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排序方式: 共有1155条查询结果,搜索用时 109 毫秒
31.
利用水蒸气蒸馏法提取马桑叶和茎中的挥发油,并采用气-质联用(GC-MS)方法对挥发油中化学成分进行分析.鉴定出了马桑叶和茎中的挥发油成分中的20及26种化合物,马桑叶挥发油中所鉴定出的主要成分为二苯胺和邻苯二甲酸异丁酯,含量分别为10.22%和10.07%.马桑茎挥发油中鉴定出的主要成分也为二苯胺和邻苯二甲酸异丁酯,但含量与马桑叶中不同,分别为1.61%和1.05%. 相似文献
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考虑了中立型随机时滞微分方程基于离散时间状态观测的反馈镇定问题.首先建立了受控系统均方指数稳定的充分条件,然后基于此用线性矩阵不等式方法设计了所需的离散时间的反馈控制器,最后举例说明了所得结果的有效性. 相似文献
34.
The relationship between crystal orientations and meso-mechanical properties of β phase Ti-7333 titanium was investigated through the combination of nanoindentation experiments and simulation. The crystal plasticity finite element(CPFE) model for nanoindentation of single body-centered cubic crystal was established based on the experimental data. And the crystal plasticity constitutive law was implemented to simulate the nanoindentation process, obtaining satisfied results with an acceptable error. From the simulated pileup morphology patterns with different crystal orientations, it was found that the β phase experienced a symmetrical and orientation-related deformation process. Meanwhile, the strain-rate sensitivity(SRS) of β phase was investigated through nanoindentation tests based on continuous stiffness measurement(CSM) under different strain rates,varying between 0.2, 0.05 and 0.01 s~(-1). Two grains with different orientations exhibited similar SRS exponents,m, calculated from the experimental results. 相似文献
35.
【目的】为了解岩溶区地下水水化学特征以及地下水成分的来源。【方法】以广西果化镇地下水为研究对象,于2017年7月共采集地下水样品21件,运用Gw_chart软件制作水化学Piper三线图,结合R软件进行相关性分析、主成分分析法、因子分析法等对数据进行处理。【结果】研究区岩溶地下水水化学类型主要为重碳酸-钙型水,Ca2+和Mg2+为地下水中主要阳离子,HCO-3和SO2-4为地下水中主要阴离子。HCO-3与Ca2+,Na++K+与Cl-,SO2-4与Mg+2、Ca2+,相关性较强,它们经历了相似的化学反应过程。通过主成分分析法提取了3个主成分,共解释了91%的方差,可以很好地代表原始数据;通过因子分析提取出3个公共因子,共解释了86%的方差。【结论】自然因素水-岩作用为水化学元素特征与来源主导因素,人类活动也起到了重要作用。 相似文献
36.
The efficient in‐situ reduction and cyclization reaction of aromatic aldehyde, 1,3‐cyclopentanedione (tetronic acid), and nitro‐compound under SnCl2·2H2O‐THF medium
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An efficient in‐situ reduction and cyclization reaction for the synthesis of pyrazolo[4,3‐f]quinoline, pyrazolo[3,4‐f]quinoline, and pyrazolo[3,2‐f]quinoline derivatives directly form 5‐nitroindazole, 6‐nitroindazole and 5‐nitroindole in the presence of SnCl2·2H2O was reported. Compared to traditional synthetic methods, this approach has the advantages of stable reagents, easy obtaining raw material, and high yields. In this research, SnCl2·2H2O is the efficient reducing agent for the in‐situ reduction and cyclization reaction of nitro‐compound. In addition, this process provided an alternative approach for the synthesis of target compounds. 相似文献
37.
JiGuang Lu Bo Peng Kuo Liu Peng Jiang YouLing Yue Meng Yu Ye-Zhao Yu FeiFei Kou Lin Wang 《中国科学:物理学 力学 天文学(英文版)》2019,(5)
Rotating radio transients(RRATs) are peculiar astronomical objects whose emission mechanism remains under investigation.In this paper, we present observations of three RRATs, J1538+2345, J1854+0306 and J1913+1330, carried out with the Fivehundred-meter Aperture Spherical radio Telescope(FAST). Specifically, we analyze the mean pulse profiles and temporal flux density evolutions of the RRATs. Owing to the high sensitivity of FAST, the derived burst rates of the three RRATs are higher than those in previous reports. RRAT J1854+0306 exhibited a time-dynamic mean pulse profile, whereas RRAT J1913+1330 showed distinct radiation and nulling segments on its pulse intensity trains. The mean pulse profile variation with frequency is also studied for RRAT J1538+2345 and RRAT J1913+1330, and the profiles at different frequencies could be well fitted with a cone-core model and a conal-beam model, respectively. 相似文献
38.
Two Pd(II)–NHC complexes bearing benzimidazole and pyridine groups have been successfully prepared and fully characterized by NMR and X‐ray diffraction analysis. The structure of palladium complexes are a typical square‐planar with palladium surrounded by two pairs of trans‐arranged benzimidazole and carbene ligands. The Pd–NHC complexes have been proved to be a highly efficient catalyst for the Mizoroki–Heck coupling reaction of aryl halides with various substituted acrylates under mild conditions in excellent yields. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
39.
Aequationes mathematicae - In this paper we study estimation, continuous dependence and Hyers–Ulam stability for continuous solutions of a second order iterative equation. First we give an... 相似文献
40.
Haoyue Shen Chun Kou Min He Han Yang Kuan Liu 《Journal of polymer science. Part A, Polymer chemistry》2014,52(6):739-751
Two novel anionic conjugated copolyelectrolytes PSDPPPV and PSDPPPE were synthesized via Heck/Sonogashira coupling reactions and characterized by FT‐IR, 1H NMR, UV‐vis, and PL spectroscopy. The two polymers are respectively constituted of 2,5‐diethoxy‐1,4‐phenyleneethynylene (DPV) and 2,5‐diethoxy‐1,4‐phenyleneethynylene (DPE) with 1,4‐diketo‐2,5‐bis(4‐sulfonylbutyl)‐3,6‐diphenylpyrrolo[3,4‐c]pyrrole (SDPP) which is a novel water soluble diketopyrrolopyrrole derivative. PSDPPPV and PSDPPPE show broad absorption band in visible region and they exhibit strong fluorescence quenching in aqueous solution. The fluorescence of their aqueous solutions can be enhanced in the presence of cationic surfactant or polymer nonionic surfactant. Fluorescence enhancement by introduction of polyvinylpyrrolidone (PVP) shows linear response. This result provides a controllable method to increase fluorescence intensity of dipyrrolopyrrole‐based conjugate polyelectrolytes in aqueous phase. The optical properties suggested that PSDPPPV and PSDPPPE which are negatively charged conjugated polymers can assemble with positively charged photovoltaic materials to form ionic photoactive layer. © 2013 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2014 , 52, 739–751 相似文献