总能量与岩石的风化程度呈负相关,轴力功与岩石的风化程度呈正相关,说明金刚石钻进能量与岩石风化程度具有很好的响应关系.动能、轴力功及黏滞能受钻进方式影响,用于地层识别将受严格的可比条件限制.金刚石钻进比功随岩石风化程度的增强而减少,在不同风化程度的岩层中具有很好的分区性.而且,在充填土及全风化、强风化花岗岩地层中,金刚石旋转钻进比功值明显低于冲击凿碎比功,在微风化的坚硬岩中,旋转钻进比功则明显高于冲击凿碎比功.     

Synthetic Studies on Halichlorine and Pinnaic Acid. Stereospecific Preparation of the Azaspiro Core Structure

Halichlorine and Pinnaic acid are two novel marine natural products isolated from a Japanese sponge, and an Okinawan bivalve respectively. The unique azaspirl[4.5]decane-core structure prexent in both compounds provides a synthetic challenge, Herein, we describe a synthetic approach to the azaspiro[4.5]decane-core structure through an intramolecular[3+2] cycloaddition followed by an intra-molecular Michael addition and in situ isomerization to afford the azaspirocyclic core structures stereospecifically in 10 steps with 40% overall yield. Alternatively, the same core structure was achieved by tandem cycloaddition and isomerization approach.