黄磷废水处理系统中氰降解菌的筛选

首次对含有氰化物的黄磷废水进行了氰降解菌筛选优化,共得耐氰菌20株,其中有9株的降氰率在90％以上,且AB2001003菌株降氰率在97.1％以上.该菌能在72 h内使含CN~-50mg·L~(-1)的黄磷废水降至0.5 mg·L~(-1)以下,达到国家一级排放标准.该菌的最佳生长pH7.7,最佳温29℃.     

关于细集料砂当量指标的探讨

通过加土的方法得到不同泥土含量的集料，进行砂当量试验，并用不同砂当量值的集料制成成心性稀浆封层混合料进行湿轮磨耗试验，试验结果表明，砂当量与集料中的泥土含量存在良好的线性关系，是评价细集料洁净程度的有效方法，试验中集料级配和取样均匀程度会对试验结果产生一定影响，砂当量低的集料会使改性剂无法发 对心性稀浆封层混合料的改性效果，建议用于心性稀浆封层的的细集料砂当量不低于60％。     

时分复用倍乘光脉冲重复率的新型光纤耦合器环状连接法分析

提出并详细分析了一种基于时分复用技术倍乘光脉冲重复率的方法：在２×２光纤耦合器的一个输入口与一个输出口间，接入时延为脉冲列半周期奇数倍的一段光纤使之形成环状连接循环耦合，而在另一输出口获得光脉冲。详细分析了该系统中光纤耦合器耦合比、插入损耗、时延光纤长度的要求，偏差的影响及其调节法，给出了理论公式、结果的计算机模拟与实验介绍；与经典的马赫陈德尔干涉仪接法及近年提出的Ｓａｇｎａｃ环接法进行了比较。该方法特别适用于对窄脉冲列进行串接复用实现重复率的多次倍乘，从而得到数千兆赫至上百千兆赫的高重复率光脉冲     

双齿配位过渡金属化合物化学——Ⅲ.钒的邻巯基苯酚配合物的顺磁谱研究

测定了二个顺磁性化合物(Ph_1P)[V_2(mp)_6](Ⅰ)和(Ph_4P)_2[NaV(mp)_3 (MeCN)(MeOH)](Ⅱ)(H_2mp=邻巯基苯酚,o-HO_1C_6H_4SH)的固态和/或溶液中的顺磁波谱。(Ⅰ)的77K固态谱及(Ⅱ)的室温固态谱均经模拟计算,认为它们的钒原子处在S=l/2的Ⅰ=7/2状态,(Ⅱ)的低温(77K)溶液谱(乙腈)与Ⅱ的固态谱相同,均有特征的八条精细结构,认为非配对电子基本上定域在钒原子的周围。     

低噪音摩阻复台材料影响因素的探讨

采用动态粘弹谱仪（ＤＤＶ）、电子扫描显微镜（ＳＥＭ）和摩擦试验机等对影响摩阻复合材料制动噪音的因素进行了探讨。结果表明，摩阻材料基体的合理改性以提高其损耗角正切ｔａｎδ对减少振动、降低噪音行之有效。同时对传统解决噪音的方法，如添加固体润滑剂、橡胶共混等进行了分析比较。     

Use of a long-spacer-side-chain liquid crystalline polysiloxane containing a crown ether as a stationary phase for capillary gas chromatography

A new kind of side chain liquid crystalline polysiloxane containing a crown ether with a longer spacer (PSC-11) has been prepared and coated on a fused silica capillary column. The main chroma-tographic characteristics including efficiency, polarity, and selectivity have been examined. The phase exhibits the retention properties of both liquid crystal and crown ether stationary phases and possesses higher efficiency and better selectivity than PSC-3, which has a shorter spacer between the main polysiloxane chain and liquid crystalline side chain.     

精测安培表内阻的新方法——电桥伏安法

本文提出了精测安培表内阻的新方法,并将其与其它测量方法进行了比较。     

关于C_(11)A_7·CaF_2稳定性的研究

本文采用X射线衍射分析方法,研究了影响C_(11)A_7·CaF_2稳定性的因素,结果表明C_(11)A_7·CaF_2在1450℃以内,能够稳定存在;Mgo,K_2O对C_(11)A_7·CaF_2稳定性没有影响;Na_2O、P_2O_5和CaO能与C_(11)A_7·CaF_2发生反应、分别生成少量NC_6A_3、Ca_5F(PO_4)_3和C_3A,但在硅酸盐水泥熟料的正常煅烧制度下,反应程度较低,对C_(11)A_7·CaF_2稳定性不大.熟料中铝酸盐相存在的形式,主要取决于氟在熟料中的分布,CaF_2掺量较低,温度超过1350℃,C_(11)A_7CaF_2消失,生成C_3A;CaG_2掺量较高时,温度高达1450℃,熟料中的铝酸盐相仍为C_(11)A_7·CaF_2,而不生成C_2A.     

Synthesis and characterization of novel thermoresponsive‐co‐biodegradable hydrogels composed of N‐isopropylacrylamide,poly(L‐lactic acid), and dextran

A series of novel multifunctional hydrogels that combined the merits of both thermoresponsive and biodegradable polymeric materials were designed, synthesized, and characterized. The hydrogels were copolymeric networks composed of N‐isopropylacrylamide (NIPAAM) as a thermoresponsive component, poly(L‐lactic acid) (PLLA) as a hydrolytically degradable and hydrophobic component, and dextran as an enzymatically degradable and hydrophilic component. The chemical structures of the hydrogels were characterized by an attenuated total reflection–Fourier transform infrared spectroscopy (ATR–FTIR) technique. The hydrogels were thermoresponsive, showing a lower critical solution temperature (LCST) at approximately 32 °C, and their swelling properties strongly depended on temperature changes, the balance of the hydrophilic/hydrophobic components, and the degradation of the PLLA component. The degradation of the hydrogels caused by hydrolytic cleavage of ester bonds in the PLLA component was faster at 25 °C below the LCST than at 37 °C above the LCST, determined by the ATR–FTIR technique. Due to their multifunctional properties, the designed hydrogels show great potential for biomedical applications, including drug delivery and tissue engineering. © 2004 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 42: 5054–5066, 2004     

有界域上具有离散全纯核的Koppelman公式与-方程

D是Cn空间中具有逐块C(1)边界的有界域,该文建立了D上一个具有离散局部全纯核的 (0,q)形式的Koppelman积分公式及其相应的■-方程解的积分表示和它的内闭一致估计式.